IP Library Granted Patent US 10,071,910
Granted Patent B2
US 10,071,910 · App. 15/033,002 · Granted Sep 11, 2018

Methods and systems for producing carbon aerogel

Inventors: Chongjun Zhao (Shanghai, CN); Jianbo Dong (Shanghai, CN); Youfu Huang (Shanghai, CN); Jingwei Ma (Shanghai, CN); Xiuzhen Qian (Shanghai, CN)
Assignee: EAST CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY
C01B31/02B01J13/0052C01B31/00C01B31/0206C01P2004/64C01P2006/12C01P2006/16
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Quick Facts
Patent No.
US 10,071,910
App. No.
15/033,002
Granted
Sep 11, 2018
Kind
B2
Abstract

Methods described herein generally relate to producing carbon aerogel. The method may include providing a carbon-containing polymeric material, and contacting the carbon-containing polymeric material with light, heat or both to produce the carbon aerogel. Systems and kits for producing carbon aerogel are also disclosed.

Claims (29)

1. A method of producing carbon aerogel, the method comprising:

providing a carbon-containing polymeric material;

exposing the carbon-containing polymeric material to at least one of light or heat selected to produce a carbon aerogel powder; and

collecting the produced carbon aerogel powder,

wherein the produced carbon aerogel powder comprises carbon nanoparticles, and wherein the carbon aerogel powder has a porous structure with an average pore diameter of about 2.5 nm.

2. The method of claim 1 , wherein the carbon-containing polymeric material comprises a synthetic polymer, a natural polymer, or a combination thereof.

3. The method of claim 1 , wherein the carbon-containing polymeric material comprises an epoxy resin, a phenolic resin, a urea resin, camphor, castor oil, turpentine, a polypropylene, a polystyrene, or a combination thereof.

4. The method of claim 1 , further comprising raising a temperature of the carbon-containing polymeric material to about 350° C. to about 650° C. when the carbon-containing polymeric material is exposed to light.

5. The method of claim 1 , wherein exposing the carbon-containing polymeric material to light comprises irradiating the carbon-containing polymeric material with the light for about 2 seconds to about 1 minute.

6. The method of claim 1 , wherein the light comprises a light beam produced by a laser that has a power of at least about 5 W.

7. The method of claim 6 , wherein the light beam has a wavelength of about 200 nm to about 11 μm.

8. The method of claim 1 , wherein the light comprises a focused beam of sunlight.

9. The method of claim 1 , wherein exposing the carbon-containing polymeric material to heat comprises heating the carbon-containing polymeric material for at least 10 minutes.

10. The method of claim 1 , wherein exposing the carbon-containing polymeric material to heat comprises heating the carbon-containing polymeric material for about 2 seconds to 1 minute.

11. The method of claim 1 , wherein the carbon nanoparticles have an average size of about 30 nm to about 75 nm.

12. The method of claim 1 , wherein the carbon nanoparticles have an average size of about 50 nm to about 55 nm.

13. The method of claim 1 , wherein at least about 60% of the carbon nanoparticles have a size of about 30 nm to about 75 nm.

14. The method of claim 1 , wherein at least about 50% of the carbon nanoparticles are porous carbon nanoparticles.

15. The method of claim 14 , wherein the porous carbon nanoparticles have an average pore diameter of at least about 1.5 nm and not more than about 50 nm.

16. The method of claim 1 , wherein the carbon aerogel powder has a BET surface area of about 600 m 2 /g to about 1100 m 2 /g.

17. The method of claim 1 , wherein the carbon aerogel powder has a bulk density of about 6 mg/cm 3 .

18. A method of producing carbon aerogel, the method comprising:

providing a carbon-containing polymeric material including at least one of an epoxy resin, a phenolic resin, a urea resin, camphor, castor oil, turpentine, a polypropylene, or a polystyrene;

exposing the carbon-containing polymeric material to at least one of light or heat selected to produce the carbon aerogel; and

collecting the produced carbon aerogel,

wherein the carbon aerogel powder has a porous structure with an average pore diameter of about 2.5 nm.

19. The method of claim 18 , wherein exposing the carbon-containing polymeric material to the at least one of light or heat produces carbon aerogel including a carbon aerogel powder that includes carbon nanoparticles.

20. The method of claim 19 , wherein the carbon nanoparticles have an average size of about 30 nm to about 75 nm.

21. The method of claim 19 , wherein the carbon nanoparticles have an average size of about 50 nm to about 55 nm.

Assignments (4)
RELEASE OF SECURITY INTEREST IN PATENTS, RECORDED ON JANUARY 29, 2019 AT REEL 048373 FRAME 0217 Recorded Sep 22, 2025
From: CRESTLINE DIRECT FINANCE, L.P., AS COLLATERAL AGENT
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 072936/0464 →
RELEASE OF SECURITY INTEREST Recorded Jul 31, 2019
From: CRESTLINE DIRECT FINANCE, L.P.
To: EMPIRE TECHNOLOGY DEVELOPMENT LLC
Reel/Frame 049924/0794 →
SECURITY INTEREST Recorded Jan 29, 2019
From: EMPIRE TECHNOLOGY DEVELOPMENT LLC
To: CRESTLINE DIRECT FINANCE, L.P.
Reel/Frame 048373/0217 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 28, 2016
From: ZHAO, CHONGJUN; DONG, JIANBO; HUANG, YOUFU; MA, JINGWEI; QIAN, XIUZHEN
To: EAST CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY
Reel/Frame 038414/0092 →
Continuity (1)
Related Publication 20160244332A1 · Aug 25, 2016