IP Library Granted Patent US 9,417,190
Granted Patent B2
US 9,417,190 · App. 13/945,661 · Granted Aug 16, 2016

Calibrations and controls for droplet-based assays

Inventors: Benjamin J. Hindson (Livermore, CA); Billy W. Colston, Jr. (San Ramon, CA); Kevin D. Ness (Pleasanton, CA); Donald A. Masquelier (Tracy, CA)
Assignee: Bio-Rad Laboratories, Inc.
G01N21/6486C12Q1/6848G01N21/6428G01N21/6456G01N2021/6441G01N2201/1242
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Quick Facts
Patent No.
US 9,417,190
App. No.
13/945,661
Granted
Aug 16, 2016
Kind
B2
Abstract

System, including methods and apparatus, for performing droplet-based assays that are controlled and/or calibrated using signals detected from droplets.

Claims (10)

1. A method of performing a droplet-based assay, comprising:

forming droplets from a same mixture, wherein only a subset of the droplets contain a target;

irradiating a region of a channel;

detecting a forward scattering signal and a fluorescence signal from a plurality of the droplets as each droplet passes through the region of the channel, wherein the fluorescence signal is detected from a label present in each droplet and varies according to whether the target is present in the droplet;

identifying accepted droplets of the plurality for which the forward scattering signal meets a condition and rejected droplets of the plurality for which the forward scattering signal does not meet the condition, wherein the condition corresponds to a permitted size of a droplet; and

determining a concentration of the target based on the fluorescence signal from the accepted droplets, and without any contribution of the fluorescence signal from the rejected droplets.

2. The method of claim 1 , wherein the forward scattering signal has an intensity that is at least substantially independent of whether or not the target is present in the droplet.

3. The method of claim 1 , wherein the forward scattering signal detected from each droplet forms a peak, and wherein the condition corresponds to a permitted width of the peak.

4. The method of claim 1 , wherein the step of determining includes a step of determining a fraction of the accepted droplets that are positive or a fraction that are negative for the target.

5. The method of claim 1 , wherein the forward scattering signal is produced by refraction of incident radiation.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 11, 2016
From: HINDSON, BENJAMIN J.; COLSTON, BILLY W., JR.; MASQUELIER, DONALD A.
To: BIO-RAD LABORATORIES, INC.
Reel/Frame 039127/0271 →
Continuity (23)
Continuation In Part 13251016 · Sep 30, 2011
Continuation In Part 13245575 · Sep 26, 2011
Continuation In Part 12976827 · Dec 22, 2010
Continuation 12586626 · Sep 23, 2009
Provisional Application 61194043 · Sep 23, 2008
Provisional Application 61206975 · Feb 5, 2009
Provisional Application 61271538 · Jul 21, 2009
Provisional Application 61275731 · Sep 1, 2009
Provisional Application 61277200 · Sep 21, 2009
Provisional Application 61277203 · Sep 21, 2009
Provisional Application 61277204 · Sep 21, 2009
Provisional Application 61277216 · Sep 21, 2009
Provisional Application 61277249 · Sep 21, 2009
Provisional Application 61277270 · Sep 22, 2009
Provisional Application 61309845 · Mar 2, 2010
Provisional Application 61341218 · Mar 25, 2010
Provisional Application 61317635 · Mar 25, 2010
Provisional Application 61380981 · Sep 8, 2010
Provisional Application 61409106 · Nov 1, 2010
Provisional Application 61409473 · Nov 2, 2010
Provisional Application 61410769 · Nov 5, 2010
Provisional Application 61417241 · Nov 25, 2010
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