Methods for determining gas extraction efficiency from a drilling fluid
It can sometimes be difficult to determine accurately the in-process degassing efficiency of a drilling fluid, thereby leading to inaccurate feedback from an ongoing drilling operation. Methods for determining degassing efficiency of a drilling fluid can comprise: combining a measured amount of an analysis gas with a drilling fluid sample; transferring the drilling fluid sample and the analysis gas to a degassing unit; withdrawing at least a portion of the analysis gas from the drilling fluid sample in the degassing unit; conveying the withdrawn analysis gas from the degassing unit to a detector with an inert carrier gas; determining an amount of the withdrawn analysis gas with the detector; and calculating an extraction efficiency of the analysis gas from the drilling fluid sample based upon the amount of the withdrawn analysis gas. The extraction efficiency may provide an estimate of the degassing extent for other gases.
1. A method comprising:
combining a measured amount of an analysis gas with a drilling fluid sample;
transferring the drilling fluid sample and the analysis gas contained therein to a degassing unit;
withdrawing at least a portion of the analysis gas from the drilling fluid sample in the degassing unit;
conveying the withdrawn analysis gas from the degassing unit to a detector, the withdrawn analysis gas being conveyed with an inert carrier gas;
determining an amount of the withdrawn analysis gas with the detector; and
calculating an extraction efficiency of the analysis gas from the drilling fluid sample based upon the amount of the withdrawn analysis gas.
2. The method of claim 1 , further comprising:
determining an amount of the inert carrier gas used to convey the withdrawn analysis gas to the detector; and
determining the amount of the withdrawn analysis gas based upon the amount of the inert carrier gas and a concentration of the analysis gas measured at the detector.
3. The method of claim 1 , further comprising:
drilling a wellbore with a drilling fluid;
obtaining the drilling fluid sample from the wellbore;
analyzing a quantity of drilling fluid exiting the wellbore for a wellbore gas; and
correlating the extraction efficiency of the analysis gas to a concentration of the wellbore gas in the drilling fluid exiting the wellbore.
4. The method of claim 1 , further comprising:
measuring the pressure and volume of the analysis gas introduced to the drilling fluid sample to determine the measured amount of the analysis gas.
5. The method of claim 1 , further comprising:
obtaining the drilling fluid sample from a wellbore before combining the analysis gas therewith.
6. The method of claim 5 , wherein the analysis gas is not natively present in the wellbore.
7. The method of claim 6 , wherein the analysis gas comprises acetylene.
8. The method of claim 1 , wherein the detector comprises a flame ionization detector.
9. The method of claim 1 , wherein the analysis gas is withdrawn from the drilling fluid sample at a sub-atmospheric pressure.
10. A method comprising:
obtaining a drilling fluid sample from a wellbore;
combining a measured amount of an analysis gas with the drilling fluid sample;
transferring the drilling fluid sample and the analysis gas contained therein to a degassing unit;
withdrawing at least a portion of the analysis gas from the drilling fluid sample in the degassing unit, the analysis gas being withdrawn from the drilling fluid sample at a sub-atmospheric pressure;
conveying the withdrawn analysis gas from the degassing unit to a detector, the withdrawn analysis gas being conveyed with an inert carrier gas;
determining a concentration of the analysis gas with the detector;
determining an amount of the inert carrier gas used to convey the withdrawn analysis gas to the detector;
determining an amount of the withdrawn analysis gas based upon the amount of the inert carrier gas and the concentration of the analysis gas measured at the detector;
calculating an extraction efficiency of the analysis gas from the drilling fluid sample based upon the amount of the withdrawn analysis gas; and
correlating the extraction efficiency of the analysis gas to a concentration of a wellbore gas in the drilling fluid.
11. The method of claim 10 , further comprising:
measuring the pressure and volume of the analysis gas introduced to the drilling fluid sample to determine the measured amount of the analysis gas.
12. The method of claim 10 , wherein the analysis gas is not natively present in the wellbore.
13. The method of claim 12 , wherein the analysis gas comprises acetylene.
14. The method of claim 10 , wherein the detector comprises a flame ionization detector.
15. The method of claim 10 , wherein the analysis gas is withdrawn from the drilling fluid sample at a sub-atmospheric pressure.