IP Library Granted Patent US 10,150,757
Granted Patent B2
US 10,150,757 · App. 15/350,663 · Granted Dec 11, 2018

Quinazolinone derivatives as PARP inhibitors

Inventors: Jerome Emile Georges Guillemont (Ande, FR); Ludo Edmond Josephine Kennis (Lier, BE); Josephus Carolus Mertens (Oud-Turnhout, BE); Jacobus Alphonsus Josephus van Dun (Kasterlee, BE); Maria Victorina Francisca Somers (Vosselaar, BE); Walter Boudewijn Leopold Wouters (Kapellen, BE)
Assignee: Janssen Pharmaceutica NV
C07D403/12A61K31/517A61K45/06C07D401/12C07D401/14C07D405/14C07D413/14C07D417/12C07D417/14
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Quick Facts
Patent No.
US 10,150,757
App. No.
15/350,663
Granted
Dec 11, 2018
Kind
B2
Abstract

The present invention provides compounds of formula (I), their use as PARP inhibitors as well as pharmaceutical compositions comprising said compounds of formula (I) wherein R 1 , R 2 , R 3 , L, X, Y and Z have defined meanings.

Claims (29)

1. A compound of formula (I),

the N-oxide forms, the pharmaceutically acceptable addition salts and the stereo-chemically isomeric forms thereof, wherein

the dotted lines represent optional bonds;

X is >N—;

is —N—C(O)— or —N═CR 4 —, wherein R 4 is hydroxy;

L is a direct bond or a bivalent radical selected from —C(O)—, —C(O)—NH—, —NH—, —C(O)—C 1-6 alkanediyl-, —C(O)—O—C 1-6 alkanediyl- or —C 1-6 alkanediyl-;

R 1 is hydrogen, halo, C 1-6 alkyloxy or C 1-6 alkyl;

R 2 is hydrogen, hydroxy, C 1-6 alkyloxy or aminocarbonyl;

R 3 is hydrogen, or C 1-6 alkyloxy;

Z is amino, cyano or a radical selected from

wherein each R 5 and R 6 is independently selected from hydrogen, halo, amino, C 1-6 alkyl, or C 1-5 alkyloxy.

2. A pharmaceutical composition comprising pharmaceutically acceptable carriers and as an active ingredient a therapeutically effective amount of a compound as claimed in claim 1 .

3. A process of preparing a pharmaceutical composition as claimed in claim 2 wherein the pharmaceutically acceptable carriers and a compound as claimed in claim 1 are intimately mixed.

4. A combination of a compound with a chemotherapeutic agent wherein said compound is a compound of formula (I)

the N-oxide forms, the pharmaceutically acceptable addition salts and the stereo-chemically isomeric forms thereof, wherein

the dotted lines represent optional bonds;

X is >N—;

is —N—C(O)— or —N═CR 4 —, wherein R 4 is hydroxy;

L is a direct bond or a bivalent radical selected from —C(O)—, —C(O)—NH—, —NH—, —C(O)—C 1-6 alkanediyl-, —C(O)—O—C 1-6 alkanediyl- or —C 1-6 alkanediyl-;

R 1 is hydrogen, halo, C 1-6 alkyloxy or C 1-6 alkyl;

R 2 is hydrogen, hydroxy, C 1-6 alkyloxy or aminocarbonyl;

R 3 is hydrogen, or C 1-6 alkyloxy;

Z is amino, cyano or a radical selected from

wherein each R 5 and R 6 is independently selected from hydrogen, halo, amino, C 1-6 alkyl, or C 1-5 alkyloxy.

5. A process for preparing a compound as claimed in claim 1 , characterized by

reacting an intermediate of formula (II) with an intermediate of formula (III), wherein W is an appropriate leaving group, with the formation of a compound of formula (I-a), wherein L 1 is —C 1-6 alkanediyl-NH— and both dotted lines can be a bond, in a reaction-inert solvent and with the addition of an appropriate base,

6. A compound having the formula

the N-oxide forms, the pharmaceutically acceptable addition salts and the stereo-chemically isomeric forms thereof.

7. A pharmaceutical composition comprising pharmaceutically acceptable carriers and as an active ingredient a therapeutically effective amount of a compound as claimed in claim 6 .

Priority Claims (1)
EP 04076887 · Jun 30, 2004 · regional
Continuity (3)
Division 14077881 · Nov 12, 2013
Division 11569892
Related Publication 20170158673A1 · Jun 8, 2017