IP Library Granted Patent US 11,459,327
Granted Patent B1
US 11,459,327 · App. 17/303,762 · Granted Oct 4, 2022

Cycloalkyl and hetero-cycloalkyl inhibitors, preparation methods therefor, and use thereof

Inventors: Binhua Lv (Shanghai, CN); Dawei Cui (Shanghai, CN); Lianjun Liu (Shanghai, CN); Tao Han (Shanghai, CN); Runqing Wang (Shanghai, CN); Peizhong Ni (Shanghai, CN); Zelin Sheng (Shanghai, CN)
Assignees: Suzhou Zelgen Biopharmaceuticals Co., Ltd.; Shanghai Zelgen Pharma.Tech Co., Ltd.
C07D471/04
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Quick Facts
Patent No.
US 11,459,327
App. No.
17/303,762
Filed
Jun 7, 2021
Granted
Oct 4, 2022
Kind
B1
Art Unit
1625
USPC
514/210.21
Abstract

Cycloalkyl and hetero-cycloalkyl inhibitors, preparation methods therefor, and the use thereof are described. Compounds of the present invention have a structure represented by formula (I). Further disclosed are preparation methods for said compounds, and the use of said compounds as KRAS G12C inhibitors. The compounds have an excellent ability to selectively inhibit KRAS G12C , improved pharmacodynamic and pharmacokinetic performance, and reduced toxic side effects.

Claims (31)

1. A compound of formula (I), and the stereoisomer, tautomer, crystal form, pharmaceutically acceptable salt, hydrate, solvate or prodrug thereof,

wherein:

A and B are N;

X is selected from 4-14 membered saturated or unsaturated heterocyclyl, wherein said saturated or unsaturated heterocyclyl may optionally be substituted by one or more R 8 ;

Y is O;

L is bond;

Z is bond;

W is bond;

R 1 is —C(O)C(R A ) C(R B ) p ;

R A is absent, or is independently selected from hydrogen, deuterium, fluorine, cyano or C 1 -C 3 alkyl;

R B is independently selected from hydrogen, deuterium, cyano or C 1 -C 3 alkyl;

p is an integer of 1 or 2;

R 2 is —(CH 2 ) n R 7 , where H in CH 2 is optionally substituted;

R 7 is selected from substituted C 3 -C 20 cycloalkyl or substituted 4-20 membered heterocyclyl; wherein “substituted” refers to substitution with one or more groups selected from the group consisting of C 1 -C 18 alkyl, deuterated C 1 -C 18 alkyl, and amino; and the C 1 -C 18 alkyl or deuterated C 1 -C 18 alkyl is substituted by one or more substituents selected from the group consisting of deuterium, halogen, cyano, amino, C 3 -C 7 cycloalkyl, 4-7 membered heterocyclyl, NHR 9 and NR 9 R 10 ; R 9 and R 10 are each independently C 1 -C 3 alkyl;

n is 1, 2, or 3;

m is an integer of 0, 1, 2 or 3;

R 3 is independently selected from the group consisting of hydrogen, deuterium, oxygen, C 1 -C 3 alkyl and C 1 -C 3 haloalkyl;

R 4 is selected from group consisting of substituted or unsubstituted C 6 -C 14 aryl and substituted or unsubstituted 5-14 membered heteroaryl;

R 5 is independently selected from substituted or unsubstituted group consisting of hydrogen, deuterium, C 1 -C 18 alkyl, deuterated C 1 -C 18 alkyl, C 1 -C 18 haloalkyl, C 3 -C 20 cycloalkyl, C 1 -C 18 alkoxy, deuterated C 1 -C 18 alkoxy, C 1 -C 18 haloalkoxy, amino, hydroxyl, 4-20 membered heterocyclyl;

R 8 is independently selected from hydrogen, deuterium, C 1 -C 6 alkyl, or CNCH 2 —;

wherein, the above “substituted” refers to be substituted with one or more groups selected from the group consisting of hydrogen, deuterium, C 1 -C 18 alkyl, deuterated C 1 -C 18 alkyl, C 1 -C 18 haloalkyl, C 3 -C 20 cycloalkyl, C 1 -C 18 alkoxy, deuterated C 1 -C 18 alkoxy, C 1 -C 18 haloalkoxy, C 6 -C 14 aryl, 5-14 membered heteroaryl, 4-20 membered heterocyclyl, halogen, nitro, hydroxy, cyano, ester, amino, amido, sulfonamido and ureido.

2. The compound, and the stereoisomer, tautomer, crystal form, pharmaceutically acceptable salt, hydrate, solvate or prodrug thereof of claim 1 , wherein it has a structure represented by formula (VIII):

R 11 and R 12 are the same or different, and each independently selected from hydrogen, deuterium, C 1 -C 18 alkyl, deuterated C 1 -C 18 alkyl;

ring A is a substituted or unsubstituted C 3 -C 20 cycloalkyl or a substituted or unsubstituted 4-20 membered heterocyclyl; and

L 1 is C 1 -C 18 alkyl, or deuterated C 1 -C 18 alkyl;

Q is C 3 -C 7 cycloalkyl, 4-7 membered heterocyclyl, NHR 9 or NR 9 R 10 ; R 9 and R 10 are each independently C 1 -C 3 alkyl.

3. A compound is selected from the group consisting of:

or a stereoisomer, tautomer, crystal form, pharmaceutically acceptable salt, hydrate, solvate or prodrug thereof.

4. A pharmaceutical composition comprises one or more of the compound, the stereoisomer, tautomer, crystal form, pharmaceutically acceptable salt, hydrate, solvate or prodrug thereof of claim 1 ; and a pharmaceutically acceptable carrier.

5. The compound, and the stereoisomer, tautomer, crystal form, pharmaceutically acceptable salt, hydrate, solvate or prodrug thereof of claim 2 , wherein R 4 is

6. The compound, and the stereoisomer, tautomer, crystal form, pharmaceutically acceptable salt, hydrate, solvate or prodrug thereof of claim 2 , wherein the compound is selected from the group consisting of:

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 7, 2021
From: LV, BINHUA; CUI, DAWEI; LIU, LIANJUN; HAN, TAO; WANG, RUNQING; NI, PEIZHONG; SHENG, ZELIN
To: SUZHOU ZELGEN BIOPHARMACEUTICALS CO., LTD.; SHANGHAI ZELGEN PHARMA.TECH CO., LTD.
Reel/Frame 056459/0102 →
Priority Claims (2)
CN 201911013680.X · Oct 23, 2019 · national
CN 201911330659.2 · Dec 20, 2019 · national
Continuity (1)
Continuation PCTCN2020138142 · Dec 21, 2020
Cited By (9)
US 12,291,538 US 12,297,208 US 12,466,840 US 12,479,834 US 12,630,559 US 12,643,885 US 12,673,041 US 12,702,658 US 12,735,425