IP Library Granted Patent US 10,017,838
Granted Patent B2
US 10,017,838 · App. 14/363,820 · Granted Jul 10, 2018

Method for extraction of lithium from lithium bearing solution

Inventors: Uong Chon (Pohang-si, KR); Ki Young Kim (Yongin-si, KR); Gi-Chun Han (Cheongju-si, KR); Chang Ho Song (Incheon, KR); Young Seok Jang (Phoang-si, KR); Kee-Uek Jeung (Pohang-si, KR); So Ra Jung (Pohang-si, KR)
Assignee: RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE & TECHNOLOGY
C22B26/12C22B3/44Y02P10/234
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Quick Facts
Patent No.
US 10,017,838
App. No.
14/363,820
Granted
Jul 10, 2018
Kind
B2
Abstract

A method of extracting lithium from a lithium bearing solution and specifically, economically extracting lithium from a lithium bearing solution comprising the steps of: adding a nucleus particle to a lithium bearing solution; and precipitating the dissolved lithium in the lithium bearing solution as lithium phosphate by adding a phosphorous supplying material to the lithium bearing solution including the nucleus particle is provided.

Claims (15)

1. A method of extracting lithium from a lithium bearing solution comprising the steps of:

adding a nucleus particle to a lithium bearing solution; and

precipitating dissolved lithium in the lithium bearing solution as lithium phosphate by adding a phosphorous supplying material to the lithium bearing solution including the nucleus particle,

wherein the nucleus particle has a particle diameter ranging from 6 to 25 μm and a specific surface area ranging from 50 to 100 m 2 /g.

2. The method of claim 1 , wherein the nucleus particle is a lithium compound.

3. The method of claim 1 , wherein the nucleus particle is an insoluble lithium compound.

4. The method of claim 1 , wherein the nucleus particle is at least one selected from an insoluble organic compound, and an insoluble inorganic compound.

5. The method of claim 1 , wherein the nucleus particle is included in an amount of less than or equal to 0.05 g/L based on a total volume of the lithium bearing solution.

6. The method of claim 1 , wherein the nucleus particle is at least one selected from Li 3 PO 4 , Li 2 CO 3 , and LiF.

7. The method of claim 1 , wherein the nucleus particle is at least one selected from Ca 3 (PO 4 ) 2 , hydroxyapatite, zirconia, TiO 2 , SeO 2 , Mg 3 (PO 4 ) 2 , MgO, MgAl 2 O 4 , Al 2 O 3 , and a plastic particle.

8. The method of claim 1 , wherein the phosphorous supplying material is at least one selected from phosphorous, phosphoric acid, a phosphate, and a mixture thereof.

9. The method of claim 1 , wherein a concentration of the lithium phosphate is at least 0.39 g/L.

10. The method of claim 1 , wherein the lithium bearing solution is brine.

11. The method of claim 1 , wherein a lithium concentration in the lithium bearing solution is greater than or equal to 0.1 g/L.

12. The method of claim 1 , further comprising a step of extracting lithium phosphate by filtering the precipitated lithium phosphate from the lithium bearing solution.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 20, 2022
From: RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE & TECHNOLOGY
To: POSCO
Reel/Frame 060249/0242 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 9, 2014
From: CHON, UONG; KIM, KI YOUNG; HAN, GI-CHUN; SONG, CHANG HO; JANG, YOUNG SEOK; JEUNG, KEE-UEK; JUNG, SO RA
To: RESEARCH INSTITUTE OF INDUSTRIAL SCIENCE & TECHNOLOGY
Reel/Frame 033105/0165 →
Priority Claims (3)
KR 10-2011-0132840 · Dec 12, 2011 · national
KR 10-2011-0144771 · Dec 28, 2011 · national
KR 10-2011-0144772 · Dec 28, 2011 · national
Continuity (1)
Related Publication 20140348734A1 · Nov 27, 2014
Cited By (3)
US 12,257,529 US 12,370,468 US 12,374,679