IP Library Granted Patent US 9,254,334
Granted Patent B2
US 9,254,334 · App. 14/575,555 · Granted Feb 9, 2016

Polyamine derivatives

Inventors: Gregory Slobodkin (Huntsville, AL); Richard Congo (Huntsville, AL); Majed Matar (Madison, AL); Jason Fewell (Madison, AL); Khursheed Anwer (Madison, AL); Brian Jeffery Sparks (Huntsville, AL)
Assignee: CLSN Laboratories, Inc.
A61K47/48061A61K9/1272A61K31/7088A61K31/713A61K47/16A61K47/48038A61K47/48815A61K47/48946C07C233/38C07C235/10C07C235/60C07D475/04C07H15/10C07K7/23C07K7/64
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Quick Facts
Patent No.
US 9,254,334
App. No.
14/575,555
Granted
Feb 9, 2016
Kind
B2
Abstract

Disclosed are compounds, compositions and methods for systemic and local delivery of biologically active molecules.

Claims (36)

1. A method for treating a disease in a mammalian subject, said method comprising administering to the subject a therapeutically effective amount of a formulation comprising a biologically active molecule, a compound of Formula A and a compound of Formula B:

wherein n1, n2, and n3 in both Formula A and Formula B are independently 1, 2, 3, or 4;

X and X′ in both Formula A and Formula B are independently a bond, oxygen, or nitrogen;

R 1 and R 2 in both Formula A and Formula B are independently C 8 -C 25 hydrocarbon groups optionally containing from 1-4 double or triple bonds;

in Formula A, G is hydrogen; and

in Formula B, G is a polyoxyalkylene, polyvinylpyrrolidone, polyacrylamide, polydimethylacrylamide, polyvinyl alcohol, dextran, poly (L-glutamic acid), styrene maleic anhydride, poly-N-(2-hydroxypropyl) methacrylamide, or polydivinylether maleic anhydride;

and wherein the biologically active molecule is selected from the group consisting of:

ribosomal RNA; antisense polynucleotides of RNA or DNA; ribozymes; siRNA; shRNA; miRNA;

and polynucleotides of genomic DNA, cDNA, or mRNA that encode for a therapeutically useful protein.

2. The method according to claim 1 , wherein in Formula B, G is a polyoxyalkylene.

3. The method according to claim 2 , wherein the polyoxyalkylene is a polyoxyethylene.

4. The method according to claim 1 , wherein the compound of Formula A is dioleoyl monoamine and the compound of Formula B is mPEG-dioleoyl monoamine.

5. The method according to claim 1 , wherein n1, n2, and n3 in both Formula A and Formula B are all 1, and X and X′ in both Formula A and Formula B are bonds.

6. The method according to claim 1 , wherein R 1 and R 2 in both Formula A and Formula B are independently C 14 -C 20 hydrocarbon groups containing 1 double bond.

7. The method according to claim 6 , wherein —C(O)X—R 1 and —C(O)X′—R 2 in both Formula A and Formula B are oleoyl groups.

8. The method according to claim 1 , wherein the disease is characterized by unregulated cell growth in the subject.

9. The method according to claim 8 , wherein the disease is cancer.

10. The method according to claim 9 , wherein the disease is lung cancer.

11. The method according to claim 1 , wherein the formulation is administered to said mammalian subject orally, topically, parenterally, by inhalation, or rectally.

12. The method according to claim 1 , wherein the formulation comprises particles comprising the biologically active molecule, the compound of Formula A, and the compound of Formula B.

13. The method according to claim 12 , wherein the particles have a median diameter of less than about 500 nm.

14. The method according to claim 1 , wherein the formulation comprises a pharmaceutically acceptable excipient.

15. A method for treating a disease in the lung tissue of a mammalian subject, said method comprising administering to the subject a therapeutically effective amount of a formulation comprising a biologically active molecule, a compound of Formula A and a compound of Formula B:

wherein n1, n2, and n3 in both Formula A and Formula B are independently 1, 2, 3, or 4;

X and X′ in both Formula A and Formula B are independently a bond, oxygen, or nitrogen;

R 1 and R 2 in both Formula A and Formula B are independently C 8 -C 25 hydrocarbon groups optionally containing from 1-4 double or triple bonds;

in Formula A, G is hydrogen; and

in Formula B, G is a polyoxyalkylene, polyvinylpyrrolidone, polyacrylamide, polydimethylacrylamide, polyvinyl alcohol, dextran, poly (L-glutamic acid), styrene maleic anhydride, poly-N-(2-hydroxypropyl) methacrylamide, or polydivinylether maleic anhydride;

and wherein the biologically active molecule is selected from the group consisting of:

ribosomal RNA; antisense polynucleotides of RNA or DNA; ribozymes; siRNA; shRNA; miRNA;

and polynucleotides of genomic DNA, cDNA, or mRNA that encode for a therapeutically useful protein.

16. The method according to claim 15 , wherein the compound of Formula A is dioleoyl monoamine and the compound of Formula B is mPEG-dioleoyl monoamine.

17. The method according to claim 15 , wherein the disease is lung cancer.

18. The method according to claim 15 , wherein the formulation is administered to said mammalian subject orally, topically, parenterally, by inhalation, or rectally.

19. The method according to claim 15 , wherein the formulation comprises particles comprising the biologically active molecule, the compound of Formula A, and the compound of Formula B.

20. The method according to claim 19 , wherein the particles have a median diameter of less than about 500 nm.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 2, 2015
From: EGEN, INC.
To: CLSN LABORATORIES, INC.
Reel/Frame 036938/0464 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 2, 2015
From: SLOBODKIN, GREGORY; CONGO, RICHARD; MATAR, MAJED; FEWELL, JASON; ANWER, KHURSHEED; SPARKS, BRIAN JEFFERY
To: EGEN, INC.
Reel/Frame 037034/0189 →
Continuity (4)
Division 13791102 · Mar 8, 2013
Division 12727987 · Mar 19, 2010
Provisional Application 61161828 · Mar 20, 2009
Related Publication 20150099000A1 · Apr 9, 2015