IP Library Granted Patent US 12,599,892
Granted Patent B2
US 12,599,892 · App. 18/070,525 · Granted Apr 14, 2026

Microplastic removal using adhesives

Inventors: Dimitris Ioannis Collias (Mason, OH); Anne McNeil (Ann Arbor, MI); Paul Takunda Chazovachii (Ann Arbor, MI); Woojung Ji (Ann Arbor, MI)
Assignees: The Procter & Gamble Company; The Regents of the University of Michigan
B01J20/265B01D53/0407B01J20/28028B01J20/3085C02F1/285C08F20/06C08J11/28B01D2253/202B01D2253/34B01D2257/40B01D2257/7022B01D2259/4508C02F2101/32C02F2101/34C02F2101/38C02F2103/002C02F2303/16C02F2307/12C08F2810/00C08J2333/02
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Quick Facts
Patent No.
US 12,599,892
App. No.
18/070,525
Granted
Apr 14, 2026
Kind
B2
Abstract

Articles comprising pressure-sensitive adhesives and methods of their use for removing micro- and nanoplastic particles from various media, including wastewater effluent, laundry effluent, and indoor air, are disclosed.

Claims (21)

1 . A method for removing micro- or nanoplastic particles from a medium, the method comprising contacting the micro- or nanoplastic particles in the medium with an article comprising one or more pressure-sensitive adhesives, wherein the one or more pressure-sensitive adhesives comprise a compound of formula (I) or formula (II):

wherein:

each n is independently an integer from 1 to 10,000;

each R 1 , R 2 , and R 3 , if present, is independently selected from the group consisting of:

wherein:

each m is independently an integer selected from the group consisting of 1, 2, 3, 4, 5, 6, 7, and 8;

p and q are each independently an integer selected from the group consisting of 1, 2, 3, 4, 5, 6, 7, and 8;

u is an integer selected from the group consisting of 1, 2, 3, 4, and 5;

v is an integer selected from the group consisting of 1, 2, 3, and 4;

w is an integer selected from the group consisting of 1, 2, and 3;

each R 4 is independently selected from the group consisting of H, C 1 -C 8 substituted or unsubstituted branched or straight-chain alkyl, hydroxyl, C 1 -C 8 alkoxyl, amino, cyano, —CF 3 , carbonyl, carboxyl, C 1 -C 8 alkynyl, acyl, carbamoyl, halogen, nitro, mercapto, and thiol; and

R 5 is a C 3 -C 20 branched alkyl.

2 . The method of claim 1 , wherein R 1 , R 2 , and R 3 , if present, are each independently selected from the group consisting of:

wherein p and q are each independently integers selected from the group consisting of 1, 2, 3, 4, 5, 6, 7, and 8.

3 . The method of claim 1 , wherein the pressure sensitive adhesive is made from a recycled superabsorbent polymer (SAP).

4 . The method of claim 3 , wherein the recycled SAP is degraded to poly (acrylic acid) (PAA); and wherein the PAA is derivatized to the pressure sensitive adhesive.

5 . The method of claim 1 , wherein the micro-or nanoplastic particles comprise a material selected from the group consisting of rubber, poly (isoprene), polyamide, polyester, poly (ethylene), poly (propylene), polystyrene, nylon, cellulose, poly (ethylene terephthalate), polyvinylfluoride (PVF), polyvinylidene fluoride (PVDF), poly (tetrafluoroethylene) (PTFE), polychlorotrifluoroethylene (PCTFE), perfluoroalkoxy alkane (PFA), fluorinated ethylene propylene (FEP), polyethylenetetrafluoroethylene (ETFE), polyethylenechlorotrifluoroethylene (ECTFE), perfluorinated elastomer (FFPM/FFKM), chlorotrifluoroethylenevinylidene fluoride (FPM/FKM), tetrafluoroethylene-propylene (FEPM), perfluoropolyether (PFPE), perfluorosulfonic acid (PFSA), perfluoropolyoxetane, and combinations thereof.

6 . The method of claim 1 , wherein the medium is selected from the group consisting of an aqueous medium and an atmospheric medium.

7 . The method of claim 6 , wherein the aqueous medium is selected from the group consisting of wastewater effluent from a wastewater treatment plant, laundry effluent from a commercial laundry facility, laundry effluent from a personal washing machine, and fill water in a washing machine during or after a washing cycle.

8 . The method of claim 4 , wherein the atmospheric environment is selected from the group consisting of indoor air, outdoor air, and the emissions, exhaust, and/or vent of a commercial or personal clothes dryer.

9 . The method of claim 1 , further comprising removing the micro- or nanoplastic particles from the one or more pressure-sensitive adhesives.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2025
From: MCNEIL, ANNE; CHAZOVACHII, PAUL TAKUNDA; JI, WOOJUNG
To: THE REGENTS OF THE UNIVERSITY OF MICHIGAN
Reel/Frame 071932/0325 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 30, 2022
From: COLLIAS, DIMITRIS IOANNIS
To: THE PROCTER & GAMBLE COMPANY
Reel/Frame 061916/0320 →
Continuity (3)
Continuation PCTUS2021039645 · Jun 29, 2021
Provisional Application 63045655 · Jun 29, 2020
Related Publication 20230234028A1 · Jul 27, 2023
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