IP Library Granted Patent US 9,757,495
Granted Patent B2
US 9,757,495 · App. 14/765,064 · Granted Sep 12, 2017

Collagen scaffolds

Inventor: Martha M. Murray (Sherborn, MA)
Assignee: Children's Medical Center Corporation
A61L27/24A61L27/3633A61L27/3691A61L27/56C07K14/78C12P21/00A61K38/00A61L2430/06A61L2430/10
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Quick Facts
Patent No.
US 9,757,495
App. No.
14/765,064
Granted
Sep 12, 2017
Kind
B2
Abstract

Methods for preparing and using collagen extracts and collagen scaffolds are provided. Additionally methods and related kits for the repair of articular tissue using the collagen material are provided.

Claims (16)

1. A method for preparing a neutralized collagen slurry comprising,

lyophilizing a source tissue;

cutting the source tissue into small pieces while keeping the tissue frozen,

performing an enzyme digestion of the small pieces of source tissue to produce a collagen extract,

lyophilizing the collagen extract to form a lyophilized collagen extract,

reconstituting the lyophilized collagen extract to form a collagen slurry having a collagen concentration of greater than 10 mg/ml, and

neutralizing the collagen slurry to produce a neutralized collagen slurry.

2. The method of claim 1 , wherein the collagen extract is treated with hyperosmotic solutions to remove cellular debris.

3. The method of claim 1 , wherein the collagen extract is treated with detergents to remove cellular debris.

4. The method of claim 2 , further comprising freeze drying a collagen extract prior to the neutralization step.

5. The method of claim 1 , further comprising adding calcium to the collagen extract.

6. The method of claim 1 , wherein the collagen slurry is added to a mold prior to neutralization.

7. The method of claim 6 , wherein the mold is cylindrical.

8. The method of claim 1 , further comprising subjecting the neutralized collagen slurry to an elevated temperature such that the neutralized collagen slurry forms a collagen scaffold comprised of self-assembled collagen fibers.

9. The method of claim 1 , wherein the source tissue is obtained from a knee.

10. The method of claim 1 , wherein the source tissue is obtained from a bovine knee.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2022
From: MURRAY, MARTHA M.
To: THE CHILDREN'S MEDICAL CENTER CORPORATION
Reel/Frame 062177/0351 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 3, 2015
From: MURRAY, MARTHA M.
To: CHILDREN'S MEDICAL CENTER CORPORATION
Reel/Frame 036944/0551 →
Continuity (2)
Provisional Application 61759868 · Feb 1, 2013
Related Publication 20150367030A1 · Dec 24, 2015