IP Library Granted Patent US 12,264,237
Granted Patent B2
US 12,264,237 · App. 17/157,959 · Granted Apr 1, 2025

Pressure-responsive particles, cartridge, apparatus for manufacturing printed matter, method for manufacturing printed matter, printed matter, sheet for manufacturing printed matter, and method for manufacturing sheet for manufacturing printed matter

Inventors: Yoshifumi Iida (Kanagawa, JP); Takashi Hasegawa (Kanagawa, JP); Satomi Kashiwagi (Kanagawa, JP); Takako Kobayashi (Kanagawa, JP); Satoshi Inoue (Kanagawa, JP)
Assignee: FUJIFILM Business Innovation Corp.
C08L25/14B42D15/02C08F220/1804C08F220/1808C08K3/22C08K3/36C08L33/10C09J125/14C09J133/10G03G9/0825G03G9/08711G03G9/08728G03G9/09371G03G9/09725C08K2003/2213C08K2003/2237C08K2201/003C08L2207/53
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,264,237
App. No.
17/157,959
Granted
Apr 1, 2025
Kind
B2
Abstract

Pressure-responsive particles include pressure-responsive base particles and first inorganic oxide particles, in which the pressure-responsive base particles contain a styrene-based resin which contains styrene and other vinyl monomers as polymerization components and a (meth)acrylic acid ester-based resin which contains at least two kinds of (meth)acrylic acid esters as polymerization components and in which a mass ratio of the (meth)acrylic acid esters to all polymerization components is 90% by mass or higher, Db/Da which is a ratio of a number average particle diameter Db of the first inorganic oxide particles to a number average particle diameter Da of the pressure-responsive base particles is 0.05 or higher and 0.25 or lower, the pressure-responsive particles have at least two glass transition temperatures, and a difference between a lowest glass transition temperature and a highest glass transition temperature is 30° C. or higher.

Claims (49)

1. Pressure-responsive particles comprising:

pressure-responsive base particles; and

first inorganic oxide particles,

wherein the pressure-responsive base particles contain a styrene-based resin which contains styrene and other vinyl monomers as polymerization components and a (meth)acrylic acid ester-based resin which contains at least two kinds of (meth)acrylic acid alkyl esters as polymerization components and in which a mass ratio of the (meth)acrylic acid alkyl esters to all polymerization components is 90% by mass or higher,

wherein among the at least two kinds of (meth)acrylic acid alkyl esters contained in the (meth)acrylic acid ester-based resin as polymerization components, a mass ratio between the two kinds of (meth)acrylic acid alkyl esters having the highest mass proportion is 80:20 to 20:80, and the pressure-responsive base particles have a core portion that contains the styrene-based resin and the (meth)acrylic acid ester-based resin and a shell layer that contains the styrene-based resin coats the core portion, wherein a mass ratio of styrene to all polymerization components of the styrene-based resin is 60% by mass or higher and 95% by mass or lower,

the other vinyl monomers that the styrene-based resin contains as the polymerization components include n-butyl acrylate,

the at least two kinds of (meth)acrylic acid alkyl esters contained in the (meth)acrylic acid ester-based resin as the polymerization component includes 2-ethylhexyl acrylate and n-butyl acrylate,

the first inorganic oxide particles include at least strontium titanate particles,

Db/Da which is a ratio of a number average particle diameter Db of the first inorganic oxide particles to a number average particle diameter Da of the pressure-responsive base particles is 0.05 or higher and 0.25 or lower,

the pressure-responsive particles have at least two glass transition temperatures, and

a difference between a lowest glass transition temperature and a highest glass transition temperature is 30° C. or higher.

2. The pressure-responsive particles according to claim 1 ,

wherein the first inorganic oxide particles satisfy the ratio Db/Da of 0.08 or higher and 0.20 or lower.

3. The pressure-responsive particles according to claim 1 , further comprising:

second inorganic oxide particles having a number average particle diameter of 200 nm or less.

4. The pressure-responsive particles according to claim 3 ,

wherein the second inorganic oxide particles include silica particles.

5. The pressure-responsive particles according to claim 1 ,

wherein an amount of the first inorganic oxide particles added to the exterior of the pressure-responsive base particles is 0.05 parts by mass or more and 3 parts by mass or less with respect to 100 parts by mass of the pressure-responsive base particles.

6. The pressure-responsive particles according to claim 5 ,

wherein the amount of the first inorganic oxide particles added to the exterior of the pressure-responsive base particles is 0.08 parts by mass or more and 1.5 parts by mass or less with respect to 100 parts by mass of the pressure-responsive base particles.

7. The pressure-responsive particles according to claim 1 ,

wherein the other vinyl monomers that the styrene-based resin contains as polymerization components further include 2-ethylhexyl acrylate.

8. The pressure-responsive particles according to claim 1 ,

wherein in the pressure-responsive base particles, a content of the styrene-based resin is higher than a content of the (meth)acrylic acid ester-based resin.

9. The pressure-responsive particles according to claim 1 ,

wherein the pressure-responsive base particles have a sea phase containing the styrene-based resin and island phases which are dispersed in the sea phase and contain the (meth)acrylic acid ester-based resin.

10. The pressure-responsive particles according to claim 9 ,

wherein an average diameter of the island phases is 200 nm or greater and 500 nm or less.

11. The pressure-responsive particles according to claim 1 , which have a viscosity of 10,000 Pas under a pressure of 4 MPa at a temperature of 90° C. or lower.

12. A cartridge that accommodates the pressure-responsive particles according to claim 1 and is attached to and detached from an apparatus for manufacturing a printed matter.

13. An apparatus for manufacturing a printed matter, comprising:

an arrangement unit that accommodates the pressure-responsive particles according to claim 1 and arranges the pressure-responsive particles on a recording medium; and

a crimping unit that folds and crimps the recording medium or stacks and crimps the recording medium and another recording medium together.

14. The apparatus for manufacturing a printed matter according to claim 13 , further comprising:

a color image forming unit that forms a color image on the recording medium by using a coloring material.

15. A method for manufacturing a printed matter, comprising:

arranging the pressure-responsive particles according to claim 1 on a recording medium; and

folding and crimping the recording medium or stacking and crimping the recording medium and another recording medium together.

16. The method for manufacturing a printed matter according to claim 15 , further comprising:

forming a color image on the recording medium by using a coloring material.

17. A printed matter wherein facing surfaces of a folded recording medium adhere to each other by the pressure-responsive particles according to claim 1 .

18. A printed matter wherein facing surfaces of a plurality of stacked recording media adhere to each other by the pressure-responsive particles according to claim 1 .

19. A sheet for manufacturing a printed matter, comprising:

a substrate; and

pressure-responsive particles arranged on the substrate,

wherein the pressure-responsive particles according to claim 1 are used as the pressure-responsive particles.

20. A method for manufacturing a sheet for manufacturing a printed matter, comprising:

arranging the pressure-responsive particles according to claim 1 on a substrate.

Assignments (2)
CHANGE OF NAME Recorded May 14, 2021
From: FUJI XEROX CO., LTD.
To: FUJIFILM BUSINESS INNOVATION CORP.
Reel/Frame 056237/0177 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 27, 2021
From: IIDA, YOSHIFUMI; HASEGAWA, TAKASHI; KASHIWAGI, SATOMI; KOBAYASHI, TAKAKO; INOUE, SATOSHI
To: FUJI XEROX CO., LTD.
Reel/Frame 055040/0868 →
Priority Claims (1)
JP 2020-147777 · Sep 2, 2020 · national
Continuity (1)
Related Publication 20220064424A1 · Mar 3, 2022
References Cited (29)
US 4645729A · Honda · 1987 [cited by examiner]
US 4873185A · Uchida · 1989 [cited by examiner]
US 4968574A · Morita · 1990 [cited by examiner]
US 5547796A · Kohtaki · 1996 [cited by examiner]
US 20100040393A1 · Kawahara · 2010 [cited by examiner]
US 20130030110A1 · Okada et al. · 2013 [cited by applicant]
US 20140349228A1 · Kadonome · 2014 [cited by examiner]
US 20180275544A1 · Chonan · 2018 [cited by examiner]
US 20190292412A1 · Yamasaki et al. · 2019 [cited by applicant]
EP 762223A2 · 1997 [cited by examiner]
JP S61120159 · 1986 [cited by applicant]
JP H05333590 · 1993 [cited by applicant]
JP 2000206733 · 2000 [cited by applicant]
JP 2006258901 · 2006 [cited by applicant]
JP 2007063473 · 2007 [cited by applicant]
JP 2007229993 · 2007 [cited by applicant]
JP 2012188512 · 2012 [cited by applicant]
JP 2014115505 · 2014 [cited by applicant]
JP 2015218210 · 2015 [cited by applicant]
JP 2016190446 · 2016 [cited by applicant]
JP 2018002889 · 2018 [cited by applicant]
JP 2018016714 · 2018 [cited by applicant]
JP 2018052046 · 2018 [cited by applicant]
JP 2018163198 · 2018 [cited by applicant]
JP 2018163256 · 2018 [cited by applicant]
JP 6468727 · 2019 [cited by applicant]
JP 2019167471 · 2019 [cited by applicant]
“Notice of Reasons for Refusal of Japan Counterpart Application”, issued on Apr. 2, 2024, with thereof, p. 1-p. 8. [cited by applicant]
“Office Action of China Counterpart Application”, issued on Jan. 27, 2025, with English translation thereof, p. 1-p. 28. [cited by applicant]