IP Library Granted Patent US 7,534,283
Granted Patent B2
US 7,534,283 · App. 11/377,249 · Granted May 19, 2009

Method of producing copper powder and copper powder

Assignee: Dowa Electronics Materials., Ltd.
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Quick Facts
Patent No.
US 7,534,283
App. No.
11/377,249
Granted
May 19, 2009
Kind
B2
Abstract

A method of producing copper powder is provided that uses electrolytic cuprous oxide as the starting material for the production of copper powder suitable for a conductive filler whose particles have an average particle diameter of not greater than 1 μm or even not greater than 0.5 μm and are of uniform size. In one aspect, the method comprises a step of mixing cuprous oxide with a reducing agent in a liquor in which a protective colloid is present and to which a water-soluble copper salt has been added and in another aspect comprises a step of reducing a water-soluble copper salt in a liquor in which a protective colloid is present, thereby forming a slurry, and a step of reducing cuprous oxide in the presence of the slurry. As the water-soluble copper salt can be used, for example, 0.1-20 moles of a monovalent copper salt such as cuprous chloride per 100 moles of the cuprous oxide. As the protective colloid can be used 1-40 parts by mass of a water-soluble polymer per 100 parts by mass of the cuprous oxide.

Claims (4)

1. A method of producing copper powder comprising a step of reducing a water-soluble copper salt in a liquor in which a protective colloid is present, thereby forming a slurry including aggregates of fine copper particles, and a step of reducing cuprous oxide in the presence of the slurry, wherein the water-soluble copper salt is a monovalent water-soluble copper salt and the cuprous oxide is produced by an electrolytic method and has an average particle diameter of 3-10 μm.

2. A method of producing copper powder according to claim 1 , wherein the monovalent water-soluble copper salt is cuprous chloride.

3. A method of producing copper powder according to claim 1 , wherein 0.1-20 moles of the monovalent water-soluble copper salt are used per 100 moles of the cuprous oxide.

4. A method of producing copper powder according to claim 1 , wherein 1-40 parts by mass of a water-soluble polymer is used as the protective colloid per 100 parts by mass of the cuprous oxide.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 7, 2008
From: DOWA HOLDINGS CO., LTD.
To: DOWA ELECTRONICS MATERIALS CO., LTD.
Reel/Frame 020323/0715 →
CHANGE OF NAME Recorded Nov 5, 2007
From: DOWA MINING CO., LTD.
To: DOWA HOLDINGS CO., LTD.
Reel/Frame 020121/0161 →
CORRECTIVE ASSIGNMENT TO CORRECT THE SPELLING OF THE FIRST INVENTOR'S FIRST NAME AND THE POSTAL CODE OF THE ASSIGNEE PREVIOUSLY RECORDED ON REEL 017845 FRAME 0314. ASSIGNOR(S) HEREBY CONFIRMS THE FIRST INVENTOR'S NAME IS TOMOYA YAMADA; THE POSTAL CODE OF THE ASSIGNEE IS 101-8617. Recorded Feb 1, 2007
From: YAMADA, TOMOYA; HIRATA, KOJI
To: DOWA MINING CO., LTD.
Reel/Frame 018833/0769 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 26, 2006
From: YAMADA, YOMOYA; HIRATA, KOJI
To: DOWA MINING CO., LTD.
Reel/Frame 017845/0314 →
Priority Claims (1)
JP 2005-081871 · Mar 22, 2005 · national
Continuity (1)
Related Publication 20060213328A1 · Sep 28, 2006