IP Library Granted Patent US 10,465,150
Granted Patent B2
US 10,465,150 · App. 15/585,189 · Granted Nov 5, 2019

Cleaning composition

Inventors: Nigel Patrick Somerville Roberts (Newcastle upon Tyne, GB); Julie Ellis (Newcastle upon Tyne, GB)
Assignee: The Procter & Gamble Company
C11D11/0023C11D3/08C11D3/122C11D3/1246C11D3/2086C11D3/3707C11D3/3769C11D3/3776C11D11/0088C11D17/0034C11D17/06
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Quick Facts
Patent No.
US 10,465,150
App. No.
15/585,189
Granted
Nov 5, 2019
Kind
B2
Abstract

A cleaning composition comprising a particle said particle comprising: (a) from 30 to 70% by weight thereof of a polymer having a softening point in the range from about 20° C. to about 60° C.; (b) from 20 to 60% by weight thereof of a first material having a BET surface area greater than 100 m2/g and a D50 from about 5 to about 20 μm; (c) from 3 wt % to 15% by weight thereof of a second material having a BET surface area from about 0.01 to about 5 m2/g and a D50 from about 30 to about 100 μm.

Claims (24)

1. A cleaning composition comprising a particle said particle comprising:

(a) from about 40 to about 60% by weight thereof of a polymer comprising from about 69 to about 89% of methylpolyethylene glycol (meth)acrylate and from about 9 to about 29% of a salt of 3-methyl-1-vinylimidazolium;

(b) from about 40 to about 50% by weight thereof of a silica having a BET surface area greater than 100 m2/g and a D50 from about 5 to about 20 μm;

(c) from about 4 wt % to about 10% by weight thereof of a sulfate having a BET surface area from about 0.01 to about 5 m2/g and a D50 from about 50 to about 80 μm; and

(d) citric acid,

wherein the residual salt in the silica is less than about 2%, by total weight of the silica.

2. A composition according to claim 1 wherein the composition is an automatic dishwashing composition.

3. A composition according to claim 1 wherein the composition or part thereof is in powder form.

4. A process for making a composition according to claim 1 said process comprising the steps of making the particle by:

a) admixing the silica and the sulfate materials;

b) adding the polymer in the form of an aqueous solution to the mixture resulting from step a);

c) drying the mixture resulting from step b); and

d) adding the particle to the remaining components of the composition.

5. A process for making a composition according to claim 1 said process comprising the steps of making the particle by:

a) admixing the silica and the sulfate materials;

b) adding the polymer in the form of an aqueous solution to the mixture resulting from step a) wherein the aqueous solution comprises from about 20% to about 50% by weight of the solution of the polymer;

c) drying the mixture resulting from step b); and

d) adding the particle to the remaining components of the composition.

6. A process for making a composition according to claim 1 wherein the particle is made by agglomeration.

7. A process for making a composition according to claim 1 said process comprising the steps of making the particle by:

a) admixing the silica and the sulfate materials;

b) adding the polymer in the form of an aqueous solution to the mixture resulting from step a);

c) drying the mixture resulting from step b) in a fluidized bed; and

d) adding the particle to the remaining components of the composition.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 7, 2021
From: THE PROCTOR & GAMBLE COMPANY
To: BASF SE
Reel/Frame 056452/0519 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2017
From: SOMERVILLE ROBERTS, NIGEL PATRICK; ELLIS, JULIE
To: THE PROCTER & GAMBLE COMPANY
Reel/Frame 042220/0812 →
Priority Claims (1)
EP 16168212 · May 3, 2016 · regional
Continuity (1)
Related Publication 20170321170A1 · Nov 9, 2017