IP Library Granted Patent US 11,953,458
Granted Patent B2
US 11,953,458 · App. 16/811,842 · Granted Apr 9, 2024

Systems and methods utilizing sensor surface functionalization

Inventors: Mita Chattoraj (Warrenville, IL); Michael J. Murcia (Dekalb, IL); Alexander P. Mantis (Brookfield, IL); Craig W. Myers (Lisle, IL)
Assignee: Ecolab USA Inc.
G01N25/00G01K7/18G01K13/00G01N17/00G01K1/12
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,953,458
App. No.
16/811,842
Granted
Apr 9, 2024
Kind
B2
Abstract

A method for characterizing a process fluid comprising applying electrical power to a first resistance temperature detector (RTD) in contact with a fluid to increase the temperature of the first RTD; allowing the first RTD to cool toward a fluid equilibrium temperature; analyzing the temperature decay profile of the first RTD over time to determine thermal characteristics; applying electrical power to a second RTD in contact with the fluid to increase the temperature of the second RTD; allowing the second RTD to cool toward the fluid equilibrium temperature; analyzing the temperature decay profile of the second RTD over time to determine thermal characteristics; comparing the thermal characteristics of the first and second RTD to determining one or more characteristics of the fluid based; and performing a corrective action. The first RTD has a first coating and the second RTD has a second coating different than the first coating.

Claims (66)

1. A method for characterizing a process fluid comprising:

applying electrical power to a first resistance temperature detector (RTD) in contact with a fluid to increase the temperature of the first RTD, the first RTD having a first coating;

allowing the first RTD to cool toward a fluid equilibrium temperature;

analyzing the temperature decay profile of the first RTD over time as it cools toward the fluid equilibrium temperature to determine thermal characteristics of the first RTD;

applying electrical power to a second RTD in contact with the fluid to increase the temperature of the second RTD, the second RTD having a second coating different from the first coating;

allowing the second RTD to cool toward the fluid equilibrium temperature;

analyzing the temperature decay profile of the second RTD over time as it cools toward the fluid equilibrium temperature to determine thermal characteristics of the second RTD;

comparing the thermal characteristics of the first RTD and the second RTD;

determining one or more characteristics of the fluid based on the comparison; and

performing a corrective action in response to the determined one or more characteristics.

2. The method of claim 1 , wherein the first coating comprises an antimicrobial material and the second coating is not antimicrobial.

3. The method of claim 2 , wherein performing the corrective action comprises adding a biocide to the fluid.

4. The method of claim 1 , wherein the first coating is hydrophobic and the second coating is hydrophilic.

5. The method of claim 1 , wherein the first coating is roughened and the second coating is smooth.

6. The method of claim 1 , wherein the first coating is metallized and the second coating has a surface that is inert.

7. The method of claim 1 , wherein the first coating has a surface with high wettability and the second coating has a surface with a low wettability.

8. The method of claim 1 , wherein

the determined thermal characteristics of the first RTD comprise a thickness of a first deposit formed on the first RTD by the fluid;

the determined thermal characteristics of the second RTD comprise a thickness of a second deposit formed on the second RTD by the fluid; and

comparing the thermal characteristics of the first RTD and the second RTD comprises comparing the thickness of the first deposit and the thickness of the second deposit.

9. The method of claim 8 , wherein the determining one or more characteristics of the fluid is based on the comparison of the thickness of the first deposit and the thickness of the second deposit and differences between the first coating and the second coating.

10. The method of claim 8 , wherein:

the determined thermal characteristics of the first RTD comprises a rate of change of the thickness of the first deposit formed on the first RTD; and

the determined thermal characteristics of the second RTD comprises a rate of change of the thickness of the second deposit formed on the second RTD.

11. The method of claim 8 , further comprising determining a temperature dependence of deposit formation on the first RTD and the second RTD.

12. The method of claim 11 , wherein the determining a temperature dependence of deposit formation on the first RTD and the second RTD comprises:

applying electrical power to a third RTD in contact with the fluid to maintain the temperature of the third RTD at a temperature above the fluid equilibrium temperature of the fluid, the third RTD having the first coating;

allowing the third RTD to cool toward the fluid equilibrium temperature;

analyzing the temperature decay profile of the third RTD over time as it cools toward the fluid equilibrium temperature to determine thermal characteristics of the third RTD; and

comparing the thermal characteristics of the first RTD and the third RTD.

13. A system comprising:

a first resistance temperature detector (RTD), the first RTD having a first coating;

a second RTD, the second RTD not having the first coating;

a power source in communication with the first RTD and being configured to provide electrical power to the first RTD; and

a controller in communication with the first RTD and the power source and being configured to:

cause the power source to provide electrical power to the first RTD;

stop applying electrical power to the first RTD:

measure the temperature of the first RTD over time after stopping applying the electrical power to the first RTD;

measure a thermal characteristic of the first RTD based on the measured temperature over time;

cause the power source to provide electrical power to the second RTD;

stop applying electrical power to the second RTD;

measure the temperature of the second RTD over time after stopping applying the electrical power to the second RTD;

measure a thermal characteristic of the second RTD based on the measured temperature over time;

compare the measured thermal characteristic of the second RTD to the measured characteristic of the first RTD;

determine one or more characteristics of a fluid in contact with the first RTD based on the comparison between the thermal characteristics of the first RTD and the second RTD, and

perform a corrective action in response to the one or more determined characteristics.

14. The system of claim 13 , wherein the first coating comprises a swellable polymer, and wherein determining one or more characteristics of the fluid comprises determining a concentration of a constituent in the fluid that is absorbable by the swellable polymer.

15. The system of claim 13 , wherein the first coating comprises an antimicrobial coating, and wherein determining one or more characteristics of the fluid comprises determining the presence of microbes in the fluid.

16. The system of claim 15 , wherein the controller is configured to cause a biocide to be applied to the fluid if microbes are determined to be present in the fluid.

17. The system of claim 13 , wherein the first coating comprises a metalized surface susceptible to corrosion, and wherein determining one or more characteristics of the fluid comprises determining a corrosivity the fluid.

18. The system of claim 13 , wherein

the measuring the thermal characteristic of the first RTD comprises measuring a thermal decay characteristic of the first RTD when power is stopped being applied to the first RTD; and

the measuring the thermal characteristic of the second RTD comprises measuring a thermal decay characteristic of the second RTD when power is stopped being applied to the second RTD.

19. A system comprising:

a first resistance temperature detector (RTD), the first RTD having a first coating;

a power source in communication with the first RTD and being configured to provide electrical power to the first RTD; and

a controller in communication with the first RTD and the power source and being configured to:

cause the power source to provide electrical power to the first RTD;

stop applying electrical power to the first RTD:

measure the temperature of the first RTD over time after stopping applying the electrical power to the first RTD;

measure a thermal characteristic of the first RTD based on the measured temperature over time;

determine one or more characteristics of a fluid in contact with the first RTD based on the measured thermal characteristic of the first RTD; and

perform a corrective action in response to the one or more determined characteristics; and wherein

first coating comprises a swellable polymer; and

determining one or more characteristics of the fluid comprises determining a concentration of a constituent in the fluid that is absorbable by the swellable polymer.

20. The system of claim 19 , wherein the controller is configured to determine one or more thermal characteristics of the swellable polymer, the one or more thermal characteristics being associated with the concentration of the constituent in the fluid.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2020
From: CHATTORAJ, MITA; MURCIA, MICHAEL J.; MANTIS, ALEXANDER P.; MYERS, CRAIG W.
To: ECOLAB USA INC.
Reel/Frame 052048/0242 →
Continuity (2)
Provisional Application 62818681 · Mar 14, 2019
Related Publication 20200292478A1 · Sep 17, 2020
Cited By (1)
US 12,347,703