Freeze dryers and drying processes for materials with low water content
View Patent ↗Various embodiments of freeze dryers and drying processes are disclosed that can be used to dry materials with low water content (no more than 20 wt % water) and/or high sugar content (at least 20 wt % sugar). Such materials include candy, confections, and the like. In one embodiment, a drying process includes drying the materials without freezing them. In another embodiment, a drying process includes warming the materials before drying them. In another embodiment, a drying process includes drying two batches of materials with low water content sequentially without defrosting the interior of freeze dryer.
1. A freeze dryer comprising:
a chamber including one or more interior walls;
a vacuum pump pneumatically linked to the chamber;
a cooling system configured to cool the one or more interior walls of the chamber;
a heating system configured to heat a material in the chamber; and
an electronic controller comprising:
a processor; and
memory communicatively linked to the processor, the memory including instructions used by the processor to operate the freeze dryer;
wherein the instructions comprise a drying process including:
warming the material in the chamber at or near ambient pressure to form a warmed material; and
reducing pressure in the chamber below ambient pressure to dry the warmed material.
2. The freeze dryer of claim 1 wherein the drying process includes warming the material in the chamber at a temperature of at least 135° F. to form the warmed material.
3. The freeze dryer of claim 1 wherein the drying process includes warming the material for 1-30 minutes to form the warmed material.
4. The freeze dryer of claim 1 wherein the drying process includes drying the warmed material in the chamber below ambient pressure for 1-4 hours.
5. The freeze dryer of claim 1 wherein the drying process includes cooling the one or more interior walls of the chamber.
6. The freeze dryer of claim 5 wherein the one or more interior walls of the chamber are cooled while warming the material in the chamber.
7. The freeze dryer of claim 1 wherein the drying process includes reducing the pressure in the chamber to 5000 mTorr or below.
8. The freeze dryer of claim 1 wherein the instructions include a freeze-drying process.
9. A freeze dryer comprising:
a chamber including one or more interior walls;
a vacuum pump pneumatically linked to the chamber;
a cooling system configured to cool the one or more interior walls of the chamber;
a heating system configured to heat a material in the chamber; and
an electronic controller comprising:
a processor;
memory communicatively linked to the processor; and
a display device communicatively linked to the processor;
wherein the electronic controller is configured to:
display an option on the display device to warm the material;
receive input selecting or confirming the option to warm the material;
warm the material in the chamber at or near ambient pressure to form a warmed material; and
reduce pressure in the chamber below ambient pressure to dry the warmed material.
10. The freeze dryer of claim 9 wherein the electronic controller is configured to:
display an option on the display device to start a candy drying process; and
receive input selecting the option to begin the candy drying process.
11. The freeze dryer of claim 10 wherein the material is a first material and wherein, after the first material is dry, the electronic controller is configured to:
display an option on the display device to start another candy drying process;
receive input selecting the option to start the another candy drying process; and
reduce the pressure in the chamber below ambient pressure to dry a second material without defrosting ice on the one or more interior walls of the chamber formed by drying the first material.
12. The freeze dryer of claim 9 wherein the electronic controller is configured to display on the display device at least one adjustable process setting.
13. The freeze dryer of claim 12 wherein the at least one adjustable process setting includes a temperature at which the material is warmed in the chamber to form the warmed material.
14. The freeze dryer of claim 12 wherein the at least one adjustable process setting includes an amount of time to warm the material in the chamber to form the warmed material.
15. The freeze dryer of claim 12 wherein the at least one adjustable process setting includes an amount of time to dry the warmed material in the chamber.
16. The freeze dryer of claim 9 wherein the electronic controller is configured to cool the one or more interior walls of the chamber after receiving the input selecting or confirming the option to warm the material.
17. The freeze dryer of claim 16 wherein the electronic controller is configured to cool the one or more interior walls of the chamber while warming the material in the chamber to form the warmed material.
18. A method for drying a material in a freeze dryer, the freeze dryer comprising:
a chamber including one or more interior walls;
a vacuum pump pneumatically linked to the chamber;
a cooling system configured to cool the one or more interior walls of the chamber;
a heating system configured to heat the material in the chamber; and
an electronic controller comprising:
a processor; and
memory communicatively linked to the processor;
the method comprising:
positioning the material in the chamber of the freeze dryer;
warming the material in the chamber at or near ambient pressure to form a warmed material; and
reducing pressure in the chamber below ambient pressure to dry the warmed material.
19. The method of claim 18 wherein the material includes at least 20 wt % sugar.
20. The method of claim 18 wherein the material includes no more than 15 wt % water before warming the material.
21. The method of claim 18 wherein the material is warmed in the chamber at a temperature of at least 135° F. to form the warmed material.
22. The method of claim 18 wherein the material is warmed in the chamber for 1-30 minutes to form the warmed material.
23. The method of claim 18 wherein the warmed material is dried in the chamber below ambient pressure for approximately 1-4 hours.
24. The method of claim 18 wherein the method includes cooling the one or more interior walls of the chamber.
25. The method of claim 24 wherein the one or more interior walls of the chamber are cooled while warming the material in the chamber.
26. The method of claim 18 wherein the pressure in the chamber is reduced to 5000 mTorr or below.
27. A method for drying a material in a freeze dryer, the freeze dryer comprising:
a chamber including one or more interior walls;
a vacuum pump pneumatically linked to the chamber;
a cooling system configured to cool the one or more interior walls of the chamber;
a heating system configured to heat the material in the chamber; and
an electronic controller comprising:
a processor;
memory communicatively linked to the processor; and
a display device communicatively linked to the processor;
the method comprising:
displaying an option on the display device to warm the material;
receiving input selecting or confirming the option to warm the material;
warming the material in the chamber at or near ambient pressure to form a warmed material; and
reducing pressure in the chamber below ambient pressure to dry the warmed material.
28. The method of claim 27 wherein the material includes at least 20 wt % sugar.
29. The method of claim 27 wherein the material includes no more than 15 wt % water before warming the material.
30. The method of claim 27 comprising:
displaying an option on the display device to start a candy drying process; and
receiving input selecting the option to begin the candy drying process.
31. The method of claim 30 wherein the material is a first material and wherein, after the first material is dry, the method comprises:
displaying an option on the display device to start another candy drying process;
receiving input selecting the option to start the another candy drying process; and
reducing the pressure in the chamber below ambient pressure to dry a second material without defrosting ice on the one or more interior walls of the chamber formed by drying the first material.
32. The method of claim 27 comprising displaying on the display device at least one adjustable process setting.
33. The method of claim 32 wherein the at least one adjustable process setting includes a temperature at which the material is warmed in the chamber, the method comprising:
receiving input selecting or confirming the temperature; and
warming the material at the temperature to form the warmed material.
34. The method of claim 33 wherein the temperature is at least 135° F.
35. The method of claim 32 wherein the at least one adjustable process setting includes an amount of time to warm the material in the chamber, the method comprising:
receiving input selecting or confirming the amount of time to warm the material; and
warming the material for the amount of time to form the warmed material.
36. The method of claim 35 wherein the amount of time approximately 1-30 minutes.
37. The method of claim 32 wherein the at least one adjustable process setting includes an amount of time to dry the warmed material in the chamber, the method comprising:
receiving input selecting or confirming the amount of time to dry the warmed material; and
drying the warmed material in the chamber below ambient pressure for the amount of time.
38. The method of claim 37 wherein the amount of time is approximately 1-4 hours.
39. The method of claim 27 comprising cooling the one or more interior walls of the chamber.
40. The method of claim 27 wherein the pressure in the chamber is reduced to 5000 mTorr or below.