IP Library Granted Patent US 11,548,907
Granted Patent B2
US 11,548,907 · App. 17/036,995 · Granted Jan 10, 2023

Method for producing allulose crystals

Inventors: Krishnan Viswanathan Iyer (Champaign, IL); James Gaddy (Algonquin, IL); Jerry Lynn Turner (Shelbyville, IL); Brian Timothy Pohrte (St. Charles, IL)
Assignee: Tate & Lyle Solutions USA LLC
C07H3/02A23L27/33C07H1/06C07B2200/13
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Quick Facts
Patent No.
US 11,548,907
App. No.
17/036,995
Granted
Jan 10, 2023
Kind
B2
Abstract

Allulose crystals are efficiently produced from an allulose syrup using seed crystals.

Claims (24)

1. A purified allulose crystal product, wherein the purified allulose crystal product has a purity of at least 90% by dry weight of the crystals, an average particle size of at least 100 microns, and one or more particles smaller than 75 microns in size in less than 25% by dry weight of the purified allulose crystal product.

2. The purified crystal product of claim 1 , wherein the purified allulose crystal product has a purity of at least 95% by dry weight of the crystals.

3. The purified crystal product of claim 1 , wherein the purified allulose crystal product has a purity of at least 99% by dry weight of the crystals.

4. The purified crystal product of claim 1 , wherein the purified allulose crystal product has an average particle size of at least 200 microns.

5. The purified crystal product of claim 1 , wherein the purified allulose crystal product has an average particle size of at least 250 microns.

6. The purified crystal product of claim 1 , wherein the purified allulose crystal product has an average particle size of from 250 to 350 microns.

7. The purified crystal product of claim 1 , wherein the purified allulose crystal product has a bulk density greater than 30 lb/ft 3 .

8. The purified crystal product of claim 1 , wherein the purified allulose crystal product has a bulk density greater than 35 lb/ft 3 .

9. The purified allulose crystal product of claim 1 , wherein crystals in the purified allulose crystal product have a well-defined three-dimensional shape.

10. A tabletop sweetener comprising the purified allulose crystal product of claim 1 .

11. A product for human and/or animal consumption comprising the purified allulose crystal product of claim 1 and at least one additional ingredient selected from the group consisting of flavorants, colorants, sweeteners other than allulose, carbohydrates, sucrose, fructose, allose, tagatose, synthetic sweeteners, sucralose, acesulfame K, saccharin, aspartame, natural high potcncy sweeteners, stevia extract sweeteners, monk fruit extract sweeteners, terpene glycosides, steviol glycosides, mogrosides, rebaudioside A, rebaudioside B, rebaudioside C, rebaudioside D, rebaudioside E, rebaudioside F, rebaudioside G, rebaudioside H, rebaudioside I, rebaudioside J, rebaudioside K, rebaudioside L, rebaudioside M, rebaudioside N, rebaudioside O, stevioside, steviolmonoside, steviolbioside, dulcoside A, dulcoside B, rubusoside, glycosylated steviol glycosides, enzyme-modified steviol glycosides, mogroside II A, mogroside II B, 7-oxomogroside II E, 11-oxomogroside A, mogroside III A 2 , 11-deoxymogroside III, 11-oxymogroside IV; A, 7-oxomogroside V, 11-oxomogroside V, mogroside V, mogroside VI, dietary fibers, soluble dietary fibers, soluble corn fiber, polydextrose, acidulants, water, and mixtures of distinct additional ingredients thereof; and

wherein the product for human and/or animal consumption is selected from the group consisting of a food product, a beverage product, a pharmaceutical product, a nutritional product, a sports product, and a cosmetic product.

12. The product for human and/or animal consumption of claim 11 , wherein the product is selected from the group consisting of a confectionary product, a chocolate product, a dessert product, a cereal product, baked goods, frozen dairy products, ice cream, meats, dairy products, yogurt, condiments, snack bars, energy bars, nutrition bars, soups, dressings, mixes, prepared foods, baby foods, diet preparations, syrups, food coatings, dried fruit, sauces, gravies, jams, jellies, a carbonated beverage, a non-carbonated beverage, fruit-flavored beverage, fruit juice, tea, milk, and coffee.

13. The product for human and/or animal consumption of claim 11 , wherein the product comprises a dry admixture of the purified allulose crystal product and the at least one additional ingredient.

14. The product for human and/or animal consumption of claim 11 , wherein the product comprises the purified allulose crystal product coated with the at least one additional ingredient.

15. A massecuite comprising mother liquor and purified allulose crystals, wherein the purified allulose crystals have a purity of at least 90% by dry weight of the purified allulose crystals, an average particle size of at least 100 microns, and one or more particles smaller than 75 microns in size in less than 25% by dry weight of the purified allulose crystals.

16. The massecuite of claim 15 , wherein the purified allulose crystals have a purity of at least 95% by dry weight of the crystals.

17. The massecuite of claim 15 , wherein the purified allulose crystals have a purity of at least 99% by dry weight of the crystals.

18. The massecuite of claim 15 , wherein the purified allulose crystals have an average particle size of at least 200 microns.

19. The massecuite of claim 15 , wherein the purified allulose crystals have an average particle size of at least 250 microns.

20. The massecuite of claim 15 , wherein the purified allulose crystals have an average particle size of from 250 to 350 microns.

21. The massecuite of claim 15 , wherein the purified allulose crystals have a bulk density greater than 30 lb/ft 3 .

22. The massecuite of claim 15 , wherein the purified allulose crystals have a bulk density greater than 35 lb/ft 3 .

23. The massecuite of claim 15 , wherein the purified allulose crystals have a well-defined three-dimensional shape.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 6, 2022
From: TATE & LYLE INGREDIENTS AMERICAS LLC
To: TATE & LYLE SOLUTIONS USA LLC
Reel/Frame 059516/0331 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 16, 2020
From: IYER, KRISHNAN VISWANATHAN; GADDY, JAMES; TURNER, JERRY LYNN; POHRTE, BRIAN TIMOTHY
To: TATE & LYLE INGREDIENTS AMERICAS LLC
Reel/Frame 054076/0795 →
Continuity (3)
Division 16341683
Provisional Application 62414280 · Oct 28, 2016
Related Publication 20210009619A1 · Jan 14, 2021