IP Library Granted Patent US 9,447,409
Granted Patent B2
US 9,447,409 · App. 12/882,194 · Granted Sep 20, 2016

Lysis buffers for extracting nucleic acids

Inventors: James Stray (San Mateo, CA); Jason Yingjie Liu (Foster City, CA); Maxim Brevnov (Union City, CA); Jaiprakash Shewale (Santa Clara, CA); Allison Holt (Burlingame, CA)
Assignee: LIFE TECHNOLOGIES CORPORATION
C12N15/1006C12N1/06C12N15/1003C12Q1/6806
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Quick Facts
Patent No.
US 9,447,409
App. No.
12/882,194
Granted
Sep 20, 2016
Kind
B2
Abstract

The present teachings relate to the extraction of nucleic acid from solid materials. Provided are useful compositions, methods and kits for obtaining nucleic acids from a solid biological sample or an adhesive material having a biological material adherent or embedded within the adhesive substrate. The extracted nucleic acid can be used in downstream applications such as genotyping, detection, quantification, and identification of the source of the biological material.

Claims (12)

1. A composition comprising 250 to 500 mM ethylene glycol tetraacetic acid and each of the following: a detergent, a reducing agent, and an enzyme, wherein the detergent is selected from one or more of N-lauroyl sarcosine, sodium deoxycholate, cetyltrimethylammonium bromide, dodecyl β-D-maltoside, nonanoyl-N-methylglucamide, polyethylene glycol p-(1,1,3,3-tetramethylbutyl)-phenyl ether, sodium dodecyl sulfate, and combinations thereof, wherein the reducing agent comprises one or more of tris(2-carboxyethyl)phosphine, dithioerythritol, and dithiothreitol, and wherein the enzyme is selected from caspase, chymotrypsin, pepsin, proteinase K, thrombin, Staphylococcus V8 protease, pronase, papain, Bacillus sp. E1A protease, and trypsin and combinations thereof.

2. The composition of claim 1 , wherein the detergent is N-lauroyl sarcosine, the reducing agent is dithiothreitol, and the enzyme is proteinase K.

3. A method of making a product, wherein the product comprises a nucleic acid, comprising:

a) incubating a solid in a solution;

b) extracting a supernatant from the incubated solid in the solution, wherein the supernatant comprises the nucleic acid extracted from the solid, wherein the solution comprises 250 to 500 mM ethylene glycol tetraacetic acid and each of the following: a detergent, a reducing agent, and an enzyme, wherein the detergent is selected from one or more of N-lauroyl sarcosine, sodium deoxycholate, cetyltrimethylammonium bromide, dodecyl β-D-maltoside, nonanoyl-N-methylglucamide, polyethylene glycol p-(1,1,3,3-tetramethylbutyl)-phenyl ether, sodium dodecyl sulfate, and combinations thereof, wherein the reducing agent comprises one or more of tris(2-carboxyethyl)phosphine, dithioerythritol, and dithiothreitol, and wherein the enzyme comprises one or more of caspase, chymotrypsin, pepsin, proteinase K, thrombin, Staphylococcus V8 protease, pronase, papain, Bacillus sp. E1A protease, and trypsin and combinations thereof.

4. A method of identification comprising:

(a) lysing a sample in a lysis solution, forming a lysate comprising a nucleic acid from the sample, wherein the lysis solution comprises 250 to 500 mM ethylene glycol tetraacetic acid and each of the following: a detergent, a reducing agent, and an enzyme, wherein the detergent is selected from one or more of N-lauroyl sarcosine, sodium deoxycholate, cetyltrimethylammonium bromide, dodecyl β-D-maltoside, nonanoyl-N-methylglucamide, polyethylene glycol p-(1,1,3,3-tetramethylbutyl)-phenyl ether, sodium dodecyl sulfate, and combinations thereof, wherein the reducing agent comprises one or more of tris(2-carboxyethyl)phosphine, dithioerythritol, and dithiothreitol, and wherein the enzyme comprises one or more of caspase, chymotrypsin, pepsin, proteinase K, thrombin, Staphylococcus V8 protease, pronase, papain, Bacillus sp. E1A protease, and trypsin and combinations thereof;

(b) extracting the lysate, wherein the nucleic acid is in the lysate;

(c) analyzing the nucleic acid; and

(d) identifying the sample based on the nucleic acid analysis.

5. The method according to claim 4 , wherein the sample is a fingerprint tape lift.

6. The method of claim 5 , further comprising comparing the fingerprint to a collection of fingerprints.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 13, 2012
From: STRAY, JAMES; LIU, JASON YINGJIE; BREVNOV, MAXIM; SHEWALE, JAIPRAKASH; HOLT, ALLISON
To: LIFE TECHNOLOGIES CORPORATION
Reel/Frame 029290/0150 →
Continuity (4)
Provisional Application 61243136 · Sep 16, 2009
Provisional Application 61360386 · Jun 30, 2010
Provisional Application 61379346 · Sep 1, 2010
Related Publication 20110159485A1 · Jun 30, 2011