Method for preparing a nickel-base superalloy article using a two-step salt quench
An article made of a nickel-base superalloy strengthened by the presence of a gamma-prime phase is prepared by solution heat treating the nickel-base superalloy at a solutionizing temperature above a gamma-prime solvus temperature of the nickel-base superalloy, thereafter first quenching the nickel-base superalloy in a first molten salt bath maintained at a temperature of from the gamma-prime solvus temperature to about 100° F. below the gamma-prime solvus temperature, thereafter second quenching the nickel-base superalloy in a second molten salt bath maintained at a temperature below an aging temperature of the nickel-base superalloy, and thereafter precipitation heat treating the nickel-base superalloy at the aging temperature to precipitate an aged microstructure having gamma prime phase in a nickel-base matrix.
1. A method for preparing an article made of a nickel-base superalloy strengthened by the presence of a gamma-prime phase, comprising the steps of
providing an initial article of the nickel-base superalloy; thereafter
solution heat treating the nickel-base superalloy at a solutionizing temperature above a gamma-prime solvus temperature of the nickel-base superalloy; thereafter
first quenching the nickel-base superalloy in a first molten salt bath maintained at a temperature of from the gamma-prime solvus to about 100° F. below the gamma-prime solvus temperature; thereafter
second quenching the nickel-base superalloy in a second molten salt bath maintained at a temperature below an aging temperature of the nickel-base superalloy; and thereafter
precipitation heat treating the nickel-base superalloy at the aging temperature to precipitate an aged microstructure comprising gamma prime phase in a nickel-base matrix.
2. The method of claim 1 , wherein the article has an average grain size coarser than ASTM 10 at the conclusion of the step of solution heat treating.
3. The method of claim 1 , wherein the step of providing the initial article includes the step of
providing the initial article having a largest thickness dimension of not less than about 3 inches.
4. The method of claim 1 , wherein the step of providing the initial article includes the step of
providing the article wherein a difference between a greatest section thickness and a smallest section thickness is at least about 2 inches.
5. The method of claim 1 , wherein the step of providing the initial article includes the step of
providing a gas turbine disk blank wherein a difference between a greatest section thickness and a smallest section thickness is at least about 2 inches.
6. The method of claim 1 , wherein the step of first quenching includes the step of
maintaining the nickel-base superalloy in the first molten salt bath for a time of at least about 5 minutes.
7. The method of claim 1 , wherein the step of first quenching includes the step of
maintaining the nickel-base superalloy in the first molten salt bath for a time of from about 5 to about 30 minutes.
8. The method of claim 1 , wherein the step of second quenching includes the step of
maintaining the nickel-base superalloy in the second molten salt bath for a time of at least about 10 minutes.
9. The method of claim 1 , including an additional step, after the step of second quenching and before the step of precipitation heat treating, of
cooling the nickel-base superalloy to room temperature.
10. The method of claim 1 , including an additional step, performed after the step of second quenching and before the step of precipitation heat treating, of
stabilize heat treating the nickel-base superalloy at a stabilizing temperature of from about 100° F. to about 200° F. above the aging temperature.
11. The method of claim 1 , wherein the step of precipitation heat treating includes the step of
precipitation heat treating the nickel-base superalloy to produce the aged microstructure having a volume percentage of gamma prime phase of at least about 40 percent.
12. The method of claim 1 , including an additional step, after the step of precipitation heat treating, of
machining the nickel-base superalloy.
13. A method for preparing an article made of a nickel-base superalloy strengthened by the presence of a gamma-prime phase, comprising the steps of
providing an initial article of the nickel-base superalloy; thereafter
solution heat treating, the nickel-base superalloy at a solutionizing temperature above about 2030° F.; thereafter
first quenching the nickel-base superalloy in a first molten salt bath maintained at a temperature of from about 1930° F. to about 2000° F.; thereafter
second quenching the nickel-base superalloy in a second molten salt bath maintained at a temperature of from about 900° F. to about 1300° F.; and thereafter
precipitation heat treating the nickel-base superalloy at an aging temperature of from about 1300° F. to about 1500° F.
14. The method of claim 13 , wherein the article has an average grain size coarser than ASTM 10 at the conclusion of the step of solution heat treating.
15. The method of claim 13 , wherein the step of providing the initial article includes the step of
providing a gas turbine disk blank wherein a difference between a greatest section thickness and a smallest section thickness is at least about 2 inches.
16. The method of claim 13 , including an additional step, performed after the step of second quenching and before the step of precipitation heat treating, of
stabilize heat treating the nickel-base superalloy at a stabilizing temperature of from about 100° F. to about 200° F. above the aging temperature.
17. The method of claim 13 , wherein the step of precipitation heat treating includes the step of
precipitation heat treating the nickel-base superalloy to produce the aged microstructure having a volume percentage of gamma prime phase of at least about 40 percent.
18. A method for preparing an article made of a nickel-base superalloy strengthened by the presence of a gamma-prime phase, comprising the steps of
providing a gas turbine disk initial article the nickel-base superalloy, wherein the initial article has a thickness dimension ranging from about 2 to about 7 inches; thereafter
solution heat treating the nickel-base superalloy at a solutionizing temperature of from about 2050° F. to about 2150° F.; thereafter
first quenching the nickel-base superalloy in a first molten salt bath maintained at a temperature of from about 1930° F. to about 2000° F. and maintaining the nickel-base superalloy in the first molten salt bath for a time of at least about 5 minutes; thereafter
second quenching the nickel-base superalloy in a second molten salt bath maintained at a temperature of from about 900° F. to about 1300° F. and maintaining the nickel-base superalloy in the second molten salt bath for a time of at least about 10 minutes; and thereafter
precipitation beat treating the nickel-base superalloy at an aging temperature of from about 1300° F. to about 1500° F.
19. The method of claim 18 , including an additional step, performed after the step of second quenching and before the step of precipitation heat treating, of
stabilize heat treating the nickel-base superalloy at a stabilizing temperature of from about 100° F. to about 200° F. above the aging temperature.
20. The method of claim 18 , wherein the step of precipitation heat treating includes the step of
precipitation heat treating the nickel-base superalloy to produce an aged microstructure having a volume percentage of gamma prime phase of at least about 40 percent.