IP Library Granted Patent US 11,655,448
Granted Patent B2
US 11,655,448 · App. 15/576,954 · Granted May 23, 2023

Placenta-derived matrix and methods of preparing and use thereof

Inventors: Michael Francis (Virginia Beach, VA); Silvia Chen (Virginia Beach, VA); Erick Breathwaite (Virginia Beach, VA); Rudy Rodriguez (Virginia Beach, VA); Alan Smith (Virginia Beach, VA); Alexander Huber (Virginia Beach, VA); Jung Bok Lee (Virginia Beach, VA)
Assignee: LifeNet Health
C12N5/0068C12N5/0605C12N2501/11C12N2501/113C12N2501/115C12N2501/119C12N2501/305C12N2501/31C12N2509/00C12N2533/52C12N2533/54C12N2533/90
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Quick Facts
Patent No.
US 11,655,448
App. No.
15/576,954
Granted
May 23, 2023
Kind
B2
Abstract

The invention relates to placenta-derived matrix, methods of preparing, and methods of use thereof. The invention also relates to methods of culturing cells, delivering cells, promoting differentiation of stem cells or tissue-specific progenitor cells, and repairing, replacing, regenerating, filling, reducing or inhibiting scarring of defects using the same. The invention further relates to methods of coating placenta-derived matrix on a surface or injecting the placenta-derived matrix into a site of interest.

Claims (21)

1. A method of preparing a hydrogel obtained from a placental tissue, said method comprising

(a) devitalizing a placenta tissue to produce a devitalized placenta tissue,

(b) digesting the devitalized placenta tissue in a digestion solution having a pepsin and hydrochloric acid (HCl) to produce a placenta-derived matrix,

(c) adjusting pH of the placenta-derived matrix from step (b) to a basic pH of 8.0 to 11.0 to irreversibly inactivate the pepsin,

(d) adjusting the pH of the placenta-derived matrix from step (c) to a neutral pH of 7.0 to 7.2 to prepare a first neutralized placenta-derived matrix,

(e) freeze-drying the first neutralized placenta-derived matrix to produce a sponge structure,

(f) dissolving the sponge structure in an acetic acid solvent to form a second placenta-derived matrix,

(g) adjusting the pH of the second placenta-derived matrix from step (f) to a neutral pH of 7.0 to 7.2 to prepare a second neutralized placenta-derived matrix, and

(h) adjusting the temperature of the second neutralized placenta-derived matrix to 36 to 38° C. to produce the hydrogel.

2. The method of claim 1 , wherein step (a) comprises treating the placenta tissue with a non-denaturing detergent.

3. The method of claim 1 , further comprising homogenizing the devitalized placenta tissue concurrently with or before digesting the devitalized placenta tissue of step (b).

4. The method of claim 3 , wherein the devitalized placenta tissue is homogenized at 4° C.

5. The method of claim 1 , wherein the concentration of pepsin in the digestive solution is from 400 to 700 units/ml, and the concentration of HCl in the digestive solution is 0.01M-1.0M.

6. The method of claim 1 , further comprising storing cells on or in the hydrogel.

7. The method of claim 6 , wherein the cells on or in the hydrogel is stored by cryopreservation.

8. The method of claim 1 , further comprising exposing a protein to the hydrogel.

9. The method of claim 1 , further comprising

(a) mixing cells in the hydrogel to produce a mixture, and

(b) injecting the mixture into a site of interest.

10. The method of claim 1 , further comprising culturing pluripotent stem cells or tissue-specific progenitor cells on or within the hydrogel.

11. The method of claim 1 , further comprising coating at least a part of a surface of a substrate with the hydrogel.

Assignments (3)
SECURITY INTEREST Recorded Apr 2, 2021
From: LIFENET HEALTH; SKIN AND WOUND ALLOGRAFT INSTITUTE, LLC
To: TRUIST BANK
Reel/Frame 055815/0623 →
SECURITY INTEREST Recorded Jun 10, 2019
From: LIFENET HEALTH; SKIN AND WOUND ALLOGRAFT INSTITUTE, LLC
To: SUNTRUST BANK
Reel/Frame 049424/0312 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 31, 2018
From: FRANCIS, MICHAEL; CHEN, SILVIA; BREATHWAITE, ERICK; RODRIGUEZ, RUDY; SMITH, ALAN; HUBER, ALEXANDER; LEE, JUNG BOK
To: LIFENET HEALTH
Reel/Frame 045943/0922 →
Continuity (2)
Provisional Application 62168397 · May 29, 2015
Related Publication 20180155678A1 · Jun 7, 2018