Method for preparing bittern-carbonization synergistic reinforced recycled aggregate
Disclosed is a method for preparing bittern-carbonization synergistic reinforced recycled aggregate, including the following steps: spray pretreatment: performing alternate spraying on recycled aggregate with bittern and lime milk at intervals for many times at 4-70° C. and a pressure of 0.05-0.6 MPa; carbonization reinforcement: introducing waste gas containing carbon dioxide for a retention time of 4-8 h after the recycled aggregate is allowed to stand for 2-4 h; and rinsing and air drying: removing soluble impurities on a surface of the recycled aggregate by rinsing in water, and performing air-drying on the recycled aggregate to obtain bittern-carbonization synergistic reinforced recycled aggregate. According to the present disclosure, the effective reinforcement of recycled aggregate at normal temperature and pressure in a short time is realized, and the method is simple in process and is convenient in operation.
1. A method for preparing bittern-carbonization synergistic reinforced recycled aggregate, comprising the following steps:
(1) performing alternate spraying on recycled aggregate with bittern and lime milk at intervals for many times at 4-70° C. and a pressure of 0.05-0.6 MPa until a surface of the recycled aggregate is wet;
(2) introducing waste gas containing carbon dioxide for a retention time of 4-8 h after the recycled aggregate is allowed to stand for 2-4 h, a volume fraction of carbon dioxide in the waste gas being 10-20%; and
(3) removing soluble impurities on the surface of the recycled aggregate by rinsing in water, and performing air-drying on the recycled aggregate to obtain bittern-carbonization synergistic reinforced recycled aggregate.
2. The method for preparing bittern-carbonization synergistic reinforced recycled aggregate according to claim 1 , wherein in step (1), the recycled aggregate is a low-quality recycled coarse aggregate with a water-cement ratio of primary concrete of 0.3-0.45 and a particle size of 5-20 mm.
3. The method for preparing bittern-carbonization synergistic reinforced recycled aggregate according to claim 1 , wherein in step (1), a concentration of magnesium ions in bittern is ≥2.3 mol/L.
4. The method for preparing bittern-carbonization synergistic reinforced recycled aggregate according to claim 3 , wherein in step (1), a concentration of magnesium ions in bittern is 2.9-3.5 mol/L.
5. The method for preparing bittern-carbonization synergistic reinforced recycled aggregate according to claim 1 , wherein in step (1), the lime milk is a calcium hydroxide suspension, a mass percentage of calcium hydroxide being 40%-60%.
6. The method for preparing bittern-carbonization synergistic reinforced recycled aggregate according to claim 1 , wherein in step (1), a volume ratio of bittern to lime milk is 25:1-35:1, and the lime milk is sprayed at intervals of 10-30 min after the bittern is sprayed every time.
7. The method for preparing bittern-carbonization synergistic reinforced recycled aggregate according to claim 1 , wherein in step (1), the alternate spraying is performed at intervals of 1-4 h for 2-4 times.
8. The method for preparing bittern-carbonization synergistic reinforced recycled aggregate according to claim 1 , wherein in step (2), a volume fraction of carbon dioxide in the waste gas is 15-20%.
9. The method for preparing bittern-carbonization synergistic reinforced recycled aggregate according to claim 1 , wherein in step (3), the rinsing is performed for 30 min-1 h.