IP Library Granted Patent US 9,845,284
Granted Patent B1
US 9,845,284 · App. 15/368,618 · Granted Dec 19, 2017

Method of obtaining complex acidic salts of divalent metals and dicarboxylic acids

Inventors: Mikhail Lvovich Uchitel (Mytishi, RU); Roman Anatolievich Trunin (Moscow, RU); Evgenij Iljich Maevskij (Pushino, RU)
C07C227/18C07C51/418
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Quick Facts
Patent No.
US 9,845,284
App. No.
15/368,618
Granted
Dec 19, 2017
Kind
B1
Abstract

A method of obtaining a complex acidic salt of a divalent metal and a dicarboxylic acid includes heating water in a reactor; adding a dicarboxylic acid to the heated water; stirring the water to dissolve the dicarboxylic acid in the heated water to produce a solution or a suspension of the dicarboxylic acid in the heated water; adding MeO to the solution or the suspension, where Me is a divalent metal; continuing the stirring of the solution or suspension until formation of the complex acidic salt Me(AcH) 2 .nH 2 O begins, where Ac is an anion of the dicarboxylic acid, and n=0-8; cooling the complex acidic salt to below a temperature of crystallization; sedimenting the complex acidic salt; filtering the complex acidic salt to remove water from the complex acidic salt; and drying the complex acidic salt.

Claims (14)

1. A method of obtaining a complex acidic salt of a divalent metal and a dicarboxylic acid, the method comprising:

heating water in a reactor;

adding a dicarboxylic acid to the heated water to produce a suspension of the dicarboxylic acid in the water;

stirring the water to dissolve the dicarboxylic acid in the heated water so as to convert the suspension into a solution of the dicarboxylic acid in the heated water;

during the stirring, and while the suspension is being converted to the solution, adding MeO to the reactor, where Me is a divalent metal, and

wherein a molar ratio of the dicarboxylic acid and the MeO in the heated water is 2.005:1-2.1:1;

continuing the stirring until formation of the complex acidic salt Me(AcH) 2 .nH 2 O begins,

where Ac is an anion of the dicarboxylic acid, and 0<=n<=8;

cooling the complex acidic salt to below a temperature of crystallization of the complex acidic salt;

sedimenting the complex acidic salt;

filtering the complex acidic salt to remove water from the complex acidic salt; and

drying the complex acidic salt.

2. The method of claim 1 , wherein the divalent metal is any of potassium, magnesium and zinc.

3. The method of claim 1 , wherein the dicarboxylic acid is any of L-aspartic acid, L,D-aspartic acid, fumaric acid and amber acid.

Assignments (6)
LICENSE Recorded Jan 28, 2021
From: AMBER IP, LLC
To: BIOGIX, INC.
Reel/Frame 055057/0626 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 22, 2020
From: TRUNIN, ROMAN ANATOLIEVICH
To: AMBER IP, LLC
Reel/Frame 053844/0298 →
RELEASE OF SECURITY INTEREST Recorded Aug 5, 2020
From: EAST WEST BANK
To: TRUNIN, ROMAN ANATOLYEVICH
Reel/Frame 053409/0260 →
LICENSE Recorded Jan 10, 2020
From: TRUNIN, ROMAN
To: BIOGIX, INC.
Reel/Frame 051473/0862 →
SECURITY INTEREST Recorded Aug 21, 2019
From: TRUNIN, ROMAN ANATOLYEVICH
To: EAST WEST BANK
Reel/Frame 050119/0731 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 28, 2019
From: UCHITEL, MIKHAIL LVOVICH; MAEVSKIJ, EVGENIJ ILJICH
To: TRUNIN, ROMAN ANATOLIEVICH
Reel/Frame 048473/0187 →
Priority Claims (1)
RU 2016137257 · Sep 16, 2016 · national