IP Library › Granted Patent US 6,952,096
Granted Patent B2
US 6,952,096 · App. 10/605,069 · Granted Oct 4, 2005

Method and apparatus for determining speed and properties of flowing fluids using NMR measurements

Assignee: Schlumberger Technology Corporation
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Quick Facts
Patent No.
US 6,952,096
App. No.
10/605,069
Granted
Oct 4, 2005
Kind
B2
Abstract

A method for determining a property of a flowing fluid by nuclear magnetic resonance includes applying a static magnetic field to the flowing fluid; acquiring a suite of nuclear magnetic resonance measurements on the flowing fluid using a pulse sequence comprising a spoiling pulse, a wait time, and an acquisition pulse sequence, wherein the suite of nuclear magnetic measurements have different values for the wait time; and fitting the suite of nuclear magnetic resonance measurements to a forward model for responses of the flowing fluid to derive a parameter selected from a flow speed, longitudinal relaxation times of the flowing fluid, and a combination thereof.

Claims (138)

1. A method for determining a property of a flowing fluid by nuclear magnetic resonance, comprising:

applying a static magnetic field to the flowing fluid;

acquiring a suite of nuclear magnetic resonance measurements on the flowing fluid using a pulse sequence comprising a spoiling pulse, a wait time, and an acquisition pulse sequence, wherein the suite of nuclear magnetic measurements have different values for the wait time; and

fitting the suite of nuclear magnetic resonance measurements to a forward model for responses of the flowing fluid to derive a parameter selected from a flow speed, longitudinal relaxation times of the flowing fluid, and a combination thereof.

2. The method of claim 1 , wherein the acquisition pulse sequence comprises one selected from a spin-echo pulse sequence and a single pulse.

3. The method of claim 1 , wherein the fitting is performed by inversion of the forward model.

4. The method of claim 1 , further comprising estimating a viscosity of the flowing fluid based on the derived flow speed and a pressure drop across a selected length of a pipe in which the flowing fluid travels.

5. The method of claim 4 , wherein the estimating is according to one selected from

η

=

Δ

⁢

⁢

P

·

r

o

2

8

·

v

·

L

⁢

⁢

and

⁢

⁢

η

=

K

·

Δ

⁢

⁢

P

v

,

where η is the viscosity, ν is an average speed of the flowing fluid, L is the selected length of the pipe, ΔP is the pressure drop over the selected length of the pipe, and r o is a radius of the pipe, and K is an experimentally determined constant.

6. The method of claim 1 , further comprising estimating a viscosity of the flowing fluid based on the derived longitudinal relaxation times and a gas-oil ratio of the flowing fluid.

7. The method of claim 6 , wherein the estimating is according to:

η

o

=

kT

T

1

,

LM

·

f

⁡

(

GOR

)

where η o is the viscosity, k is an empirically determined constant for the flowing fluid, T is a temperature in Kelvin, T 1,LM is a logarithmic mean of the longitudinal relaxation times of the flowing fluid, and ƒ(GOR) is an empirically determined function of the gas-oil ratio.

8. A method for determining a property of a flowing fluid by nuclear magnetic resonance, comprising:

applying a static magnetic field to the flowing fluid;

acquiring a suite of nuclear magnetic resonance measurements on the flowing fluid using a pulse sequence comprising a longitudinal relaxation investigation pulse sequence and an acquisition pulse sequence, wherein the suite of nuclear magnetic measurements have different values for a delay time within the longitudinal relaxation investigation pulse; and

fitting the suite of nuclear magnetic resonance measurements to a forward model for responses of the flowing fluid to derive a parameter selected from a flow speed, longitudinal relaxation times of the flowing fluid, and a combination thereof.

9. The method of claim 8 , wherein the longitudinal-relaxation-investigation pulse comprises one selected from a inversion-recovery pulse sequence and a saturation-recovery pulse sequence.

10. The method of claim 8 , wherein the acquisition pulse sequence comprises one selected from a spin-echo pulse sequence and a single pulse.

11. The method of claim 8 , wherein the fitting is performed by inversion of the forward model.

12. The method of claim 8 , further comprising estimating a viscosity of the flowing fluid based on the derived flow speed and a pressure drop across a selected length of a pipe in which the flowing fluid travels.

13. The method of claim 12 , wherein the estimating is according to one selected from

η

=

Δ

⁢

⁢

P

·

r

o

2

8

·

v

·

L

⁢

⁢

and

⁢

⁢

η

=

K

·

Δ

⁢

⁢

P

v

,

where η is the viscosity, ν is an average speed of the flowing fluid, L is the selected length of the pipe, ΔP is the pressure drop over the selected length of the pipe, and r o is a radius of the pipe, and K is an experimentally determined constant.

14. The method of claim 8 , further comprising estimating a viscosity of the flowing fluid based on the derived longitudinal relaxation times and a gas-oil ratio of the flowing fluid.

15. The method of claim 14 , wherein the estimating is according to:

η

o

=

kT

T

1

,

LM

·

f

⁡

(

GOR

)

where η o is the viscosity, k is an empirically determined constant for the flowing fluid, T is a temperature in Kelvin, T 1,LM is a logarithmic mean of the longitudinal relaxation times of the flowing fluid, and ƒ(GOR) is an empirically determined function of the gas-oil ratio.

16. A method for monitoring contamination in a flowing fluid being withdrawn into a formation fluid testing tool using nuclear magnetic resonance, comprising:

applying a static magnetic field to the flowing fluid;

acquiring a suite of nuclear magnetic resonance measurements of the flowing fluid using a pulse sequence comprising a spoiling pulse, a wait time, and an acquisition pulse sequence, wherein the suite of nuclear magnetic measurements have different values for the wait time;

fitting the suite of nuclear magnetic resonance measurements to a forward model for responses of the flowing fluid to derive a property of the flowing fluid; and

monitoring a level of contamination in the flowing fluid based on the derived property of the flowing fluid.

17. The method of claim 16 , wherein the property of the flowing fluid comprises one selected from a distribution of longitudinal relaxation times, a logarithmic mean of longitudinal relaxation times, and a combination thereof.

18. The method of claim 16 , wherein the property of the flowing fluid is a viscosity.

19. A nuclear magnetic resonance apparatus, comprising:

a flow pipe including a prepolarization section and an investigation section, wherein the prepolarization section is upstream of the investigation section;

a magnet disposed around the flow pipe for creating a static magnetic field covering the prepolarization section and the investigation section;

an antenna disposed around the flow pipe at the investigation section for generating an oscillating magnetic field having a magnetic dipole substantially perpendicular to a magnetic dipole of the static magnetic field, and for receiving a nuclear magnetic resonance signal; and

a circuitry for controlling generation of the oscillating magnetic field and reception of the nuclear magnetic resonance signal by the antenna, wherein the circuitry includes a program having instructions for acquiring a suite of nuclear magnetic resonance measurements of a flowing fluid using a pulse sequence comprising a spoiling pulse, a wait time, and an acquisition pulse sequence.

20. The apparatus of claim 19 , wherein the acquisition pulse sequence comprises one selected from a spin-echo pulse sequence and a single pulse.

21. The apparatus of claim 19 , wherein the program further comprises instructions for fitting the suite of nuclear magnetic resonance measurements to a forward model for responses of a flowing fluid to derive a parameter selected from a flow speed, longitudinal relaxation times of the flowing fluid, and a combination thereof.

22. The apparatus of claim 21 , wherein the fitting is performed by inversion of the forward model.

23. The apparatus of claim 21 , wherein the program further comprising instructions for estimating a viscosity of the flowing fluid based on the derived flow speed or the derived longitudinal relaxation times.

24. A nuclear magnetic resonance apparatus, comprising:

a flow pipe including a prepolarization section and an investigation section, wherein the prepolarization section is upstream of the investigation section;

a magnet disposed around the flow pipe for creating a static magnetic field covering the prepolarization section and the investigation section;

an antenna disposed around the flow pipe at the investigation section for generating an oscillating magnetic field having a magnetic dipole substantially perpendicular to a magnetic dipole of the static magnetic field, and for receiving a nuclear magnetic resonance signal; and

a circuitry for controlling generation of the oscillating magnetic field and reception of the nuclear magnetic resonance signal by the antenna, wherein the circuitry includes a program having instructions for acquiring a suite of nuclear magnetic resonance measurements of a flowing fluid using a pulse sequence comprising a longitudinal relaxation investigation pulse sequence and an acquisition pulse sequence, wherein the suite of nuclear magnetic measurements have different values for a delay time within the longitudinal relaxation investigation pulse.

25. The apparatus of claim 24 , wherein the acquisition pulse sequence comprises one selected from a spin-echo pulse sequence and a single pulse.

26. The apparatus of claim 24 , wherein the program further comprises instructions for fitting the suite of nuclear magnetic resonance measurements to a forward model for responses of a flowing fluid to derive a parameter selected from a flow speed, longitudinal relaxation times of the flowing fluid, and a combination thereof.

27. The apparatus of claim 26 , wherein the fitting is performed by inversion of the forward model.

28. The apparatus of claim 26 , wherein the program further comprising instructions for estimating a viscosity of the flowing fluid based on the derived flow speed or the derived longitudinal relaxation times.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 5, 2003
From: FREEDMAN, ROBERT
To: SCHLUMBERGER TECHNOLOGY CORPORATION
Reel/Frame 013941/0428 →
Continuity (1)
Related Publication 20050140368A1 · Jun 30, 2005