IP Library Granted Patent US 11,633,709
Granted Patent B2
US 11,633,709 · App. 16/306,216 · Granted Apr 25, 2023

Treatment apparatus

Inventors: Yasunori Tsukahara (Osaka, JP); Satoshi Morikawa (Osaka, JP); Yukari Deguchi (Osaka, JP); Yuka Kotake (Osaka, JP); Hideshi Kurihara (Osaka, JP); Hisao Watanabe (Osaka, JP); Fumihiro Kayamori (Osaka, JP); Kanako Kaihara (Osaka, JP)
Assignee: Microwave Chemical Co., Ltd.
B01J19/126C07H1/00C07K1/045B01J2219/1224B01J2219/1242B01J2219/1266
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Quick Facts
Patent No.
US 11,633,709
App. No.
16/306,216
Granted
Apr 25, 2023
Kind
B2
Abstract

In order to provide a treatment apparatus that can efficiently perform microwave irradiation, a treatment apparatus includes: a vessel made of a microwave-reflecting material, and having a first end and an irradiation opening portion, which is an emitting portion of microwaves that are emitted into the vessel; a first filter located so as to partition the vessel, and configured to separate solids that are to be separated, from the contents of the vessel; and a first reflecting member located closer to the first end than the emitting portion is and so as to partition the vessel, and configured to allow at least the contents having passed through the first filter to pass through the first reflecting member, and to reflect microwaves.

Claims (41)

1. A treatment apparatus comprising:

a vessel made of a microwave-reflecting material, and having a first end and a window or an opening portion for emitting microwaves into the vessel;

a first filter located so as to partition the vessel, and configured to separate solids that are to be separated, from contents held in the vessel; and

a first reflecting member located closer to the first end than a position of the opening portion is and so as to partition the vessel, the first reflective member partitioning a space in the vessel to suppress microwave irradiation by reflecting microwave to the opposite side of the first end with respect to the first filter, and configured to allow at least one of the contents having passed through the first filter to pass through the first reflecting member or allow the at least one of the contents having passed through the first reflecting member to pass through the first filter, and to reflect the microwaves,

wherein the first reflecting member has one or more holes or opening portions through which the at least one of contents pass, wherein a diameter of each hole or opening portion is smaller than a half-wavelength of the microwaves.

2. The treatment apparatus according to claim 1 , wherein the first reflecting member is located closer to the first end than the first filter is, or between the first filter and the opening portion.

3. The treatment apparatus according to claim 1 , wherein the first filter and the first reflecting member are laid over each other.

4. The treatment apparatus according to claim 1 , wherein the first reflecting member is located between the first filter and the opening portion, and configured to allow the solid to pass through the first reflecting member.

5. The treatment apparatus according to claim 1 , wherein the first filter and the first reflecting member together configure a first reflecting filter that separates solids that are to be separated, from contents of the vessel, and that reflects microwaves.

6. The treatment apparatus according to claim 1 ,

wherein the vessel further has a second end,

the opening portion is provided between the first end and the second end of the vessel, and

the treatment apparatus further comprises:

a second filter located closer to the second end than the first filter and the first reflecting member are and so as to partition the vessel, and configured to separate solids that are to be separated, from contents of the vessel; and

a second reflecting member located closer to the second end than the first filter and the opening portion are and so as to partition the vessel, and configured to allow at least contents having passed through the second filter to pass through the second reflecting member, and to reflect microwaves.

7. The treatment apparatus according to claim 6 , wherein the second reflecting member is located closer to the second end than the second filter is, or between the second filter and the opening portion.

8. The treatment apparatus according to claim 6 , wherein the second filter is laid over the second reflecting member.

9. The treatment apparatus according to claim 6 , wherein the second reflecting member is located between the second filter and the opening portion, and configured to allow the solid to pass through the second reflecting member.

10. The treatment apparatus according to claim 6 , wherein the second filter and the second reflecting member together configure a second reflecting filter that separates solids that are to be separated, from contents of the vessel, and that reflects microwaves.

11. The treatment apparatus according to claim 1 , wherein, in the vessel, a first opening portion through which at least one of supply and discharge of contents is performed is located closer to the first end than the first filter and the first reflecting member are.

12. The treatment apparatus according to claim 6 , wherein, in the vessel, a first opening portion through which at least one of supply and discharge of contents is performed is located closer to the first end than the first filter and the first reflecting member are, and a second opening portion through which at least one of supply and discharge of contents is performed is located closer to the second end than the second filter and the second reflecting member are.

13. The treatment apparatus according to claim 11 ,

wherein the first end is a lower end of the vessel, and the first opening portion is a discharge port for discharging contents.

14. The treatment apparatus according to claim 12 , wherein microwave irradiation from the opening portion is performed between the first opening portion and the second opening portion in a state in which contents flow inside the vessel.

15. The treatment apparatus according to claim 12 , for performing:

treatment that is performed inside the vessel while supplying contents from the first opening portion and discharging the contents from the second opening portion; and

treatment that is performed inside the vessel while supplying contents from the second opening portion and discharging the contents from the first opening portion.

16. The treatment apparatus according to claim 6 ,

wherein the vessel is a cylindrical member having a first end that is open and a second end that is open,

the opening portion of the vessel is provided on a side face of the cylindrical member,

the first filter is located so as to obstruct a first end side of the cylindrical member,

the first reflecting member is located so as to obstruct a first end side of the cylindrical member,

the second filter is located so as to obstruct a second end side of the cylindrical member, and

the second reflecting member is located so as to obstruct a second end side of the cylindrical member.

17. The treatment apparatus according to claim 16 , wherein the treatment apparatus is a column.

18. The treatment apparatus according to claim 1 ,

wherein the treatment apparatus is a treatment apparatus used for solid-phase synthesis, and

the solid is a solid-phase synthesis carrier used for solid-phase synthesis.

19. The treatment apparatus according to claim 18 , wherein the solid-phase synthesis is solid-phase synthesis for synthesizing a peptide or a nucleotide chain bound to a solid-phase synthesis carrier.

20. The treatment apparatus according to claim 1 , wherein the treatment apparatus is a treatment apparatus in which microwave irradiation is performed in a multi-mode.

21. The treatment apparatus according to claim 1 , wherein the treatment apparatus further includes an irradiation unit configured to perform microwave irradiation from the opening portion into the vessel.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 3, 2018
From: TSUKAHARA, YASUNORI; MORIKAWA, SATOSHI; DEGUCHI, YUKARI; KOTAKE, YUKA; KURIHARA, HIDESHI; WATANABE, HISAO; KAYAMORI, FUMIHIRO; KAIHARA, KANAKO
To: MICROWAVE CHEMICAL CO., LTD.
Reel/Frame 047661/0406 →
Priority Claims (5)
JP JP2017-101859 · May 23, 2017 · national
JP JP2017-119846 · Jun 19, 2017 · national
JP JP2018-033004 · Feb 27, 2018 · national
JP JP2018-070798 · Apr 2, 2018 · national
JP JP2018-070799 · Apr 2, 2018 · national
Continuity (1)
Related Publication 20190329213A1 · Oct 31, 2019