IP Library › Granted Patent US 7,226,613
Granted Patent B2
US 7,226,613 · App. 10/728,653 · Granted Jun 5, 2007

Seamless filled capsules

Assignee: Symrise GmbH & Co. KG
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Quick Facts
Patent No.
US 7,226,613
App. No.
10/728,653
Granted
Jun 5, 2007
Kind
B2
Abstract

Spherical capsule having a liquid core and a seamless solid shell surrounding the core, in which: the diameter of the capsule is in the range of 4-8 mm; the thickness of the shell is in the range of 20-200 μm; the shell thickness to capsule diameter ratio is in the range of 0.004-0.04; the shell contains 70-90% (m/m) gelatin and 10-30% (m/m) plasticizer, based on the solids content of the shell; and the core has a flavoring content in the range of 1-100% (m/m), based on the total mass of the core.

Claims (43)

1. A spherical capsule comprising a liquid core and a seamless solid shell surrounding said core, wherein

the capsule has a diameter in the range of 4-8 mm,

the shell has a thickness in the range of 20-200 μm,

the shell thickness to capsule diameter ratio is in the range of 0.004-0.04,

the shell comprises 70-90% (m/m) gelatin and 10-30% (m/m) plasticizer, based on the solids content of the shell, and

the core has a flavoring content in the range of 1-100% (m/m), based on the total mass of the core, wherein the shell comprises (a) a gelatin having a Bloom value of at least 200 and (b) a gelatin having a Bloom value of 0, a fish gelatin having a Bloom value of <200, or both.

2. The capsule according to claim 1 , wherein

the diameter of the capsule is in the range of 4.5-6.5 mm,

the thickness of the shell is in the range of 50-150 μn,

the shell thickness to capsule diameter ratio is in the range of 0.01-0.03.

3. The capsule according to claim 1 , wherein the shell is prepared from a mixture containing gelatin and plasticizer which has a gel point in the range between 15° C. and 60° C.

4. The capsule according to claim 1 , wherein the fish gelatin is a cold water fish gelatin and/or has a gel point of <20° C.

5. The capsule according to claim 1 , wherein the liquid core contains a sweetener that is selected from the group that consists of thaumatin, neohesperidine, miraculin and mixtures thereof.

6. The capsule according to claim 1 , wherein the concentration of the plasticizer in the shell is 10-30% (m/m), based on the total solids content of the shell.

7. The capsule according to claim 1 , wherein the plasticizer comprises one or more polyols.

8. The capsule according to claim 1 , wherein the gelatin is selected from the group that consists of pig gelatin, cattle gelatin, chicken gelatin, fish gelatin and mixtures thereof.

9. The capsule according to claim 1 wherein the shell contains a sweetener that is selected from the group that consists of sucralose, aspartame, acesulfame K, thaumatin, Na saccharine, neohesperidin and mixtures thereof.

10. The capsule according to claim 1 , wherein the shell contains gellan gum.

11. The capsule according to claim 10 , wherein the shell contains 0.4-3% (m/m) gellan gum, based on the solids content of the shell.

12. The capsule according to claim 2 , wherein

the diameter of the capsule is in the range of 4.5-5.5 mm,

the thickness of the shell is in the range of 50-90 μm, and

the shell thickness to capsule diameter ratio is in the range of 0.01-0.02.

13. The capsule according to claim 3 , wherein the shell is prepared from a mixture containing gelatin and plasticizer which has a gel point in the range between 20° C. and 40° C.

14. The capsule according to claim 13 , wherein the shell is prepared from a mixture containing gelatin and plasticizer which has a gel point in the range between 25° C. and 35° C.

15. The capsule according to claim 1 , wherein a gelatin having a Bloom value in the range of 240-300 is used for the preparation of the shell.

16. The capsule according to claim 6 , wherein the concentration of the plasticizer in the shell is 15-20% (m/m), based on the total solids content of the shell.

17. The capsule according to claim 7 , wherein said polyol is selected from the group that consists of glycerol, propylene glycol, sorbitol and maltitol.

18. A method for the preparation of a capsule according to claim 1 , said method comprising simultaneously pumping a liquid core material and a gelatin-containing curable shell mixture through a concentric multi-component nozzle so that they drip into a cooling liquid with the formation of a capsule.

19. The method according to claim 18 , wherein said curable shell mixture comprises gelatin and plasticizer.

20. The method of claim 18 , further comprising the step of adjusting the hardness and dissolving power of the shell of said spherical capsule using a mixture consisting of (a) a gelatin having a Bloom value of at least 200 and (b) a gelatin having a Bloom value of 0 and/or a fish gelatin.

21. A spherical capsule comprising a liquid care and a seamless solid shell surrounding said core, wherein

the capsule has a diameter in the range of 4-8 mm,

the shell has a thickness in the range of 20-200 μn,

the shell thickness to capsule diameter ratio is in the range of 0.004-0.04,

the shell comprises 70-90% (m/m) gelatin and 10-30% (m/m) plasticizer, based on the solids content of the shell, and

the core has a flavoring content in the range of 1-100% (m/m), based on the total mass of the core, wherein the shell contains gellan gum.

22. A spherical capsule comprising a liquid core and a seamless solid shell surrounding said cores, wherein

the capsule has a diameter in the range of 4-8 mm,

the shell has a thickness in the range of 20-200 μm,

the shell thickness to capsule diameter ratio is in the range of 0.004-0.04,

the shell comprises 70-90% (m/m) gelatin and 10-30% (m/m) plasticizer, based on the solids content of the shell, and

the core has a flavoring content in the range of 1-100% (m/m), based on the total mass of the core, wherein the shell contains 0.4-3% (m/m) gellan gum, based on the solids content of the shell.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 16, 2004
From: SCHLEIFENBAUM, BIRGIT; VOIGT, INES; AICKELE, FRANK
To: SYMRISE GMBH & CO. KG
Reel/Frame 015214/0244 →
Priority Claims (1)
EP 02027190 · Dec 5, 2002 · regional
Continuity (1)
Related Publication 20050079215A1 · Apr 14, 2005