Freeze-drying system and method therefor
View Patent ↗The invention relates to a freeze-drying system for drying products containing liquid and to a method for operating a freeze-drying system, said freeze-drying system having a vacuum chamber, in which at least one holding device for holding the products containing liquid is inserted, a coolable condenser being provided, on which liquid drawn from the product in a drying phase can be condensed from a vapor phase. According to the invention, at least one sound generator is arranged on the holding device, by means of which sound generator sound can be applied to the product during the drying phase.
1. A freeze-drying system for freeze-drying products containing liquid, wherein in a drying phase the products are kept at a temperature below or close to the freezing point of the liquid and exposed to a low-pressure atmosphere, so that drying by sublimation of the frozen liquid takes place, the freeze-drying system comprising:
a vacuum chamber in which at least one reception device for receiving the products containing liquid is introduced; and
at least one sound generator by which the products can be treated with sound during the drying phase is arranged at the reception device;
wherein a coolable condenser is present at which liquid withdrawn from the products in the drying phase can be precipitated from a vapor phase; and
the reception device comprises a conducting device for conducting a fluid to cool or to heat the products at the reception device, with the sound generator being arranged at the conducting device and designed to send a sound into the fluid.
2. The freeze-drying system in accordance with claim 1 , wherein the reception device comprises one or more reception plates, with the products being able to be placed on an upper side of the reception plate, and with the at least one sound generator being arranged at a lower side of the reception plate disposed opposite the upper side.
3. The freeze-drying system in accordance with claim 1 , wherein a reception space is formed in the vacuum chamber, with the condenser being introduced in the reception space together with the reception device and the products.
4. The freeze-drying system in accordance with claim 1 , wherein the condenser is spatially formed such that is surrounds the reception device at an outer side.
5. The freeze-drying system in accordance with claim 1 , wherein the reception device comprises a reception plate that is formed by a base plate of the vacuum chamber.
6. The freeze-drying system in accordance with claim 1 , wherein the sound generator forms an ultrasound generator and sends a sound into the products at a sound frequency of at least 16 kHz by a solid-borne sound transfer in a reception plate of the reception device and/or via a fluid column of the fluid in a fluid line.
7. A method of freeze-drying products containing liquid using a freeze-drying system, wherein in a drying phase the products are kept at a temperature below or close to the freezing point of the liquid and exposed to a low-pressure atmosphere, so that drying by sublimation of the frozen liquid takes place, the freeze-drying system comprising:
at least one sound generator arranged at a reception device for receiving the products containing liquid in a vacuum chamber and with the products being treated with sound during the drying phase by a sound wave conducting through at least a part of the reception device by the sound generator; and
wherein the reception device comprises a conducting device for conducting a fluid to cool or to heat the products at the reception device, with the sound generator being arranged at the conducting device and sending a sound into the fluid so that the sound is conducted through the fluid to a reception plate of the reception device and thus to the products.