Method of preparing liquid compositions for delivery of N-[N- (3,3-dimethylbutyl-L-α-aspartyl]-L-phenylalanine 1-methyl ester in food and beverage systems
This invention provides a method for preparing a liquid composition of N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester comprising the steps of (a) providing a liquid carrier; and (b) mixing N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester with said liquid carrier in a ratio of up to 3:2 by weight to produce a liquid composition. The resulting liquid composition would be capable of fully dissolving or suspending neotame and may be mixed with or added to a food or beverage product in an amount effective to sweeten the food or beverage product. This invention is also directed to the novel liquid compositions prepared by the process of this invention and to the food and beverage products sweetened thereby. The liquid carriers of this invention include water, alcohol and mixtures thereof.
1. A method for preparing an alcohol-free liquid composition of N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester comprising the steps of:
(a) providing an alcohol-free liquid carrier consisting of water and a suspending agent selected from the group consisting of carboxymethyl cellulose, algin, gum arabic, carrageenan, xanthan gum, guar gum, tragancanth, hydroxypropyl methyl cellulose, methylcellulose, pectin, locust bean gum, sodium alginate, propylene glycol alginate, caramel and mixtures thereof; and
(b) mixing N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester with said alcohol-free liquid carrier, said alcohol-free liquid carrier consisting of water and a suspending agent selected from the group consisting of carboxymethyl cellulose, algin, gum arabic, carrageenan, xanthan gum, guar gum, tragancanth, hydroxypropyl methyl cellulose, methylcellulose, pectin, locust bean gum, sodium alginate, propylene glycol alginate, caramel and mixtures thereof, in a ratio of up to 3:2 to produce an alcohol-free liquid composition;
wherein the N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester is mixed until fully dissolved or suspended.
2. The method according to claim 1 , wherein the suspending agent is selected from the group consisting carboxymethyl cellulose, carrageenan, xanthan gum or tragancanth.
3. The method according to claim 1 , wherein the suspending agent may be effectively incorporated in the liquid composition in amounts of from 0.001% to about 0.5% of the total weight of the composition.
4. The method according to claim 1 , wherein neotame is present in an amount of 1% to 70% by weight of the liquid composition.
5. The method according to claim 4 , wherein neotame is present in an amount of 20% to 55% by weight of the liquid composition.
6. The method according to claim 5 , wherein neotame is present in an amount of 20% to 35% by weight of the liquid composition.
7. The method according to claim 1 , wherein the N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester is mixed with said liquid carrier at a temperature in the range of about −20° C. to about 30° C.
8. The method according to claim 7 , wherein the N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester is mixed with said liquid carrier at a temperature in the range of about −10° C. to about 10° C.
9. The liquid composition produced according to the method of claim 1 .
10. A method for preparing an alcohol-free liquid composition of N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester comprising the step of:
mixing 30% by weight of N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester with an alcohol-free liquid carrier consisting of water; wherein the N-[N-(3,3-dimethylbutyl)-L-α-aspartyl]-L-phenylalanine 1-methyl ester is mixed until fully dissolved or suspended.