IP Library Granted Patent US 10,401,274
Granted Patent B2
US 10,401,274 · App. 15/378,305 · Granted Sep 3, 2019

Methods and systems for determining gas permeability of a subsurface formation

Inventors: Hui-Hai Liu (Houston, TX); Bitao Lai (Houston, TX); Jilin Jay Zhang (Houston, TX); Daniel Georgi (Houston, TX); Xinwo Huang (Houston, TX)
Assignee: Saudi Arabian Oil Company
G01N15/0826G01N33/24
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Quick Facts
Patent No.
US 10,401,274
App. No.
15/378,305
Granted
Sep 3, 2019
Kind
B2
Abstract

Methods and systems for determining permeability, as a function of pore pressure, and porosity of a subsurface formation. The method includes positioning a sample in a sample assembly comprising of a gas and a pressure gauge, inside a pressure vessel comprising gas or liquid and a pressure gauge, measuring a first gas pressure, p i , of the sample inside the pressure vessel, applying a second gas pressure, p o , to the pressure vessel, the second gas pressure being greater than the first gas pressure, measuring a third gas pressure, p, at time, t, at location, x, from the inlet of sample inside the pressure vessel, determining a total gas mass per unit volume of the subsurface formation, m, and determining the permeability, k, of the subsurface formation as a function of pore pressure based at least in part on the first gas pressure, the second pressure, the third gas pressure, and the gas density, with a single test run.

Claims (125)

1. A transient flow method for determining gas permeability of a subsurface formation, comprising:

acquiring a sample of the subsurface formation;

positioning the sample in a pressure vessel comprising a fluid and a pressure gauge;

equilibrating the sample at a predetermined first pore gas pressure, p i ;

applying a predetermined constant second pore gas pressure, p o , to an inlet of the sample, the second pore gas pressure being greater than the first pore gas pressure;

measuring a third pore gas pressure, p, as a function of time, t, at location, x, along the axis of the sample in the pressure vessel, wherein the location, x, is at a predetermined distance from the inlet of the sample;

in a computer, determining a gas density or total gas mass per unit volume of the subsurface formation, m; and

in the computer, determining the gas permeability of the subsurface formation as a function of pore pressure, k(p), based at least in part on the first pore gas pressure, the second pore gas pressure, the third pore gas pressure as a function of time, and the gas density as a function of pore pressure, with a single test run.

2. The method of claim 1 , wherein the subsurface formation comprises at least one of shale, limestone, and sandstone.

3. A transient flow method for determining gas permeability of a subsurface formation, comprising:

acquiring a sample of the subsurface formation;

positioning the sample in a pressure vessel comprising a fluid and a pressure gauge;

equilibrating the sample at a predetermined first pore gas pressure, p i ;

applying a predetermined constant second pore gas pressure, p o , to an inlet of the sample, the second pore gas pressure being greater than the first pore gas pressure;

measuring a third pore gas pressure, p, as a function of time, t, at location, x, along the axis of the sample in the pressure vessel, wherein the location, x, is at a predetermined distance from the inlet of the sample;

in a computer, determining a gas density or total gas mass per unit volume of the subsurface formation, m;

in the computer, determining the gas permeability of the subsurface formation as a function of pore pressure, k(p), based at least in part on the first pore gas pressure, the second pore gas pressure, the third pore gas pressure as a function of time, and the gas density as a function of pore pressure, with a single test run; and

determining a transport parameter of the subsurface formation, D(p), using a first formula:

D

(

p

)

=

-

p

i

p

λ

2

dm

dp

dp

dp

d

λ

where λ is an independent variable calculated using the formula λ=xt −1/2 ; and

determining gas permeability k of the subsurface formation from D(p) using

D

(

p

)

=

k

ρ

μ

where μ stands for gas viscosity, and ρ for gas density.

4. The method of claim 3 , further comprising:

determining the total gas mass per unit volume of the subsurface formation, m, using a second formula:

m =ϕρ+(1−ϕ)ρ a

where Φ is porosity of the subsurface formation, ρ is gas density of the gas, and ρ a is adsorbed gas mass per unit volume of the subsurface formation.

5. The method of claim 4 , further comprising:

determining the porosity Φ of the subsurface formation using a third formula:

ϕ

=

B

-

A

p

i

p

0

λ

d

ρ

a

dp

dp

A

p

i

p

0

λ

d

(

ρ

-

ρ

a

)

dp

dp

where A is a cross-sectional area of the sample, and B is a slope of a curve of the cumulative gas flow into the sample at x=0 versus t 1/2 .

6. The method of claim 5 , further comprising:

determining the slope of the curve, B, using a fourth formula:

B

=

A

p

i

p

0

λ

dm

dp

dp

.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2017
From: LIU, HUI-HAI; LAI, BITAO; ZHANG, JILIN JAY; GEORGI, DANIEL T; HUANG, XINWO
To: ARAMCO SERVICES COMPANY
Reel/Frame 041386/0432 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2017
From: ARAMCO SERVICES COMPANY
To: SAUDI ARABIAN OIL COMPANY
Reel/Frame 041386/0491 →
Continuity (2)
Provisional Application 62267091 · Dec 14, 2015
Related Publication 20170167964A1 · Jun 15, 2017
Cited By (2)
US 12,529,638 US 12,560,521