IP Library Granted Patent US 12,416,588
Granted Patent B2
US 12,416,588 · App. 17/701,431 · Granted Sep 16, 2025

Separation column inspection using off axis gamma scanning

Inventors: Daryl Hanson (San Antonio, TX); Charles Winfield (Muldoon, TX)
Assignee: Ecolab USA Inc.
G01N23/095G01N23/10G01N23/12G01N23/18G01N2223/043G01N2223/3303G01N2223/646
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Quick Facts
Patent No.
US 12,416,588
App. No.
17/701,431
Granted
Sep 16, 2025
Kind
B2
Abstract

A method of inspecting a separation vessel may utilize off axis gamma scanning. During scanning, a gamma radiation source can emit gamma radiation through a separation vessel toward a detector, and the detector can detect radiation emitted by the gamma radiation source and passing through the separation vessel. The gamma radiation source may be positioned at a first vertical elevation along the separation vessel and the detector positioned at a second vertical elevation along the separation vessel different than the first vertical elevation. As a result, a radiation path may be defined between the gamma radiation source and the detector that transects the separation vessel at a non-zero degree angle with respect to a horizontal plane.

Claims (19)

1. A method of scanning a separation vessel, the method comprising:

positioning a gamma radiation source and a detector on opposed sides of a separation vessel;

positioning the gamma radiation source and the detector at a plurality of different vertical elevation pairs along a length of the separation vessel, wherein at each of the plurality of different vertical elevation pairs the gamma radiation source is at a different vertical elevation than the detector such that a radiation path between the gamma radiation source and the detector transects the separation vessel at a non-zero degree angle, and at each of the plurality of different vertical elevation pairs a vertical distance between the gamma radiation source and the detector is substantially a same distance; and

at each of the different vertical elevation pairs, emitting gamma radiation by the gamma radiation source through the separation vessel and detecting, by the detector, radiation emitted by the gamma radiation source and passing through the separation vessel, and

wherein the separation vessel comprises a plurality of trays with a spacing defined between adjacent trays of the plurality of trays, the vertical distance between the gamma radiation source and the detector at each of the plurality of different vertical elevation pairs is less than the spacing between adjacent trays, and greater than a thickness of at least one of the plurality of trays.

2. The method of claim 1 , wherein positioning the gamma radiation source and the detector at the plurality of different vertical elevation pairs along the length of the separation vessel comprises moving the gamma radiation source and the detector at least 25 mm between each of the plurality of different vertical elevation pairs.

3. The method of claim 2 , wherein, at each of the different vertical elevation pairs, the radiation path transects at least 25 mm of vertical elevation of the separation vessel between the gamma radiation source and the detector.

4. The method of claim 1 , wherein the non-zero degree angle ranges from 2 degrees to 75 degrees with respect to a horizontal plane.

5. The method of claim 1 , wherein the separation vessel has a substantially circular cross-sectional shape, and a length of the radiation path between the gamma radiation source and the detector is substantially the same at each of the plurality of different vertical elevation pairs.

6. The method of claim 1 , further comprising determining, by a controller, a condition inside of the separation vessel based on radiation information measured by the detector.

7. The method of claim 6 , wherein the condition comprises a missing and/or damaged one of the plurality of trays.

8. The method of claim 6 , wherein the condition comprises plugging of one of the plurality of trays.

9. The method of claim 1 , wherein the thickness of at least one of the plurality of trays is 15 mm or less.

10. The method of claim 1 , further comprising positioning a second detector at a same elevation as the gamma radiation source and detecting, by the second detector, radiation emitted by the gamma radiation source and passing through the separation vessel.

11. The method of claim 1 , wherein emitting gamma radiation by the gamma radiation source through the separation vessel and detecting, by the detector, radiation emitted by the gamma radiation source and passing through the separation vessel comprises emitting gamma radiation and detecting radiation absorption during operation of the separation vessel in which fluid is fractionated.

12. The method of claim 1 , wherein positioning the gamma radiation source and the detector at the plurality of different vertical elevation pairs comprises performing a single scan at each of the plurality of different vertical elevation pairs before moving to a different one of the plurality of different vertical elevation pairs.

13. The method of claim 1 , further comprising determining, by a controller, density information inside of the separation vessel based on the equation:

I=I o e ρμx

wherein I o is an intensity of an initial radiation, I is an intensity after passing through an absorbing material, ρ is a density of the absorbing material, x is a thickness of the absorbing material, and μ is an absorption coefficient.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 23, 2022
From: HANSON, DARYL; WINFIELD, CHARLES
To: ECOLAB USA INC.
Reel/Frame 059992/0282 →
Continuity (3)
Provisional Application 63176550 · Apr 19, 2021
Provisional Application 63164034 · Mar 22, 2021
Related Publication 20220299453A1 · Sep 22, 2022
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