IP Library Granted Patent US 9,598,544
Granted Patent B2
US 9,598,544 · App. 14/184,540 · Granted Mar 21, 2017

Particles coated with zwitterionic polymers comprising sulfobetaine or carboxybetaine

Inventors: Shaoyi Jiang (Redmond, WA); Shengfu Chen (Hangzhou, CN); Yung Chang (Luzhu Township, TW); Zheng Zhang (Cambridge, MA)
Assignee: University of Washington through its Center for Commercialization
C08J3/075A61K49/18C07C317/08C07C317/28C07C317/44C07C317/50C08F120/36C08F292/00C09D5/1637C09D7/1225C09D7/1266C09D7/1275B82Y30/00C08F2220/365C08F2438/01C08K3/16C08K3/34C08K9/08
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Quick Facts
Patent No.
US 9,598,544
App. No.
14/184,540
Granted
Mar 21, 2017
Kind
B2
Abstract

Nanoparticles zwitterionic polymers grafted thereto or grafted therefrom, and methods for making and using the nanoparticles. Zwitterionic nanogels, and methods for making and using the nanogels.

Claims (19)

1. A surface having a layer of sulfobetaine polymers coupled thereto, wherein the density of the sulfobetaine polymers in the layer provides a surface having a fibrinogen adsorption of less than about 30 ng/cm 2 in a fibrinogen binding assay when the surface is incubated at 37° C. for 90 minutes with a 1.0 mg/mL fibrinogen solution (0.15 M phosphate buffered saline at pH 7.4).

2. The surface of claim 1 , wherein the sulfobetaine polymers are prepared from one or more monomers selected from the group consisting of a sulfobetaine acrylate, a sulfobetaine acrylamide, a sulfobetaine methacrylate, and mixtures thereof.

3. The surface of claim 1 , wherein the layer of sulfobetaine polymers comprises an interpenetrating sulfobetaine polymer network.

4. The surface of claim 3 , wherein the interpenetrating sulfobetaine polymer network further comprises one or more polymers selected from the group consisting of a polyurethane, a silicone, a polyester, a polyethylene, and a polyamide.

5. The surface of claim 1 , wherein the layer of sulfobetaine polymers comprises a sulfobetaine copolymer.

6. The surface of claim 1 , wherein the layer comprises sulfobetaine polymers covalently attached to a substrate surface.

7. The surface of claim 1 on all or part of a particle.

8. The surface of claim 1 , wherein the fibrinogen adsorption is less than 10 ng/cm 2 .

9. The surface of claim 1 , wherein the fibrinogen adsorption is less than 5 ng/cm 2 .

10. The surface of claim 1 , wherein the fibrinogen adsorption is less than 0.3 ng/cm 2 .

11. The surface of claim 1 , wherein the sulfobetaine polymers are prepared from one or more monomers selected from the group consisting of a sulfobetaine vinyl compound, a sulfobetaine epoxide, and mixtures thereof.

12. A substrate comprising a surface having a layer of sulfobetaine polymers grafted from the surface, wherein the density of the sulfobetaine polymers in the layer provides a surface having a fibrinogen adsorption of less than about 30 ng/cm 2 in a fibrinogen binding assay when the surface is incubated at 37° C. for 90 minutes with a 1.0 mg/mL fibrinogen solution (0.15 M phosphate buffered saline at pH 7.4).

13. The substrate of claim 12 , wherein the sulfobetaine polymers are prepared from one or more monomers selected from the group consisting of a sulfobetaine acrylate, a sulfobetaine acrylamide, a sulfobetaine methacrylate, and mixtures thereof.

14. The substrate of claim 12 , wherein the layer of sulfobetaine polymers comprises a sulfobetaine copolymer.

15. The substrate of claim 12 , wherein the fibrinogen adsorption is less than 10 ng/cm 2 .

16. The substrate of claim 12 , wherein the fibrinogen adsorption is less than 5 ng/cm 2 .

17. The substrate of claim 12 , wherein the fibrinogen adsorption is less than 0.3 ng/cm 2 .

18. The substrate of claim 12 on or forming all or part of a particle.

19. The substrate of claim 12 , wherein the sulfobetaine polymers are prepared from one or more monomers selected from the group consisting of a sulfobetaine vinyl compound, a sulfobetaine epoxide, and mixtures thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2014
From: JIANG, SHAOYI; CHEN, SHENGFU; CHANG, YUNG; ZHANG, ZHENG
To: UNIVERSITY OF WASHINGTON THROUGH ITS CENTER FOR COMMERCIALIZATION
Reel/Frame 033139/0425 →
Continuity (6)
Continuation 12941938 · Nov 8, 2010
Continuation In Part 12020998 · Jan 28, 2008
Continuation PCTUS2006028988 · Jul 25, 2006
Provisional Application 61259081 · Nov 6, 2009
Provisional Application 60711613 · Aug 25, 2005
Related Publication 20140235803A1 · Aug 21, 2014