IP Library Granted Patent US 11,219,219
Granted Patent B2
US 11,219,219 · App. 16/637,380 · Granted Jan 11, 2022

Liquid composition and process thereof

Inventors: Carlos Eduardo Fabri (Sao Paulo, BR); Manubhai Panchal Digish (Mumbai, IN); Jaidev Rajnikant Shroff (Dubai, AE); Vikram Rajnikant Shroff (Dubai, AE)
Assignee: UPL LTD.
A01N59/06
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Quick Facts
Patent No.
US 11,219,219
App. No.
16/637,380
Granted
Jan 11, 2022
Kind
B2
Abstract

The present invention provides a liquid composition for defoliation of crop plants comprising a metal chlorate and alkali metal halide. The invention also provides a process for preparing the liquid composition for defoliation of crop plants and a method of defoliating crop plants.

Claims (38)

1. A liquid composition for defoliation of crop plants, the liquid composition consisting of:

about 10 wt % to about 80 wt % magnesium chlorate;

about 2 wt % to about 30 wt % of sodium chloride, each based on a total weight of the liquid composition, and

water.

2. The liquid composition as claimed in claim 1 , wherein the sodium chloride is present in an amount from about 2% to about 10% of the total weight of the liquid composition.

3. The liquid composition as claimed in claim 1 , wherein the sodium chloride is present in an amount less than 20% by the total weight of the liquid composition.

4. The liquid composition as claimed in claim 1 , wherein the sodium chloride is present in an amount less than 10% by the total weight of the liquid composition.

5. The liquid composition as claimed in claim 1 , wherein the sodium chloride is present in an amount less than 7.5% by the total weight of the liquid composition.

6. A process for preparing a liquid composition for defoliation of crop plants, wherein the process comprising:

a) dissolving an alkali metal chlorate and alkali metal halide separately in water at a temperature of less than or equal to about 40° C. to provide a solution; and

b) heating the solution to a temperature not less than about 90° C. and adding magnesium chloride to the heated solution to obtain a reaction mixture;

c) heating the reaction mixture at a temperature not less than about 100° C. for at least about four hours to obtain a first product;

d) removing water from the first product to form a second product;

e) adding acetone to the second product and stirring for at least 60 minutes at a temperature of not less than 50° C. to form a third product, and further cooling the third product;

f) filtering the third product after cooling to obtain a precipitate;

g) removing acetone from the precipitate at a temperature not exceeding 90° C. obtain a fourth product, and adding water to the fourth product thereby forming the liquid composition.

7. The process for preparing a liquid composition as claimed in claim 6 , wherein

the alkali metal chlorate consists of of sodium chlorate and the alkali metal halide consists of sodium chloride.

8. A method of defoliating crop plants, said method comprising applying, to the crop plants that are required to be defoliated, a liquid composition consisting of about 10 wt % to about 80 wt % of magnesium chlorate; about 2 wt % to about 30 wt % of sodium chloride, each based on a total weight of the composition; and water.

9. The liquid composition of claim 1 , wherein the liquid composition consists of:

about 20 wt % to about 70 wt % of the magnesium chlorate;

about 2 wt % to about 10 wt % of the sodium chloride, each based on the total weight of the liquid composition; and

water.

10. The liquid composition of claim 9 , wherein the sodium chloride is present in an amount of about 2 wt % to less than 7.5 wt. % based on the total weight of the liquid composition.

11. The method of claim 7 , wherein the liquid composition consists of:

about 10 wt % to about 80 wt % of the magnesium chlorate;

about 2 wt % to about 30 wt % of the sodium chloride, each based on the total weight of the liquid composition; and

water.

12. The method of claim 7 , wherein the liquid composition consists of:

about 20 wt % to about 70 wt % of the magnesium chlorate;

about 2 wt % to about 10 wt % of the sodium chloride, each based on the total weight of the liquid composition; and

water.

13. The method of claim 12 , wherein the sodium chloride is present in an amount of about 2 wt % to less than 7.5 wt. % based on the total weight of the liquid composition.

14. The method of claim 8 , wherein the liquid compositions consists of:

about 20 wt % to about 70 wt % of the magnesium chlorate;

about 2 wt % to about 10 wt % of the sodium chloride, each based on the total weight of the liquid composition; and

water.

15. The method of claim 14 , wherein the sodium chloride is present in an amount of about 2 wt % to less than 7.5 wt. % based on the total weight of the liquid composition.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 23, 2021
From: FABRI, CARLOS EDUARDO; DIGISH, MANUBHAI PANCHAL; SHROFF, JAIDEV RAJNIKANT; SHROFF, VIKRAM RAJNIKANT
To: UPL LTD
Reel/Frame 058190/0454 →
Priority Claims (1)
IN 201731004976 · Feb 11, 2017 · national
Continuity (1)
Related Publication 20200404924A1 · Dec 31, 2020