Modification of diamond feeds for improving polycrystalline diamond cutter
A superabrasive compact and a method of making the superabrasive compact are disclosed. A superabrasive compact may comprise a superabrasive volume and a substrate. The substrate may be attached to the superabrasive volume via an interface. The superabrasive volume may be formed by a plurality of polycrystalline superabrasive particles. The superabrasive particles may have nano or sub-micron scale surface texture.
1. A method of making a polycrystalline superabrasive compact, comprising:
treating a plurality of milled diamond particles in a pre-determined temperature at a pre-set atmosphere in such that diamond particles form nano-scale or sub-micron surface texture;
providing a substrate positioned proximate to the plurality of treated diamond particles; and
subjecting the substrate and the plurality of treated diamond particles to conditions of elevated temperature and pressure suitable for producing the polycrystalline superabrasive compact in which a solvent catalyst is melted and swept through the plurality of treated diamond particles to promote diamond-to-diamond bonding between the plurality of treated diamond particles.
2. The method of the claim 1 , wherein the substrate is cemented tungsten carbide.
3. The method of the claim 1 , wherein the pre-set atmosphere comprises hydrogen.
4. The method of the claim 1 , wherein the pre-determined temperature is from about 550° C. to about 700° C.
5. The method of the claim 1 , wherein the pre-set atmosphere is flowing air or flowing oxygen.
6. The method of the claim 1 , wherein the pre-determined temperature is from about 750° C. to about 900° C.
7. The method of the claim 6 , wherein the pre-set atmosphere is non-flowing or static air.
8. The method of the claim 5 , wherein the elevated temperature and pressure are from about 1400° C. to about 2500° C. and about 10 to about 80 Kbar, respectively.
9. The method of claim 5 , wherein the plurality of diamond particles are treated at the pre-determined temperature and the pre-set atmosphere such that the diamond particles undergo a weight loss from about 2% to 20% weight.
10. The method of claim 7 , wherein the plurality of diamond particles are treated at the pre-determined temperature and the pre-set atmosphere such that the diamond particles undergo a weight loss from about 10% to 30% weight.
11. The method of claim 1 , wherein the plurality of diamond particles are treated at the pre-determined temperature and the pre-set atmosphere such that crystal lattice defects of the diamond particles are removed.
12. The method of claim 11 , wherein the crystal lattice defects are selected from the group consisting of as-grown inclusions, impurities, and dislocations.
13. The method of claim 1 , wherein the plurality of diamond particles are treated at the pre-determined temperature and the pre-set atmosphere such that sharp corners of the milled diamond particles are at least partially rounded.
14. The method of claim 1 , wherein the treatment of the plurality of milled diamond particles reduces the friction of the diamond particles.
15. The method of claim 1 , wherein the treatment of the plurality of milled diamond particles modifies the surface energy of the milled diamond particles and increases inter-diamond sintering activity during conditions of elevated temperature and pressure in which the polycrystalline superabrasive compact is produced.
16. The method of claim 1 , wherein the nano-scale or sub-micron surface texture is dissolved from the diamond particles by the molten solvent catalyst during conditions of elevated temperature and pressure.