IP Library Granted Patent US 9,233,368
Granted Patent B2
US 9,233,368 · App. 13/477,332 · Granted Jan 12, 2016

Moisture-activated self-heating analysis device

Inventors: Haim H. Bau (Swarthmore, PA); Changchun Liu (Philadelphia, PA); Michael G. Mauk (Wilmington, DE); Robert W. Hart (Philadelphia, PA); Xianbo Qiu (Philadelphia, PA)
Assignee: The Trustees Of The University Of Pennsylvania
B01L3/5027B01L7/525C12Q1/6806B01L3/502707B01L2200/148B01L2300/0681B01L2400/0406B01L2400/0481
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Quick Facts
Patent No.
US 9,233,368
App. No.
13/477,332
Granted
Jan 12, 2016
Kind
B2
Abstract

Provided are disposable, moisture-activated, self-heating cartridges useful for, e.g., isothermal nucleic acid amplification, incubation, and thermal actuation, and visual fluorescent detection of the amplification products. These devices may be self-contained and do not require any special instruments to operate.

Claims (18)

1. A device, comprising:

a heating material that undergoes an exothermic reaction upon contact with moisture;

a thermal storage medium in thermal communication with the moisture-activated heating source, the thermal storage medium comprising a phase-changing material; and

a conduit placing the heating material in fluid communication with a reservoir adapted to contain a fluid, the conduit comprising a material capable of transporting liquid by capillary action,

wherein the heating material is in thermal communication with an enzymatic amplification reaction chamber, a thermally-actuated fluidic element, or any combination thereof.

2. The device of claim 1 , wherein the conduit comprises a fibrous material.

3. The device of claim 2 , wherein the fibrous material comprises filter paper, cellulose, polytetafluoroethylene (PTFE), nitrocellulose, an acrylic copolymer, polypropylene, polyethylene, polyvinylidene fluoride (PVDF), or any combination thereof.

4. The device of claim 1 , wherein the conduit comprises a material comprising two or more different fiber sizes, two or more different pore sizes, or both.

5. The device of claim 1 , wherein the enzymatic amplification chamber is adapted for isothermal amplification.

6. A device, comprising:

a heating material that undergoes an exothermic reaction upon contact with moisture;

a thermal storage medium in thermal communication with the moisture-activated heating source, the thermal storage medium comprising a phase-changing material; and

a conduit placing the heating material in fluid communication with a reservoir adapted to contain a fluid, the conduit comprising a material capable of transporting liquid by capillary action,

wherein the heating material is in thermal communication with an incubation and culture growth reaction chamber, a thermally-actuated fluidic element, or any combination thereof.

7. The device of claim 1 , wherein the thermally-actuated fluidic element comprises a valve, a piston, a membrane, a cantilever, thermally-releasable reagents, or any combination thereof.

8. The device of claim 1 , wherein the thermal storage medium comprises a wax, a thermoplastic, a salt hydrate, a fatty acid, a fatty acid ester, or any combination thereof.

9. The device of claim 1 , wherein the heating material comprises magnesium-iron alloy, calcium oxide, sodium acetate, potassium permanganate, or any combination thereof.

10. The device of claim 6 , wherein the thermally-actuated fluidic element comprises a valve, a piston, a membrane, a cantilever, thermally-releasable reagents, or any combination thereof.

Assignments (2)
CONFIRMATORY LICENSE Recorded Mar 6, 2015
From: UNIVERSITY OF PENNSYLVANIA
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 035155/0402 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2012
From: BAU, HAIM H.; LIU, CHANGCHUN; MAUK, MICHAEL G.; HART, ROBERT W.; QIU, XIANBO
To: THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
Reel/Frame 028850/0340 →
Continuity (2)
Provisional Application 61488823 · May 23, 2011
Related Publication 20120315638A1 · Dec 13, 2012