Micro encapsulation using high-voltage, low-current, high frequency alternating-current spray atomization
View Patent ↗Disclosed is a spray drying system and process for encapsulating a core material, such as a volatile flavor oil, within a carrier or wall material. The process is achieved by atomizing a liquid emulsion comprising the core material, the wall material, and a liquid solvent, applying a high-voltage, low-current, high frequency alternating-current charge or a high-voltage, low-current, low frequency alternating-current charge at the site of atomization, and drying the atomized emulsion into an encapsulated, free-flowing powder. Applying a high-voltage, low current alternating-current at the site of atomization allows the spray drying to be accomplished at significantly reduced temperatures, in particular, at inlet temperatures in the range of 25° C. to 150° C., and outlet temperatures in the range of 25° C. to 110° C. The low drying temperatures impart improvements in the resulting encapsulated powdered product, including better retention of volatile flavor components, a flavor profile comparable to that of the starting liquid formulation, and better hydration and dissolution in water-based applications.
1. A spray drying system for drying a liquid into a dried powder, the system comprising:
(a) a drying chamber having an inlet through which the drying chamber receives a drying gas for drying the liquid, and an outlet through which the dried powder can be collected;
(b) an atomizer adapted to receive the liquid, and arranged to atomize the liquid into the drying chamber in the form of droplets, which contact the drying gas in the drying chamber;
(c) a high-voltage alternating-current source in electrical contact with the atomizer and configured to directly impart an electrical charge to the liquid atomized by the atomizer,
wherein the electrical charge imparted to the liquid atomized by the atomizer is a high-voltage charge.
2. The system of claim 1 , wherein the high-voltage alternating-current source is a high-voltage low-current high frequency alternating-current source, where the high-frequency is in the range of 3 MHz to 30 MHz.
3. The system of claim 1 , wherein the high-voltage alternating-current source is a high-voltage low-current low frequency alternating-current source, where the low-frequency is in the range of about 50 kHz to 3 MHz.
4. The system of claim 1 , wherein a voltage of the high-voltage alternating-current source is in the range of about 2 kVAC to about 200 kVAC.
5. The system of claim 4 , wherein a current of the high-voltage low-current alternating-current power source is less than 1 mA.
6. The system of claim 4 , wherein the high-voltage alternating-current source is an electrical resonant transformer circuit.
7. The system of claim 1 , wherein the atomizer is a dual-fluid spray nozzle, a rotary atomizer nozzle, or a pressurized nozzle.
8. The system of claim 7 , wherein the atomizer further includes a liquid inlet for receiving the liquid to be atomized, and a hollow electrode that is in electrical contact with the high voltage alternating current source, and wherein the liquid inlet is coupled to the hollow electrode so that the liquid is received by and travels through the hollow electrode.
9. The system of claim 1 , wherein the system further includes a recirculation unit in communication with the inlet and the outlet of the drying chamber, the recirculation unit comprising a condenser, for processing the drying gas exiting from the outlet to remove moisture from the drying gas, and a heater, for heating the processed drying gas prior to introducing the processed drying gas to the inlet of the drying chamber.
10. The system of claim 1 , wherein the atomized droplets in the drying chamber form a spray cloud.
11. The system of claim 10 , wherein the spray cloud of droplets develops a capacitance.
12. The system of claim 11 , wherein the high-voltage alternating-current source is tuned for resonance with the capacitance developed in the spray cloud.