IP Library Granted Patent US 12,622,985
Granted Patent B2
US 12,622,985 · App. 18/382,182 · Granted May 12, 2026

Sterilization method for medical rubber part

Inventors: Yogun Kida (Kobe, JP); Kei Tajima (Kobe, JP); Kazuki Nojiri (Kobe, JP); Yuichiro Matsutani (Kobe, JP); Shumpei Morita (Kobe, JP)
Assignee: SUMITOMO RUBBER INDUSTRIES, LTD.
A61L2/081A61L2103/23
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,622,985
App. No.
18/382,182
Granted
May 12, 2026
Kind
B2
Abstract

A sterilization method for a medical rubber part is a sterilization method for a medical rubber part that can include a body made from an elastic material and that can include an inactive resin film stacked on at least a portion of a surface of the body, where the sterilization method can include irradiating a packaging article with gamma ray, the packaging article accommodating a plurality of the medical rubber parts and having an oxygen concentration not higher than 5%.

Claims (20)

1 . A sterilization method for a medical rubber part that includes a body made from an elastic material and that includes an inactive resin film stacked on at least a portion of a surface of the body, the sterilization method comprising:

irradiating a packaging article with gamma ray, the packaging article accommodating a plurality of the medical rubber parts and having an oxygen concentration not higher than 5%,

wherein the elastic material is a cured product of a medical rubber composition containing a (a) base polymer containing a halogenated isobutylene-isoprene rubber and a proportion of the halogenated isobutylene-isoprene rubber contained in the (a) base polymer is not lower than 90% by mass.

2 . The sterilization method for the medical rubber part, according to claim 1 , further comprising irradiating a packaging article with the gamma ray, the packaging article having an oxygen concentration not higher than 3%.

3 . The sterilization method for the medical rubber part, according to claim 1 , wherein the packaging article having an oxygen concentration not higher than 5% is a packaging article in which nitrogen is sealed.

4 . The sterilization method for the medical rubber part, according to claim 1 , wherein the packaging article having an oxygen concentration not higher than 5% is a packaging article in which an oxygen adsorber is sealed.

5 . The sterilization method for the medical rubber part, according to claim 1 , further comprising performing irradiation with the gamma ray such that an absorbed dose of the gamma ray is not lower than 15 kGy.

6 . The sterilization method for the medical rubber part, according to claim 1 , wherein the elastic material has a JIS-A hardness not lower than 30 and not higher than 70, and has a compression set not higher than 20%.

7 . The sterilization method for the medical rubber part, according to claim 1 , wherein the inactive resin is polytetrafluoroethylene (PTFE), tetrafluoroethylene-ethylene copolymer, or ultrahigh-molecular-weight polyethylene.

8 . The sterilization method for the medical rubber part, according to claim 1 , wherein the inactive resin film has a thickness of 10 μm to 150 μm.

9 . The sterilization method for the medical rubber part, according to claim 1 , wherein the medical rubber part is a rubber plug for a vial, a cap or a plunger stopper for a syringe, or a rubber plug for a vacuum blood collection tube.

10 . The sterilization method for the medical rubber part, according to claim 1 , wherein the (a) base polymer consists essentially of the halogenated isobutylene-isoprene rubber.

11 . The sterilization method for the medical rubber part, according to claim 10 , wherein the medical rubber composition contains a triazine derivative as a (b) crosslinking agent.

12 . The sterilization method for the medical rubber part, according to claim 11 , wherein the (b) crosslinking agent consists essentially of the triazine derivative.

13 . The sterilization method for the medical rubber part, according to claim 12 , wherein the medical rubber composition contains no vulcanization accelerator.

14 . The sterilization method for the medical rubber part, according to claim 12 , wherein the triazine derivative includes a compound represented by a formula (1):

wherein in the formula (1):

R represents —SH, —OR 1 , —SR 2 , —NHR 3 , or —NR 4 R 5 , where R 1 , R 2 , R 3 , R 4 , and R 5 each represent an alkyl group, an alkenyl group, an aryl group, an aralkyl group, an alkylaryl group, or a cycloalkyl group,

M 1 and M 2 each represent H, Na, Li, K, ½Mg, ½Ba, ½Ca, an aliphatic primary, secondary, or tertiary amine, a quaternary ammonium salt, or a phosphonium salt.

15 . The sterilization method for the medical rubber part, according to claim 5 , wherein the irradiation is performed in a dose that falls within a range of not lower than 1.4 times 25 kGy and not higher than 2.0 times 25 kGy.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 20, 2023
From: KIDA, YOGUN; TAJIMA, KEI; NOJIRI, KAZUKI; MATSUTANI, YUICHIRO; MORITA, SHUMPEI
To: SUMITOMO RUBBER INDUSTRIES, LTD.
Reel/Frame 065293/0846 →
Priority Claims (1)
JP 2022-169472 · Oct 21, 2022 · national
Continuity (1)
Related Publication 20240189463A1 · Jun 13, 2024
References Cited (8)
US 20170197024A1 · Kiminami · 2017 [cited by examiner]
US 20170233124A1 · Fournier · 2017 [cited by examiner]
CA 2254696A1 · 1999 [cited by examiner]
ES 2545204T3 · 2015 [cited by examiner]
JP 2002301133A · 2002 [cited by applicant]
JP 2017531604A · 2017 [cited by applicant]
English translation ES-2545204-T3 (Year: 2015). [cited by examiner]
English translation of CA-2254696-A1 (Year: 1999). [cited by examiner]