IP Library Granted Patent US 9,090,851
Granted Patent B2
US 9,090,851 · App. 13/801,296 · Granted Jul 28, 2015

Oil extraction method and composition for use in the method

Inventors: Dean Blankenburg (West Bend, WI); Clayton Lepak (West Bend, WI); Dave Parkinson (West Bend, WI)
Assignee: Hydrite Chemical Co.
C11B13/00B01D17/04B01D17/047B01F17/0071
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Quick Facts
Patent No.
US 9,090,851
App. No.
13/801,296
Granted
Jul 28, 2015
Kind
B2
Abstract

A composition is disclosed for aiding extraction of an emulsified oil from an oil and water emulsion. The composition includes silicon containing particles at a level of 0.1 wt. % to 30 wt. %; an emulsifying agent at a level of 1 wt. % to 30 wt. %; and water at a level of 40 wt. % to 99 wt. %. A method of extracting oil from an oil and water emulsion in a material is also disclosed. The method includes the steps of (a) dispersing silicon containing particles into the material using a mechanical blending device; and (b) separating the oil from the material. A method of extracting oil from an oil and water emulsion in a material is also disclosed. The method includes the steps of (a) providing a dispersion of silicon containing particles in water; (b) metering the dispersion into the material; and (c) separating the oil from the material.

Claims (58)

1. A composition for aiding extraction of an emulsified oil from an oil and water emulsion, the composition comprising:

silicon containing particles at a level of 0.1 wt. % to 30 wt. %;

an emulsifying agent at a level of 1 wt. % to 30 wt. %; and

water at a level of 40 wt. % to 99 wt. %,

wherein the emulsifying agent is a polysorbate, and

wherein the silicon containing particles are dispersed in the water.

2. The composition of claim 1 wherein:

the silicon containing particles are present at greater than 5 wt. % to 15 wt. %;

the emulsifying agent is present at a level of 4 wt. % to 15 wt. %; and

water is present at a level of 70 wt. % to 90 wt. %.

3. The composition of claim 1 wherein:

the silicon containing particles are selected from the group consisting of silica, talc, clay, quartz, diatomaceous earth, and mixtures thereof.

4. The composition of claim 1 wherein:

the silicon containing particles are precipitated silica particles.

5. The composition of claim 4 wherein:

the silicon containing particles are hydrophilic.

6. The composition of claim 1 wherein:

the silicon containing particles have an average particle size of less than 100 micrometers.

7. A method of extracting oil from an oil and water emulsion in a material, the method comprising:

(a) dispersing hydrophilic silicon containing particles and a polysorbate into the material using a mechanical blending device; and

(b) separating the oil from the material.

8. The method of claim 7 wherein:

the silicon containing particles are selected from the group consisting of silica, talc, clay, quartz, diatomaceous earth, and mixtures thereof.

9. The method of claim 7 wherein:

the silicon containing particles are precipitated silica particles.

10. The method of claim 7 wherein:

the silicon containing particles have an average particle size of less than 20 micrometers.

11. The method of claim 7 wherein:

the mechanical blending device is selected from a dry blending hopper, a tri-blender, and physical addition.

12. The method of claim 7 wherein:

the oil is selected from the group consisting of vegetable oils, animal fats, and petroleum oil.

13. The method of claim 7 wherein:

the oil and water emulsion comprises a vegetable oil and/or an animal fat emulsified by a biological surfactant comprising phospholipids and proteins.

14. The method of claim 7 wherein:

the oil is corn oil, and

step comprises (b) centrifuging the material to separate the oil.

15. The method of claim 14 wherein:

the material is whole stillage, thin stillage, or thick stillage.

16. A method of extracting oil from an oil and water emulsion in a material, the method comprising:

(a) providing a dispersion of silicon containing particles and a polysorbate in water;

(b) metering the dispersion into the material; and

(c) separating the oil from the material.

17. The method of claim 16 wherein:

the silicon containing particles are selected from the group consisting of silica, talc, clay, diatomaceous earth, and mixtures thereof.

18. The method of claim 16 wherein:

the silicon containing particles are precipitated silica particles.

19. The method of claim 18 wherein:

the silicon containing particles are hydrophilic.

20. The method of claim 16 wherein:

the silicon containing particles have an average particle size of less than 20 micrometers.

21. The method of claim 16 wherein:

the silicon containing particles are present in the dispersion at up to 15 wt. %.

22. The method of claim 16 wherein:

step (a) comprises dispersing the silicon containing particles under high shear.

23. The method of claim 16 wherein:

the dispersion includes a suspending agent, the suspending agent is selected from gums or celluloses.

24. The method of claim 16 wherein:

the dispersion comprises silicon containing particles at a level of greater than 5 wt. % to 15 wt. %, the polysorbate at a level of 4 wt. % to 15 wt. %, and water at a level of 70 wt. % to 90 wt. %.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 2, 2013
From: BLANKENBURG, DEAN; PARKINSON, DAVE; LEPAK, CLAYTON
To: HYDRITE CHEMICAL CO.
Reel/Frame 030930/0380 →
Continuity (1)
Related Publication 20140275589A1 · Sep 18, 2014