IP Library Granted Patent US 12,559,652
Granted Patent B2
US 12,559,652 · App. 18/021,505 · Granted Feb 24, 2026

Film including solvent barrier and primer layer

Inventors: Tianyu Wu (St. Paul, MN); Rajdeep S. Kalgutkar (Woodbury, MN); Ning Zhou (Vadnais Heights, MN); David B. Bilbrey (Woodbury, MN)
Assignee: 3M Innovative Properties Company
C09J7/29B32B27/34B32B37/15C08J7/043C09J7/20C09J7/255C09J7/38C09J7/40C09J7/50B32B2250/05B32B2250/24B32B2307/702B32B2307/75B32B2377/00C08J2477/00C09J2467/006C09J2477/001
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Quick Facts
Patent No.
US 12,559,652
App. No.
18/021,505
Granted
Feb 24, 2026
Kind
B2
Abstract

Films including solvent barriers and primer layers are described. In particular, films including a substrate, the substrate including polylactic acid, a primer layer disposed on the substrate, a barrier layer disposed on the surface of the primer layer opposite the substrate, and an adhesive layer disposed on a surface of the barrier layer opposite the primer layer. The barrier layer includes an amorphous aliphatic polyamide with a glass transition temperature of at least 40 #C. Such films can provide acceptable adhesion and barrier performance to polylactic acid based graphics film systems.

Claims (20)

1 . A film, comprising:

a substrate, the substrate including polylactic acid;

a primer layer disposed on the substrate;

a barrier layer disposed on a surface of the primer layer opposite the substrate; and

an adhesive layer disposed on a surface of the barrier layer opposite the primer layer;

wherein the barrier layer includes a polyamide;

wherein the polyamide is (i) an amorphous aliphatic polyamide,

and includes (ii) secondary amine units resulting in tertiary amide linkages.

2 . The film of claim 1 , wherein the film includes a release liner disposed on a surface of the adhesive layer opposite the barrier layer.

3 . The film of claim 1 , wherein the polyamide includes piperazine.

4 . The film of claim 1 , wherein the adhesive is a pressure sensitive adhesive.

5 . The film of claim 1 , wherein the polyamide of the barrier layer is extrudable.

6 . The film of claim 1 , wherein the polyamide of the barrier layer dissolves in a polar solvent.

7 . The film of claim 6 , wherein the polar solvent includes 1-propanol.

8 . The film of claim 6 , wherein the polar solvent includes 1-butanol.

9 . The film of claim 1 , further comprising an ink-receptive layer on a surface of the substrate opposite the primer layer.

10 . The film of claim 1 , wherein the polyamide has (iii) a glass transition temperature of at least 40° C. and at most 70° C.

11 . The film of claim 1 , wherein the film consists of the substrate, the primer layer, the barrier layer, and the adhesive layer.

12 . The film of claim 1 , wherein the barrier layer consists of a single layer of the polyamide.

13 . The film of claim 1 , wherein the barrier layer consists essentially of the polyamide.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 21, 2023
From: BILBREY, DAVID B.
To: 3M INNOVATIVE PROPERTIES COMPANY
Reel/Frame 064978/0886 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 18, 2023
From: WU, TIANYU; KALGUTKAR, RAJDEEP S.; ZHOU, NING
To: 3M INNOVATIVE PROPERTIES COMPANY
Reel/Frame 064939/0189 →
Continuity (2)
Provisional Application 63068773 · Aug 21, 2020
Related Publication 20230295391A1 · Sep 21, 2023
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