IP Library Granted Patent US 9,427,427
Granted Patent B2
US 9,427,427 · App. 14/159,679 · Granted Aug 30, 2016

Pharmaceutical composition with improved bioavailability

Inventors: Steve Lomuscio (Union, NJ); Hua Ma (Wayne, NJ); Michael Allen Matchett (Montville, NJ); Harpreet K. Sandhu (West Orange, NJ); Navnit Hargovindas Shah (Clifton, NJ); Yu-E Zhang (Wayne, NJ)
Assignee: HOFFMANN-LA ROCHE INC.
A61K31/40A61K9/10A61K9/146A61K9/1641A61K9/2054A61K9/2027A61K47/38
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,427,427
App. No.
14/159,679
Granted
Aug 30, 2016
Kind
B2
Abstract

The invention relates to solid dispersions of poorly water soluble compounds, in particular Compound A as disclosed herein, formed by solvent co-precipitation or spray drying, resulting in improved bioavailability, safety and tolerability of said compounds.

Claims (23)

1. A physically stable solid dispersion comprising compound (A):

and a stabilizing polymer, wherein said stabilizing polymer is Poly(methacylic acid)-co-methyl methacrylate or Poly(vinylpyrrolidone-co-vinyl acetate)(6+4).

2. The solid dispersion of claim 1 , wherein the stabilizing polymer is Poly(methacylic acid)-co-methyl methacrylate.

3. The solid dispersion of claim 1 , wherein the stabilizing polymer is Poly(vinylpyrrolidone-co-vinyl acetate)(6+4).

4. The solid dispersion according to claim 1 wherein the ratio of the amount by weight of Compound A within the solid dispersion to the amount by weight of the stabilizing polymer therein is between 5:95 to 70:30.

5. A physically stable solid dispersion, comprising compound (A):

and a stabilizing polymer that is Poly(vinylpyrrolidone-co-vinyl acetate)(6+4), wherein the ratio of the amount by weight of Compound A in the solid dispersion to the amount by weight of the stabilizing polymer therein is between 5:95 to 70:30.

6. The solid dispersion of claim 4 wherein the ratio of the amount by weight of the Compound A within the solid dispersion to the amount by weight of the stabilizing polymer therein is 30:70 to 50:50.

7. The solid dispersion of claim 5 wherein the ratio of the amount by weight of the Compound A within the solid dispersion to the amount by weight of the stabilizing polymer therein is preferably 30:70 to 50:50.

8. The solid dispersion of claim 5 , wherein the solid dispersion is obtained by spray drying of a solution comprising Compound A and Poly(vinylpyrrolidone-co-vinyl acetate)(6+4).

9. The solid dispersion of claim 7 , wherein the solid dispersion is obtained by spray drying of a solution comprising Compound A and Poly(vinylpyrrolidone-co-vinyl acetate)(6+4).

10. A unit dose solid formulation comprising: the solid dispersion according to claim 1 , together with commonly used pharmaceutical ingredients selected from the group consisting of disintegrants, diluents, lubricants, and glidants together with a film coat.

11. A unit dose solid formulation comprising: the solid dispersion according to claim 5 , together with commonly used pharmaceutical ingredients selected from the group consisting of disintegrants, diluents, lubricants, and glidants together with a film coat.

12. A unit dose solid formulation, comprising approximately 80% of the solid dispersion according to claim 1 as an amorphous solid dispersion, together with about 7% croscarmellose sodium, about 6.8% mannitol, about 4% crospovidone, about 1.5% colloidal silicon dioxide and about 0.7% of magnesium stearate which is then encapsulated or compressed and coated as tablet.

13. A unit dose solid formulation, comprising approximately 80% of the solid dispersion according to claim 3 as an amorphous solid dispersion, together with about 7% croscarmellose sodium, about 6.8% mannitol, about 4% crospovidone, about 1.5% colloidal silicon dioxide and about 0.7% of magnesium stearate which is then encapsulated or compressed and coated as tablet.

14. A pharmaceutical preparation containing the solid dispersion according to claim 1 , together with additional pharmaceutically acceptable adjuvants.

15. A pharmaceutical preparation containing the solid dispersion according to claim 4 , together with additional pharmaceutically acceptable adjuvants.

16. A pharmaceutical preparation containing the solid dispersion according to claim 5 , together with additional pharmaceutically acceptable adjuvants.

17. A pharmaceutical preparation containing the solid dispersion according to claim 6 , together with additional pharmaceutically acceptable adjuvants.

18. A pharmaceutical preparation containing the solid dispersion according to claim 7 , together with additional pharmaceutically acceptable adjuvants.

19. A pharmaceutical preparation containing the solid dispersion according to claim 8 , together with additional pharmaceutically acceptable adjuvants.

20. A unit dose solid formulation comprising: the solid dispersion according to claim 7 , together with commonly used pharmaceutical ingredients selected from the group consisting of disintegrants, diluents, lubricants, and glidants together with a film.

21. A method of treating AML or prostate cancer, comprising the step of administering a therapeutically effective amount of the physically stable solid dispersion of claim 6 to a subject in need thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 29, 2014
From: LOMUSCIO, STEVE; SANDHU, HARPREET; ZHANG, YU-E; MA, HUA, `; MATCHETT, MICHAEL; SHAH, NAVNIT
To: HOFFMANN-LA ROCHE INC.
Reel/Frame 032985/0297 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 29, 2014
From: HOFFMANN-LA ROCHE INC.
To: F. HOFFMANN-LA ROCHE AG
Reel/Frame 032985/0389 →
Continuity (2)
Provisional Application 61755074 · Jan 22, 2013
Related Publication 20140206742A1 · Jul 24, 2014