IP Library Granted Patent US 12,397,282
Granted Patent B2
US 12,397,282 · App. 17/459,969 · Granted Aug 26, 2025

Trapping and sequestering of contaminants with prehydrated microparticles

Inventor: Donald J. Wagner, II (Pittsburgh, PA)
Assignee: Echo Scientific LLC
B01J20/28004B01J20/28028B01J20/28083B01J20/28085B01J20/3085C02F1/28C25B15/085C02F2303/04
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Quick Facts
Patent No.
US 12,397,282
App. No.
17/459,969
Granted
Aug 26, 2025
Kind
B2
Abstract

A method of trapping and removing contaminants from a source of contamination using a microparticle media includes the steps of: providing the microparticle media, wherein the microparticle media includes a plurality of microparticles, and wherein each of the microparticles includes a substrate having pores; prehydrating the pores of the microparticles by mixing the microparticle media with at least one of a water or water of a electrolysis supernatant solution to form a prehydrated microparticle media having a portion of the water or water of the electrolysis supernatant solution absorbed or adsorbed in the pores of the microparticles; introducing the prehydrated microparticle media to the contaminants, wherein the prehydrated microparticle media trap or bind to the contaminants; and separating the prehydrated microparticle media and the contaminants trapped or bound to the prehydrated microparticle media from the source of contamination.

Claims (30)

1. A method of trapping and removing contaminants from a source of contamination using a microparticle media comprising the steps of:

providing the microparticle media, wherein the microparticle media comprises a plurality of microparticles, and wherein each of the microparticles comprises a substrate having pores;

prehydrating the pores of the microparticles by mixing the microparticle media with at least one of a water or water of an electrolysis supernatant solution to form a prehydrated microparticle media having a portion of the water or water of the electrolysis supernatant solution absorbed in the pores of the microparticles;

introducing the prehydrated microparticle media to the contaminants, the water or water of the electrolysis supernatant solution present and absorbed in the pores of the microparticles when introducing the prehydrated microparticle media to the contaminants, wherein the prehydrated microparticle media trap or bind to the contaminants; and

separating the prehydrated microparticle media and the contaminants trapped or bound to the prehydrated microparticle media from the source of contamination.

2. The method of trapping and removing contaminants of claim 1 , wherein the prehydrated microparticle media trap or bind to the contaminants by at least one of the pores of the microparticles absorbing the contaminants, the substrate of the microparticles adsorbing the contaminants, or the water or water of the electrolysis supernatant solution in the pores of the microparticles bonding to or dissolving the contaminants.

3. The method of trapping and removing contaminants of claim 1 , wherein the microparticles of the microparticle media comprise at least one of: siliceous compounds including silica or silicates; porous carbons; metal organic framework compounds; calcites; diatomaceous earth or diatomites; zeolites or aluminosilicate minerals; clays; montmorillonite intermixes; halloysites; or cellulosic materials.

4. The method of trapping and removing contaminants of claim 1 , wherein the prehydrating step uses both the water and the water of the electrolysis supernatant solution, the method further comprising:

prehydrating the pores of the microparticles by mixing the microparticle media with the water and the water of the electrolysis supernatant solution to form a prehydrated microparticle media having a portion of the water and a portion of the water of the electrolysis supernatant solution absorbed in the pores of the microparticles, wherein the water of the electrolysis supernatant absorbed in the pores of the microparticles has a hydrogen to oxygen ratio ranging from 4:1 to about 18:1.

5. The method of trapping and removing contaminants of claim 4 , wherein the contaminants are microorganisms selected from the group consisting of neutrophiles, acidophiles, or alkaliphiles, and wherein the pH of the water of the electrolysis supernatant absorbed in the pores of the microparticles is buffered to match the pH of the surviving conditions of the microorganisms or buffered to oppose the pH of the surviving conditions of the microorganisms.

6. The method of trapping and removing contaminants of claim 1 , wherein the substrate of the microparticles of the microparticle media is treated with a surface treatment of at least one of hydrophobic functional groups, hydrophilic functional groups, or corona discharge treatment.

7. The method of trapping and removing contaminants of claim 1 , wherein the step of introducing the prehydrated microparticle media to the contaminants comprises at least one of applying the prehydrated microparticle media to, mixing the prehydrated microparticle media with, or spraying the prehydrated microparticle media on a surface or bulk solution that includes the source of contamination.

8. The method of trapping and removing contaminants of claim 1 , wherein the microparticle media further comprises non-woven fabric, wherein the microparticles are bound to the non-woven fabric.

9. The method of trapping and removing contaminants of claim 8 ,

wherein the step of introducing the prehydrated microparticle media to the contaminants includes contacting the non-woven fabric, having the microparticles bound to the non-woven fabric, to a surface that includes the source of contamination, and

wherein the step of separating the prehydrated microparticle media and the contaminants trapped or bound to the prehydrated microparticle media from the source of contamination includes wiping away the non-woven fabric from the surface that includes the source of contamination.

10. The method of trapping and removing contaminants of claim 1 , wherein the geometric structure of the microparticles is at least one of a sphere, disc, cylinder or rod, cone, cube, prism, polyhedron, or irregular structure.

11. The method of trapping and removing contaminants of claim 1 , wherein the microparticles have a particle size ranging from 0.5 micron to 175 microns.

12. The method of trapping and removing contaminants of claim 1 , wherein the geometric structure of the pores of the microparticles is at least one of a sphere, disc, cylinder or rod, cone, cube, prism, polyhedron, or irregular structure.

13. The method of trapping and removing contaminants of claim 1 , wherein the pores of the microparticles have a pore size ranging from 0.01 micron to 2 microns.

14. The method of trapping and removing contaminants of claim 1 , wherein the contaminants are at least one of microorganisms, viruses, or organic or inorganic matter.

15. A prehydrated microparticle media for trapping and removing contaminants from a source of contamination comprising:

a plurality of microparticles, wherein each of the microparticles comprises a substrate having pores; and

at least one of a water or water of an electrolysis supernatant solution absorbed in the pores of the microparticles,

wherein the water or water of the electrolysis supernatant solution is present and absorbed in the pores of the microparticles when introducing the prehydrated microparticle media to the contaminants.

16. The prehydrated microparticle media of claim 15 , wherein the prehydrated microparticle media trap or bind to the contaminants by at least one of the pores of the microparticles absorbing the contaminants, the substrate of the microparticles adsorbing the contaminants, or the water or water of the electrolysis supernatant solution in the pores of the microparticles bonding to or dissolving the contaminants.

17. The prehydrated microparticle media of claim 15 , wherein the microparticles of the prehydrated microparticle media comprise at least one of: siliceous compounds including silica or silicates; porous carbons; metal organic framework compounds; calcites; diatomaceous earth or diatomites; zeolites or aluminosilicate minerals; clays; montmorillonite intermixes; halloysites; or cellulosic materials.

18. The prehydrated microparticle media of claim 15 , wherein the water or water of the electrolysis supernatant solution absorbed in the pores of the microparticles has a hydrogen to oxygen ratio ranging from 4:1 to about 18:1.

19. The prehydrated microparticle media of claim 18 , wherein the substrate of the microparticles of the microparticle media is treated with a surface treatment of at least one of hydrophobic functional groups, hydrophilic functional groups, or corona discharge treatment.

20. The prehydrated microparticle media of claim 15 , wherein the microparticle media further comprises non-woven fabric, wherein the microparticles are bound to the non-woven fabric.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 7, 2021
From: WAGNER, DONALD J., II
To: ECHO SCIENTIFIC LLC
Reel/Frame 057397/0445 →
Continuity (3)
Provisional Application 63108658 · Nov 2, 2020
Provisional Application 63071675 · Aug 28, 2020
Related Publication 20220062859A1 · Mar 3, 2022
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