IP Library Granted Patent US 11,905,656
Granted Patent B2
US 11,905,656 · App. 17/405,028 · Granted Feb 20, 2024

Approach to biomass delignification

Inventors: Clay Purdy (Medicine Hat, CA); Markus Weissenberger (Calgary, CA); Markus Pagels (Calgary, CA); Kyle G Wynnyk (Calgary, CA); Matthew Dewit (Calgary, CA); Andrew M Corbett (Calgary, CA)
Assignee: SixRing Inc.
D21C3/04C01B15/04C09K3/00D21C3/003D21C9/163
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Quick Facts
Patent No.
US 11,905,656
App. No.
17/405,028
Granted
Feb 20, 2024
Kind
B2
Abstract

A process to separate lignin from a lignocellulosic feedstock, said process comprising the steps of: providing said lignocellulosic feedstock; providing a composition comprising; an acid; a modifying agent selected from the group consisting of: sulfamic acid; imidazole; imidazole derivatives; taurine; a taurine derivative; a taurine-related compound; alkylsulfonic acid; arylsulfonic acid; triethanolamine; and combinations thereof; a peroxide salt; and a peroxide; exposing said lignocellulosic feedstock to said composition for a period of time sufficient to depolymerize substantially all of the lignin present in said lignocellulosic feedstock into lignin oligomers and lignin monomers; wherein said process is carried out at atmospheric pressure.

Claims (17)

1. A process to separate lignin from a lignocellulosic feedstock, said process comprising the steps of:

providing said lignocellulosic feedstock;

providing a vessel;

providing a composition comprising;

an acid;

a modifying agent selected from the group consisting of: sulfamic acid; imidazole; imidazole derivatives; taurine; a taurine derivative; a taurine-related compound; alkylsulfonic acid; arylsulfonic acid; triethanolamine; and

combinations thereof;

a peroxide salt; and

a peroxide;

exposing said lignocellulosic feedstock to said composition in said vessel for a period of time sufficient to depolymerize substantially all of the lignin present in said lignocellulosic feedstock into lignin oligomers and lignin monomers;

wherein said process is carried out at atmospheric pressure.

2. The process according to claim 1 , wherein the taurine derivative or taurine-related compound is selected from the group consisting of: taurolidine; taurocholic acid; tauroselcholic acid; tauromustine; 5-taurinomethyluridine and 5-taurinomethyl-2-thiouridine; homotaurine (tramiprosate); acamprosate; and taurates.

3. The process according to claim 1 , wherein the alkylsulfonic acid is selected from the group consisting of: methanesulfonic acid; ethanesulfonic acid; sulfamic acid and combinations thereof.

4. The process according to claim 1 , wherein the arylsulfonic acid is selected from the group consisting of: orthanilic acid; metanilic acid; sulfanilic acid; benzenesulfonic acid; and toluenesulfonic acid.

5. The process according to claim 1 , wherein the initial temperature of the composition prior to the step of exposing it to the lignocellulosic feedstock is below 50° C.

6. The process according to claim 1 , wherein an amount of peroxide salt is added after a first run of separating lignin from a lignocellulosic feedstock to the remaining composition left in said vessel prior to a second run using the same composition.

7. The process according to claim 1 , wherein the peroxide salt is selected from the group consisting of: organic peroxides; hydroperoxides; inorganic peroxides; and combinations thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 5, 2024
From: PURDY, CLAY; WEISSENBERGER, MARKUS; PAGELS, MARKUS; WYNNYK, KYLE G.; DEWIT, MATTHEW; CORBETT, ANDREW M.
To: SIXRING INC.
Reel/Frame 066036/0589 →
Priority Claims (1)
CA CA 3102925 · Dec 18, 2020 · national
Continuity (1)
Related Publication 20220195664A1 · Jun 23, 2022
Cited By (7)
US 12,234,604 US 12,371,853 US 12,371,854 US 12,378,727 US 12,398,037 US 12,692,653 US 12,709,648