IP Library Granted Patent US 10,183,754
Granted Patent B1
US 10,183,754 · App. 15/849,020 · Granted Jan 22, 2019

Three dimensional graphene foam reinforced composite coating and deicing systems therefrom

Inventors: Arvind Agarwal (Miami, FL); Benjamin Boesl (Plantation, FL); Jenniffer Bustillos (Miami, FL); Cheng Zhang (Hollywood, FL)
Assignee: THE FLORIDA INTERNATIONAL UNIVERSITY BOARD OF TRUSTEES
B64D15/20B64D15/14C01B32/182C08J9/35F01D25/02F02C7/047B64D2033/0233
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Quick Facts
Patent No.
US 10,183,754
App. No.
15/849,020
Granted
Jan 22, 2019
Kind
B1
Abstract

An efficient deicing system is a silicone-graphene foam composite connected to a source of electrical energy for current promoted heating of the silicone-graphene foam composite. The deicing system can be constructed by infusion and curing a silicone resin infused into the graphene foam attached to electrical contacts. The deicing system can be attached to surfaces of an aircraft for rapid deicing of the aircraft.

Claims (23)

1. A deicing system comprising a silicone-graphene foam composite connected to a source of electrical energy, wherein the graphene foam is continuous throughout the silicone-graphene composite and wherein the silicone-graphene foam composite is in the form of a free-standing system or a coating for a metal substrate.

2. The deicing system according to claim 1 , wherein the graphene foam comprises less than 2 percent by volume.

3. The deicing system according to claim 1 , wherein the graphene foam comprises at least 0.1 percent by volume.

4. The deicing system according to claim 1 , wherein the graphene foam is an interconnected graphene three-dimensional architecture with pore sizes of 100 to 300 μm in diameter.

5. The deicing system according to claim 1 , wherein the source of electrical energy provides a current of 0.8 A or less.

6. The deicing system according to claim 1 , wherein the source of electrical energy provides a current of 0.4 A or less.

7. The deicing system according to claim 1 , wherein the power density is 0.30 W·cm −2 or less.

8. The deicing system according to claim 1 , wherein the silicone of the silicone-graphene composite is the product of an addition cured polydimethylsiloxane resin.

9. The deicing system according to claim 1 , wherein the metal substrate is an aircraft component material.

10. A method of preparing a deicing system according to claim 1 , comprising:

providing a graphene foam;

attaching electrical contacts to the graphene foam;

providing a silicone resin:

infusing the silicone resin into and on the graphene foam to form a silicone infused graphene foam;

curing the silicone infused graphene foam to form a silicone-graphene foam composite;

applying the silicone-graphene foam composite to a metal substrate; and

connecting the electrical contacts to a source of electrical energy.

11. The method according to claim 10 , wherein curing is an addition curing.

12. The method according to claim 10 , wherein attaching is adhering with a silver paste.

13. The method according to claim 10 , further comprising surface treating the metal substrate.

14. The method according to claim 13 , wherein the surface treating comprises grit blasting.

15. A method of deicing an aircraft, comprising applying an electrical current to an aircraft with a deicing system according to claim 1 attached to a portion of the external surface of the aircraft.

16. The method of claim 15 , where in the deicing system is a coating over the external surface of the aircraft.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 18, 2018
From: AGARWAL, ARVIND; BOESL, BENJAMIN; BUSTILLOS, JENNIFFER; ZHANG, CHENG
To: THE FLORIDA INTERNATIONAL UNIVERSITY BOARD OF TRUSTEES
Reel/Frame 044651/0872 →
Cited By (3)
US 12,414,204 US 12,415,335 US 12,590,560