IP Library Granted Patent US 11,584,841
Granted Patent B1
US 11,584,841 · App. 16/576,517 · Granted Feb 21, 2023

Fluid-infused elastomers

Inventors: Mark C. Grubelich (Albuquerque, NM); Erica Marie Redline (Albuquerque, NM)
Assignee: National Technology & Engineering Solutions of Sandia, LLC
C08K5/02C08J7/065C08J2327/12
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Quick Facts
Patent No.
US 11,584,841
App. No.
16/576,517
Granted
Feb 21, 2023
Kind
B1
Abstract

The present invention relates to fluid-infused elastomers that outperform their non-infused base elastomer in harsh environmental conditions. These fluid-infused polymers may be used in applications including geothermal technologies where the oil-infused elastomers may be subject to harsh conditions.

Claims (25)

1. A material, consisting essentially of:

an elastomer infused with an amount of a fluid;

wherein the amount of the fluid is greater than 0% and less than or equal to 50% by volume of the material;

wherein the elastomer is selected from the group consisting of fluorocarbon, hydrocarbon, fluorosilicone and silicone-based elastomers; and

wherein the fluid is a halocarbon selected from a group consisting of fluorocarbon, chlorocarbon and bromocarbon-based oils; and

wherein the fluid is chemically inert with the elastomer; and

wherein the material has a thickness, and wherein the fluid is infused to a depth greater than the surface up to and including to a depth of 10 percent the thickness of the material.

2. The material of claim 1 , wherein the halocarbon fluid is a fluorocarbon-based fluid.

3. The material of claim 1 , wherein the fluorocarbon-based fluid is a perfluoropolyether.

4. The material of claim 1 , wherein the elastomer is a fluorocarbon-based elastomer and the fluid is a fluorocarbon-based oil.

5. The material of claim 1 , wherein the amount of the fluid is greater than 5% and less than or equal to 30% by volume of the material.

6. The material of claim 1 , wherein the material is an O-ring or gasket.

7. A method of forming a material, comprising:

subjecting the material having a surface and a thickness and consisting essentially of an elastomer to a temperature and a pressure while submerged in a halocarbon fluid to infuse an amount of the halocarbon fluid into the material to a depth greater than the surface;

wherein the elastomer is selected from the group consisting of fluorocarbon, hydrocarbon, fluorosilicone and silicone-based elastomers; and

wherein the halocarbon fluid is selected from the group consisting of fluorocarbon, chlorocarbon and bromocarbon-based oils; and

wherein the halocarbon fluid is chemically inert with the elastomer; and

wherein the material has a thickness, and wherein the fluid is infused to a depth greater than the surface up to and including to a depth of 10 percent the thickness of the material.

8. The method of claim 7 , wherein the temperature is between 100° C. and 350° C.

9. The method of claim 7 , wherein the material has a thickness, and wherein the fluid is infused to a depth greater than the surface up to and including to a depth of 50 percent the thickness of the material.

10. The method of claim 7 , wherein the fluid is infused to an amount greater than 5% and less than or equal to 30% by volume of the material.

11. The method of claim 7 , wherein the halocarbon fluid is a fluorocarbon-based fluid.

12. The method of claim 7 , wherein the fluid is a fluorocarbon-based fluid and the fluorocarbon-based fluid is a perfluoropolyether.

13. The method of claim 7 , wherein the elastomer is a fluorocarbon-based elastomer and the fluid is a fluorocarbon-based oil.

14. The method of claim 7 , wherein the infusion takes place in an infusion reactor.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 25, 2019
From: GRUBELICH, MARK C.; REDLINE, ERICA MARIE
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 051105/0105 →
CONFIRMATORY LICENSE Recorded Nov 4, 2019
From: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 050901/0920 →