IP Library Granted Patent US 11,148,085
Granted Patent B2
US 11,148,085 · App. 16/207,857 · Granted Oct 19, 2021

Electrostatically-charged nanofiber media and fabrication method thereof

Inventor: Wallace Woon Fong Leung (Hong Kong, CN)
Assignee: THE HONG KONG POLYTECHNIC UNIVERSITY
B01D39/1623B01D46/10B32B5/022B32B5/26D01D5/0076B32B2250/20
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Quick Facts
Patent No.
US 11,148,085
App. No.
16/207,857
Granted
Oct 19, 2021
Kind
B2
Abstract

A charged multilayer nanofiber filter for air filtration and the fabrication method thereof is disclosed. The charged multilayer nanofiber filter has a plurality of charged nanofiber mats. Each of the plurality of charged nanofiber mats is obtained by charging nanofiber mats individually before assembling. The nanofiber mat comprises a nanofiber layer and a substrate layer. The plurality of charged nanofiber mats is assembled such that the nanofiber layers and the substrate layers are stacked together in an alternative manner. The charged multilayer nanofiber filter can be fabricated by electrospinning a polymer solution on the substrate layer to obtain a nanofiber mat, charging the nanofiber mat to obtain a charged nanofiber mat, and assembling a plurality of charged nanofiber mats to form the charged multilayer nanofiber filter.

Claims (27)

1. A method for fabricating a charged multilayer nanofiber filter having a first gsm, the charged multilayer nanofiber filter capable of inducing dipoles on neutrally charged particles to obtain charged particles, and capturing the charged particles for performing air filtration, the method comprising the steps of:

fabricating a plurality of charged nanofiber mats wherein fabricating an individual charged nanofiber mat comprises the steps of:

electrospinning a polymer solution on a substrate layer to obtain a nanofiber mat consisting of a nanofiber layer and the substrate layer; and

charging the nanofiber mat to obtain the individual charged nanofiber mat of a second gsm, causing a surface potential of the individual charged nanofiber mat to be increased to thereby improve a filtration efficiency of the charged multilayer nanofiber filter, wherein the second gsm is less than the first gsm; and

assembling the plurality of charged nanofiber mats to form the charged multilayer nanofiber filter, wherein the plurality of charged nanofiber mats is arranged in parallel to each other; and the charged multilayer nanofiber filter has a higher filtration efficiency and a lower pressure drop than a single layer filter or an uncharged filter having said first gsm.

2. The method of claim 1 , wherein the fabricating of the individual charged nanofiber mat further comprises the step of drying the nanofiber mat in a vacuum oven to remove any residual solvent.

3. The method of claim 1 , wherein the fabricating of the individual charged nanofiber mat further comprises the step of discharging the nanofiber mat by soaking the nanofiber mat in alcohol or water to remove residual charges from electrospinning prior to charging, thereby charging performance of the nanofiber mat is improved.

4. The method of claim 1 , wherein the step of assembling the plurality of charged nanofiber mats comprises assembling the plurality of charged nanofiber mats such that the nanofiber layers and the substrate layers in the plurality of charged nanofiber mats are stacked together in an alternative manner.

5. The method of claim 1 , wherein the charging the nanofiber mat comprises charging the nanofiber mat by corona discharge with a charging voltage of 10 kV to 20 kV and a charging distance of 20 mm to 40 mm for a period of 20 to 100 seconds.

6. The method of claim 1 , wherein the step of charging the nanofiber mat comprises charging the nanofiber mat by corona discharge with a charging voltage of 15 kV and a charging distance of 30 mm for a period of 60 seconds.

7. The method of claim 1 , wherein the step of charging the nanofiber mat comprises charging the nanofiber mat by triboelectric effect.

8. The method of claim 1 , wherein the polymer solution comprises PVDF, DMF, and acetone.

9. The method of claim 1 , wherein the substrate is a grounded or negatively charged collector made of anti-static nonwoven microfibers for removing residual charges after electrospinning.

10. A charged multilayer nanofiber filter having a first gsm, the charged multilayer nanofiber filter having a plurality of charged nanofiber mats assembled, wherein:

the charged multilayer nanofiber filter is capable of inducing dipoles on neutrally charged particles to obtain charged particle, and capturing the charged particles for performing air filtration;

each individual charged nanofiber mat having a second gsm is a nanofiber mat being electrostatically charged individually, causing a surface potential of the individual charged nanofiber mat to be increased to thereby improve a filtration efficiency of the charged multilayer nanofiber filter; and

the nanofiber mat consists of a nanofiber layer and a substrate layer,

wherein:

the second gsm is less than the first gsm; and

the charged multilayer nanofiber filter has a higher filtration efficiency and a lower pressure drop than a single layer filter or an uncharged filter having said first gsm.

11. The charged multilayer nanofiber filter of claim 10 , wherein the nanofiber mat is a discharged nanofiber mat having residual charges from electrospinning removed, wherein the discharged nanofiber mat is obtained by soaking a pristine nanofiber mat in alcohol or water.

12. The charged multilayer nanofiber filter of claim 10 , wherein the plurality of charged nanofiber mats is assembled such that the nanofiber layers in the plurality of charged nanofiber mats and the substrate layers are stacked together in an alternative manner.

13. The charged multilayer nanofiber filter of claim 10 , wherein each charged nanofiber mat is charged by corona discharge with a charging voltage of 10 kV to 20 kV and a charging distance of 20 mm to 40 mm for a period of 20 to 100 seconds.

14. The charged multilayer nanofiber filter of claim 10 , wherein each charged nanofiber mat is charged by corona discharge with a charging voltage of 15 kV and a charging distance of 30 mm for a period of 60 seconds.

15. The charged multilayer nanofiber filter of claim 10 , wherein each charged nanofiber mat is charged by triboelectric effect.

16. The charged multilayer nanofiber filter of claim 10 , wherein the polymer comprises PVDF, DMF, and acetone.

17. The charged multilayer nanofiber filter of claim 10 , wherein the substrate is made of anti-static nonwoven microfibers for removing residual charges after electrospinning.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 4, 2018
From: LEUNG, WALLACE WOON FONG
To: THE HONG KONG POLYTECHNIC UNIVERSITY
Reel/Frame 047669/0660 →
Continuity (2)
Provisional Application 62657966 · Apr 16, 2018
Related Publication 20190314746A1 · Oct 17, 2019