IP Library Granted Patent US 10,897,907
Granted Patent B2
US 10,897,907 · App. 16/719,414 · Granted Jan 26, 2021

Colorless material with improved antimicrobial performance

Inventors: Joydeep Lahiri (Corning, NY); Florence Christine Monique Verrier (Corning, NY)
Assignee: CORNING INCORPORATED
A01N59/20C03C3/097C03C4/0035C03C14/004C08K3/015C08K3/40C08K5/17C09D5/14C09D7/61C03C2204/02C03C2204/04C03C2214/04
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Quick Facts
Patent No.
US 10,897,907
App. No.
16/719,414
Granted
Jan 26, 2021
Kind
B2
Abstract

Aspects of this disclosure pertain to a colorless material that includes a carrier, copper-containing particles, and quaternary ammonium. In one or more embodiments, the material exhibits, in the CIE L*a*b* system, an L* value in the range from about 91 to about 100, and a C* value of less than about 7, wherein C* equals √(a* 2 +b* 2 ). In some embodiments, the material exhibits a greater than 3 log reduction in a concentration of Staphylococcus aureus , under the EPA Test Method for Efficacy of Copper Alloy as a Sanitizer testing conditions.

Claims (41)

1. A material comprising:

a carrier;

copper-containing particles; and

quaternary ammonium,

wherein the carrier exhibits, in the CIE L*a*b* system, as measured at normal incidence using a standard CIE illuminant, an L* value in the range from about 88 to about 100, and a C* value of less than about 10, wherein C* equals √(a* 2 +b* 2 ),

wherein the material exhibits a greater than 1 log reduction in a concentration of Staphylococcus aureus , under the EPA Test Method for Efficacy of Copper Alloy as a Sanitizer testing conditions,

wherein the copper-containing particles are present in an amount of from about 20 g/gallon to about 100 g/gallon of the carrier or less, and

further wherein the quaternary ammonium is present in an amount of about 5 wt % to about 0.01 wt %.

2. The material of claim 1 , wherein the copper-containing particles comprise a copper-containing glass or cuprous oxide.

3. The material of claim 1 , wherein the carrier comprises a polymer, a monomer, a binder or a solvent.

4. The material of claim 2 , wherein the copper-containing glass comprises a cuprite phase comprising a plurality of Cu 1+ ions, and comprising at least one of B 2 O 3 , P 2 O 5 and R 2 O.

5. The material of claim 4 , wherein the copper-containing glass further comprises a glass phase comprising more than 40 mol % SiO 2 .

6. The material of claim 5 , wherein the glass phase is present in an amount by weight greater than the cuprite phase.

7. The material of claim 5 , wherein the cuprite phase is dispersed in the glass phase.

8. The material of claim 5 , wherein either one or both the cuprite phase and the glass phase comprise Cu 1+ .

9. A material comprising:

a carrier;

copper-containing particles; and

quaternary ammonium,

wherein, after the material is applied to a surface as a layer and dried for 2 minutes or more, the layer exhibits, in the CIE L*a*b* system, as measured at normal incidence using a standard CIE illuminant, an L* value in the range from about 88 to about 100, and a C* value of less than about 10, wherein C* equals √(a* 2 +b* 2 ),

wherein the material exhibits a greater than 1 log reduction in a concentration of Staphylococcus aureus , under the EPA Test Method for Efficacy of Copper Alloy as a Sanitizer testing conditions,

wherein the copper-containing particles are present in an amount of from about 20 g/gallon to about 100 g/gallon of the carrier or less, and

wherein the quaternary ammonium is present in an amount of about 5 wt % to about 0.01 wt %.

10. The material of claim 9 , wherein the copper-containing particles comprise a copper-containing glass or cuprous oxide.

11. The material of claim 9 , wherein the carrier comprises a polymer, a monomer, a binder or a solvent.

12. The material of claim 10 , wherein the copper-containing glass comprises a cuprite phase comprising a plurality of Cu 1+ ions, and comprising at least one of B 2 O 3 , P 2 O 5 and R 2 O.

13. The material of claim 12 , wherein the copper-containing glass further comprises a glass phase comprising more than 40 mol % SiO 2 .

14. The material of claim 13 , wherein the glass phase is present in an amount by weight greater than the cuprite phase.

15. The material of claim 13 , wherein the cuprite phase is dispersed in the glass phase.

16. The material of claim 13 , wherein either one or both the cuprite phase and the glass phase comprise Cu 1+ .

17. The material of claim 12 , wherein the cuprite phase comprises crystals having an average major dimension of about 5 micrometers (μm) or less, and wherein the cuprite phase is degradable and leaches in the presence of water.

18. A material comprising:

a carrier;

copper-containing particles; and

quaternary ammonium,

wherein the carrier exhibits, in the CIE L*a*b* system, as measured at normal incidence using a standard CIE illuminant, one or more of: (a) an L* value in the range from about 88 to about 100 and (b) a C* value of less than about 10, wherein C* equals √(a* 2 +b* 2 ),

wherein the material exhibits a greater than 1 log reduction in a concentration of Staphylococcus aureus , under the EPA Test Method for Efficacy of Copper Alloy as a Sanitizer testing conditions,

wherein the copper-containing particles are present in an amount of from about 1 g/gallon to about 100 g/gallon of the carrier or less, and

further wherein the quaternary ammonium is present in an amount of about 5 wt % to about 0.01 wt %.

19. The material of claim 18 , wherein the copper-containing particles comprise a copper-containing glass, and further wherein the copper-containing glass comprises a cuprite phase comprising a plurality of Cu 1+ ions, and comprising at least one of B 2 O 3 , P 2 O 5 and R 2 O.

20. The material of claim 19 , wherein the copper-containing glass further comprises a glass phase comprising more than 40 mol % SiO 2 , and further wherein the glass phase is present in an amount by weight greater than the cuprite phase.

Continuity (3)
Division 16072747
Provisional Application 62288735 · Jan 29, 2016
Related Publication 20200120938A1 · Apr 23, 2020