IP Library Granted Patent US 9,586,348
Granted Patent B2
US 9,586,348 · App. 15/093,848 · Granted Mar 7, 2017

Apparatus and system for expanding expandable polymeric microspheres

Inventors: Frank Shaode Ong (Solon, OH); Stefan Muessig (Sagamore Hills, OH); Darren Gambatesa (Chagrin Falls, OH); James C. Smith (Cuyahoga Falls, OH); Rick Paponetti (Bedford, OH); Mark A. Bury (Middleburg Heights, OH); Fredrik Svensson (Sundsvall, SE); Jan Nordin (Kvissleby, SE); Jermaine Simmons (Duluth, GA)
Assignees: Construction Research & Technology GmbH; AkzoNobel Chemicals International B.V.
B29C44/3461B29C44/3403B29C44/60C04B16/08C04B20/06C08J9/16B29K2101/12B29K2105/0076B29K2105/048B29L2031/756
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Quick Facts
Patent No.
US 9,586,348
App. No.
15/093,848
Granted
Mar 7, 2017
Kind
B2
Abstract

An apparatus including: (a) a steam generator having a power output of less than or equal to about 6 boiler horsepower; (b) a steam conduit in fluid communication with the steam generator; (c) a fluid material conduit in fluid communication with a source of a fluid material, wherein the fluid material includes unexpanded, expandable polymeric microspheres; (d) a treatment zone in fluid communication with the steam generator via the steam conduit, and with the fluid material conduit, such that the fluid material is contacted by steam within the treatment zone; and (e) a back pressure generator in fluid communication with the treatment zone, capable of increasing pressure in the treatment zone, which results in expansion of the expandable polymeric microspheres when the fluid material exits the treatment zone.

Claims (32)

1. An apparatus comprising:

a. a steam generator;

b. a steam conduit in fluid communication with the steam generator;

c. a fluid material conduit in fluid communication with a source of a fluid material, wherein the fluid material comprises unexpanded, expandable polymeric microspheres;

d. a treatment zone in fluid communication with the steam generator via the steam conduit, and with the fluid material conduit, such that the fluid material is contacted by steam within the treatment zone; and

e. a back pressure generator in fluid communication with the treatment zone, capable of increasing pressure in the treatment zone, which results in expansion of the expandable polymeric microspheres when the fluid material exits the treatment zone, wherein the back pressure generator comprises at least one of:

(ii) a conduit which has an interior size which is smaller than the interior size of either or both of the fluid material conduit or the steam conduit, such that the temperature and/or pressure inside the treatment zone are maintained or increased; or

(iii) a conduit which has an irregular interior wall pattern, such that the temperature and/or pressure inside the treatment zone are maintained or increased;

wherein the apparatus has a footprint which allows the apparatus to be placed inside an existing manufacturing facility without substantially adversely affecting production of products of manufacture produced at the existing manufacturing facility, and without requiring adding space to the existing manufacturing facility.

2. The apparatus of claim 1 , wherein the apparatus consumes less than or equal to about 70 kw during steady-state operation.

3. The apparatus of claim 1 , wherein the apparatus consumes less than or equal to about 45 kw during steady-state operation.

4. The apparatus of claim 1 , wherein the footprint of the apparatus is less than or equal to about 60 ft 2 .

5. The apparatus of claim 1 , further comprising a manual and/or automatic site gauge engaged with the fluid material conduit.

6. The apparatus of claim 1 , wherein the inside diameter of the fluid material conduit is from about 0.2 to about 1.5 inches.

7. The apparatus of claim 1 , wherein the treatment zone comprises a treatment conduit.

8. The apparatus of claim 7 , wherein the steam conduit and the fluid material conduit are joined via a conduit junction proximate to an inlet end of the treatment conduit.

9. The apparatus of claim 7 , wherein the steam conduit and the fluid material conduit are joined via a conduit junction engaged with an inlet end of the treatment conduit.

10. The apparatus of claim 7 , wherein the back pressure generator is engaged with an outlet end of the treatment conduit.

11. The apparatus of claim 1 , wherein the temperature inside the treatment zone is from about 80° C. to about 160° C.

12. The apparatus of claim 1 , wherein the temperature inside the treatment zone is from about 105° C. to about 145° C.

13. The apparatus of claim 1 , wherein the pressure inside the treatment zone is from about 46.1 kPa to about 618.1 kPa.

14. The apparatus of claim 1 , wherein the pressure inside the treatment zone is from about 120 kPa to about 420 kPa.

15. The apparatus of claim 1 , further comprising:

f. a control device to manually and/or automatically control the function of the apparatus; and

g. a manual and/or automatic site gauge engaged with the fluid material conduit;

wherein:

i. the treatment zone comprises a treatment conduit;

ii. the steam conduit and the fluid material conduit converge via a conduit junction engaged with an inlet end of the treatment conduit; and

iii. the back pressure generator is engaged with an outlet end of the treatment conduit.

16. A system for providing expanded polymeric microspheres comprising the apparatus of claim 1 and at least one batch tank to receive the expanded expandable polymeric microspheres, optionally wherein the at least one batch tank comprises at least one mixing device.

17. The system of claim 16 , comprising a plurality of batch tanks to receive the expanded polymeric microspheres.

18. The apparatus of claim 1 , wherein the back pressure generator comprises a rifled conduit.

Assignments (4)
CHANGE OF NAME Recorded Feb 22, 2022
From: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: NOURYON CHEMICALS INTERNATIONAL B.V.
Reel/Frame 059217/0394 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE'S NAME PREVIOUSLY RECORDED AT REEL: 038355 FRAME: 0020. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jul 15, 2016
From: SVENSSON, FREDRIK; NORDIN, JAN; SIMMONS, JERMAINE
To: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
Reel/Frame 039383/0514 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 22, 2016
From: SVENSSON, FREDRIK; NORDIN, JAN; SIMMONS, JERMAINE
To: AKZONOBEL CHEMICALS INTERNATIONAL B.V.
Reel/Frame 038355/0020 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 22, 2016
From: ONG, FRANK SHAODE; MUESSIG, STEFAN; GAMBATESA, DARREN; SMITH, JAMES C; PAPONETTI, RICK; BURY, MARK A
To: CONSTRUCTION RESEARCH & TECHNOLOGY GMBH
Reel/Frame 038355/0220 →
Continuity (8)
Continuation 14515201 · Oct 15, 2014
Continuation PCTUS2013037455 · Apr 19, 2013
Continuation In Part 13866702 · Apr 19, 2013
Provisional Application 61790312 · Mar 15, 2013
Provisional Application 61695134 · Aug 30, 2012
Provisional Application 61635562 · Apr 19, 2012
Provisional Application 61635562 · Apr 19, 2012
Related Publication 20160221232A1 · Aug 4, 2016