Systems and methods for manufacturing carbon fiber from coal
View Patent ↗Embodiments discloses herein relate to methods of processing coal. A method to process coal includes subjecting raw coal to a liquefaction process to form a pitch resin and refining the pitch resin to produce a mesophase pitch. The method further includes subjecting the mesophase pitch to a low crystallinity spinning process to form a raw fiber. The raw fiber is then further subjected to a stabilization process configured to oxygen cross-link the fiber to form a stabilized fiber and then subjecting the stabilized fiber to a carbonization process to form a carbon fiber.
1. A method of producing carbon fiber, the method comprising:
subjecting raw coal to a liquefaction process to form a pitch or a pitch resin;
refining the pitch or pitch resin to produce a mesophase pitch with a degree of anisotropy between 20% and 99%;
blending graphene with a thermoplastic blend additive and the mesophase pitch;
subjecting the mesophase pitch or pitch resin to a low-crystallinity spinning process to form raw fiber;
subjecting the raw fiber to a fiber stabilization process using oxygen to produce stabilized carbon fibers; and
subjecting the stabilized carbon fiber to a carbonization process to form a carbonized or calcinated carbon fiber.
2. The method of claim 1 , wherein the pitch or pitch resin comprises
an isotropic pitch.
3. The method of claim 1 , further comprising distilling coal tar to produce the pitch or pitch resin.
4. The method of claim 1 , further comprising heat treating coal tar to produce the pitch or pitch resin.
5. The method of claim 1 , further comprising stabilizing the raw fiber, wherein stabilizing the raw fiber includes heating the pitch to a stabilization temperature of about 280° C. and maintaining the pitch at the stabilization temperature for about 2 hours.
6. The method of claim 1 , wherein subjecting the raw fiber or stabilized fiber to a carbonization process includes heating the raw fiber to a carbonization temperature of about 1000° C. and maintaining the raw fiber at the carbonization temperature for about 30 minutes.
7. The method of claim 1 , wherein subjecting the raw fiber or stabilized fiber to a carbonization process includes heating the raw fiber in an inert gas environment.
8. The method of claim 1 , wherein the carbon fiber comprises a tensile strength of from about 1.51 GPa to about 1.64 GPa and a modulus of about 356 GPa.