IP Library Granted Patent US 9,328,111
Granted Patent B2
US 9,328,111 · App. 14/369,388 · Granted May 3, 2016

Substituted cycloocta[5,6]pyrido[4,3,2-de]phthalazines as PARP inhibitors

Inventors: Changyou Zhou (Princeton, NJ); Bo Ren (Beijing, CN); Hexiang Wang (Beijing, CN)
Assignee: BeiGene Ltd.
C07D471/14C07D471/04C07D471/06C07D471/16
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Quick Facts
Patent No.
US 9,328,111
App. No.
14/369,388
Granted
May 3, 2016
Kind
B2
Abstract

The present invention provides a compound of Formula (I): wherein the variables Z, n, Y and p are as defined herein, and pharmaceutically acceptable salts thereof, which can inhibit the activity of poly (ADP-ribose)polymerases, and pharmaceutical compositions comprising the same.

Claims (37)

1. A compound of Formula (I):

or a pharmaceutically acceptable salt thereof,

wherein:

Y, at each occurrence, is independently selected from —CR 1 R 2 ;

p is 5;

Z, at each occurrence, is independently selected from hydrogen, halogen, alkyl, alkenyl, alkynyl, cycloalkyl, aryl, heterocyclyl, heteroaryl, —CN, —NO 2 , —OR 6 , —NR 6 R 7 , —NR 6 COR 7 , —NR 6 —NR 7 COR 8 , —NR 6 SO 2 R 7 , —CONR 6 R 7 , —COOR 6 , and —SO 2 R 6 , wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted with at least one substituent R 9 ;

n is 0, 1, 2 or 3;

R 1 and R 2 , which may be the same or different, are each selected from hydrogen, halogen, alkyl, alkenyl, alkynyl, cycloalkyl, aryl, heterocyclyl, heteroaryl, —NR 6 R 7 , —OR 6 , —COR 6 , —CO 2 R 6 , —CONR 6 R 7 , —NR 6 CONR 7 R 8 , —NR 6 CO 2 R 7 , —NR 6 SO 2 R 7 , and —SO 2 R 6 , wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted with at least one substituent R 9 ;

R 6 , R 7 and R 8 , which may be the same or different, are each selected from hydrogen, alkyl, alkenyl, alkynyl, cycloalkyl, heterocyclyl, aryl, and heteroaryl, wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted by at least one substituent R 9 ; and

R 9 , at each occurrence, is independently selected from halogen, haloalkyl, alkyl, alkenyl, cycloalkyl, aryl, heteroaryl, heterocyclyl, alkynyl, oxo, —CN, —OR′, —NR′R″, —COR′, —CO 2 R′, —CONR′R″, —C(═NR′)NR″R′″, —NR′COR″, —NR′CONR′R″, —NR′CO 2 R″, —SR′, —SOR′, —SO 2 R′, —NR′SO 2 NR″R′″, and NR′SO 2 R″, wherein R′, R″, and R′″ are independently selected from hydrogen, haloalkyl, alkyl, arylalkyl, alkenyl, alkynyl, cycloalkyl, heterocyclyl, aryl, and heteroaryl.

2. The compound of claim 1 , which is a compound of Formula (II-1):

or a pharmaceutically acceptable salt thereof,

wherein

p is 5;

Z, is selected from hydrogen, halogen, alkyl, alkenyl, alkynyl, cycloalkyl, aryl, heterocyclyl, heteroaryl, —CN, —NO 2 , —OR 6 , —NR 6 R 7 , —NR 6 COR 7 , —NR 6 —NR 7 COR 8 , —NR 6 SO 2 R 7 , —CONR 6 R 7 , —COOR 6 , and —SO 2 R 6 , wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted with at least one substituent R 9 ;

R 1 and R 2 , which may be the same or different, are each selected from hydrogen, halogen, alkyl, alkenyl, alkynyl, cycloalkyl, aryl, heterocyclyl, heteroaryl, —NR 6 R 7 , —OR 6 , —COR 6 , —CO 2 R 6 , —CONR 6 R 7 , —NR 6 CONR 7 R 8 , —NR 6 CO 2 R 7 , —NR 6 SO 2 R 7 , and —SO 2 R 6 , wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted with at least one substituent R 9 ;

R 6 , R 7 and R 8 , which may be the same or different, are each selected from hydrogen, alkyl, alkenyl, alkynyl, cycloalkyl, heterocyclyl, aryl, and heteroaryl, wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted by at least one substituent R 9 ; and

R 9 , at each occurrence, is independently selected from hydrogen, halogen, haloalkyl, alkyl, alkenyl, cycloalkyl, aryl, heteroaryl, heterocyclyl, alkynyl, oxo, —CN, —OR′, —NR′R″, —COR′, —CO 2 R′, —CONR′R″, —C(═NR′)NR″R′″, —NR′COR″, —NR′CONR′R″, —NR′CO 2 R″, —SR′, —SOR′, —SO 2 R′, —NR′SO 2 NR″R′″, and NR′SO 2 R″, wherein R′, R″, and R′″ are independently selected from hydrogen, haloalkyl, alkyl, arylalkyl, alkenyl, alkynyl, cycloalkyl, heterocyclyl, aryl, and heteroaryl.

3. The compound of claim 1 , which is a compound of Formula (II-2):

or a pharmaceutically acceptable salt thereof,

wherein

p is 5;

Z is selected from hydrogen, halogen, alkyl, alkenyl, alkynyl, cycloalkyl, aryl, heterocyclyl, heteroaryl, —CN, —NO 2 , —OR 6 , —NR 6 R 7 , —NR 6 COR 7 , —NR 6 —NR 7 COR 8 , —NR 6 SO 2 R 7 , —CONR 6 R 7 , —COOR 6 , and —SO 2 R 6 , wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted with at least one substituent R 9 ;

R 1 and R 2 , which may be the same or different, are each selected from hydrogen, halogen, alkyl, alkenyl, alkynyl, cycloalkyl, aryl, heterocyclyl, heteroaryl, —NR 6 R 7 , —OR 6 , —COR 6 , —CO 2 R 6 , —CONR 6 R 7 , —NR 6 CONR 7 R 8 , —NR 6 CO 2 R 7 , —NR 6 SO 2 R 7 , and —SO 2 R 6 , wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted with at least one substituent R 9 ;

R 6 , R 7 and R 8 , which may be the same or different, are each selected from hydrogen, alkyl, alkenyl, alkynyl, cycloalkyl, heterocyclyl, aryl, and heteroaryl, wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted by at least one substituent R 9 ; and

R 9 , at each occurrence, is independently selected from halogen, haloalkyl, alkyl, alkenyl, cycloalkyl, aryl, heteroaryl, heterocyclyl, alkynyl, oxo, —CN, —OR′, —NR′R″, —COR′, —CO 2 R′, —CONR′R″, —C(═NR′)NR″R′″, —NR′COR″, —NR′CONR′R″, —NR′CO 2 R″, —SR′, —SOR′, —SO 2 R′, —NR′SO 2 NR″R′″, and NR′SO 2 R″, wherein R′, R″, and R′″ are independently selected from hydrogen, haloalkyl, alkyl, arylalkyl, alkenyl, alkynyl, cycloalkyl, heterocyclyl, aryl, and heteroaryl.

4. The compound of claim 1 , which is a compound of Formula (II-3):

or a pharmaceutically acceptable salt thereof,

wherein

p′ is 3;

Z is selected from the group consisting of hydrogen, halogen, alkyl, alkenyl, alkynyl, cycloalkyl, aryl, heterocyclyl, heteroaryl, —CN, —NO 2 , —OR 6 , —NR 6 R 7 , —NR 6 COR 7 , —NR 6 —NR 7 COR 8 , —NR 6 SO 2 R 7 , —CONR 6 R 7 , —COOR 6 , and —SO 2 R 6 , wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted with at least one substituent R 9 ;

R 1 and R 2 , which may be the same or different, are each selected from hydrogen, halogen, alkyl, alkenyl, alkynyl, cycloalkyl, aryl, heterocyclyl, heteroaryl, —NR 6 R 7 , —OR 6 , —COR 6 , —CO 2 R 6 , —CONR 6 R 7 , —NR 6 CONR 7 R 8 , —NR 6 CO 2 R 7 , —NR 6 SO 2 R 7 , and —SO 2 R 6 , wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted with at least one substituent R 9 ;

R 6 , R 7 and R 8 , which may be the same or different, are each selected from hydrogen, alkyl, alkenyl, alkynyl, cycloalkyl, heterocyclyl, aryl, and heteroaryl, wherein each of the alkyl, alkenyl, alkynyl, cycloalkyl, heteroaryl, aryl, and heterocyclyl is optionally substituted by at least one substituent R 9 ; and

R 9 , at each occurrence, is independently selected from hydrogen, halogen, haloalkyl, alkyl, alkenyl, cycloalkyl, aryl, heteroaryl, heterocyclyl, alkynyl, oxo, —CN, —OR′, —NR′R″, —COR′, —CO 2 R′, —CONR′R″, —C(═NR′)NR″R′″, —NR′COR″, —NR′CONR′R″, —NR′CO 2 R″, —SR′, —SOR′, —SO 2 R′, —NR′SO 2 NR″R′″, and NR′SO 2 R″, wherein R′, R″, and R′″ are independently selected from hydrogen, haloalkyl, alkyl, arylalkyl, alkenyl, alkynyl, cycloalkyl, heterocyclyl, aryl, and heteroaryl.

5. A pharmaceutical composition comprising at least one pharmaceutically acceptable carrier and as an active ingredient a therapeutically effective of the compound of claim 1 , or a pharmaceutically acceptable salt thereof.

6. A compound:

or a pharmaceutically acceptable salt thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 20, 2025
From: BEIGENE, LTD.
To: BEONE MEDICINES I GMBH
Reel/Frame 073116/0803 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 5, 2015
From: ZHOU, CHANGYOU; REN, BO; WANG, HEXIANG
To: BEIGENE LTD.
Reel/Frame 035097/0705 →
Continuity (1)
Related Publication 20150018356A1 · Jan 15, 2015