IP Library Granted Patent US 11,279,712
Granted Patent B2
US 11,279,712 · App. 16/642,441 · Granted Mar 22, 2022

Macrocyclic compounds that inhibit MCL-1 protein

Inventors: Sean P. Brown (San Francisco, CA); Yunxiao Li (Thousand Oaks, CA); Paul E. Harrington (Thousand Oaks, CA); Brian Alan Lanman (Woodland Hills, CA); Jonathan D. Low (Reseda, CA); Ana Elena Minatti (Los Angeles, CA); Vu Van Ma (Oak Park, CA); Kexue Li (Newbury Park, CA)
Assignee: AMGEN INC.
C07D513/04A61P35/00C07D519/00A61K31/496A61K31/5377A61K31/7068
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Quick Facts
Patent No.
US 11,279,712
App. No.
16/642,441
Granted
Mar 22, 2022
Kind
B2
Abstract

Provided herein are myeloid cell leukemia 1 protein (Mcl-1) inhibitors, methods of their preparation, related pharmaceutical compositions, and methods of using the same. For example, provided herein are compounds of Formula I, or a stenoisomer thereof; and pharmaceutically acceptable salts thereof and pharmaceutical compositions containing the compounds. The compounds and compositions provided herein may be used, for example, in the treatment of diseases or conditions, such as cancer.

Claims (39)

1. A compound of Formula IA:

a stereoisomer thereof, a pharmaceutically acceptable salt thereof, or a pharmaceutically acceptable salt of the stereoisomer thereof,

wherein:

Z is C or N;

b, represented by the symbol , is a single or double chemical bond which may be cis or trans;

R 1 is selected from H, halo, or C 1-6 alkyl;

R 2 is selected from H, halo, or C 1-6 alkyl;

R 3 is selected from H or —C 1-6 alkyl;

each of R 4 , R 5 , R 6 , R 7 , and R 8 is independently selected from H, —C 1-6 alkyl, or —C 1-6 alkyl-O—C 1-6 alkyl;

each of R 4A , R 5A , R 6A , R 7A , and R 8A is independently selected from H, or —C 1-6 alkyl;

R 7A and R 8A are absent when b is a double chemical bond;

R 9 is —C 1-6 alkyl, unsubstituted or substituted with 1, 2, 3 or 4 R 10 substituents independently selected from halo, —OH, —NR a R b ; —(═O), —OC 1-6 alkyl, —SO 2 R a , a 5- to 12-membered spirocycloalkyl or spiroheterocycloalkyl, or a 3- to 12-membered monocyclic or bicyclic heterocycloalkyl group, wherein the heteroaryl, spiroheterocycloalkyl and heterocycloalkyl groups have 1, 2, 3 or 4 heteroatoms independently selected from O, N or S,

wherein the aryl, heteroaryl, cycloalkyl, heterocycloalkyl, spirocycloalkyl and spiroheterocycloalkyl groups of any of the R 10 substituents can be unsubstituted or substituted with 1, 2, 3 or 4 R 2 substituents independently selected from halo, —NR a R b , —C 1-6 alkyl, —(═O), —C 1-6 alkyl-O—C 1-6 alkyl, —SO 2 R a , —C(═O)R a , and —C(═O)OR a ;

wherein R a and R b are each independently H, —C 1-6 alkyl, or —(CH 2 CH 2 O) n CH 3 , and

wherein n is 1.

2. The compound of claim 1 , wherein the compound has the Formula IIa:

a stereoisomer thereof, a pharmaceutically acceptable salt thereof, or a pharmaceutically acceptable salt of the stereoisomer thereof.

3. The compound of claim 1 , wherein R 1 is halo.

4. The compound of claim 1 , wherein R 3 is H.

5. The compound of claim 1 , wherein R 4 is independently selected from H, —C 1-6 alkyl, or —C 1-6 alkyl-O—C 1-6 alkyl.

6. The compound of claim 1 , wherein R 5 is selected from H or —C 1-6 alkyl.

7. The compound of claim 1 , wherein R 6 is selected from H or —C 1-6 haloalkyl.

8. The compound of claim 1 , wherein R 9 is —C 1-6 haloalkyl unsubstituted or substituted with 1, 2, or 3 R 10 substituents.

9. The compound of claim 1 , wherein R 10 is independently selected from halo, —OH, —NR a R b ; —(═O), —OC 1-6 alkyl, —SO 2 R a , a 5- to 12-membered spirocycloalkyl or spiroheterocycloalkyl, or a 3- to 12-membered monocyclic or bicyclic heterocycloalkyl group, wherein the heteroaryl, spiroheterocycloalkyl and heterocycloalkyl groups have 1, 2, 3 or 4 heteroatoms independently selected from O, N or S.

10. The compound of claim 9 , wherein R 10 is a 3- to 12-membered monocyclic or bicyclic heterocycloalkyl group, wherein the heterocycloalkyl group has 1, 2, 3 or 4 heteroatoms independently selected from O, S, or N.

11. The compound of claim 1 , wherein R 9 is independently selected from —CH 3 , —CH 2 OH, CH(OH)CF 3 , —C(═O), —C(═O)OH, —CHCH 2 (OH), —CH(OH)CH 3 , —CH 2 (O)CH 3 , —C(═O)CH 3 , —CH 2 S(O) 2 CH 3 , —C(═O)NH(CH 2 ) 2 OCH 3 ,

12. The compound of claim 1 , wherein the compound has the Formula Ma:

or a stereoisomer thereof, a pharmaceutically acceptable salt thereof, or a pharmaceutically acceptable salt of the stereoisomer thereof.

13. The compound of claim 12 , wherein R 1 is halo.

14. The compound of claim 12 , wherein R 4 is —C 1-6 alkyl.

15. The compound of claim 12 , wherein R 5 is —C 1-6 alkyl.

16. The compound of claim 12 , wherein R 6 is H.

17. The compound of claim 12 , wherein R 9 is —CH 2 OH, —CH(OH)CH 2 CH 3 ,

18. A compound, wherein the compound has a structure selected from:

or a stereoisomer thereof; a pharmaceutically acceptable salt thereof, or a pharmaceutically acceptable salt of the stereoisomer thereof.

19. A compound, wherein the compound has a structure selected from:

or a pharmaceutically acceptable salt thereof.

20. A pharmaceutical composition comprising the compound of claim 19 or the pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier or diluent.

21. A pharmaceutical composition comprising the compound of claim 1 or the pharmaceutically acceptable salt thereof, and a pharmaceutically acceptable carrier or diluent.

Continuity (2)
Provisional Application 62551718 · Aug 29, 2017
Related Publication 20200247821A1 · Aug 6, 2020