IP Library Granted Patent US 7,811,391
Granted Patent B2
US 7,811,391 · App. 11/116,165 · Granted Oct 12, 2010

Composition and process for preparing protective coatings on metal substrates

Assignee: The United States of America as represented by the Secretary of the Navy
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 7,811,391
App. No.
11/116,165
Granted
Oct 12, 2010
Kind
B2
Abstract

This invention comprises an acidic aqueous solution for treating metal substrates to improve the adhesion bonding and corrosion protection of the metal surface which comprises effective amounts of water soluble trivalent chromium compounds, fluorozirconates, effective amounts of at least one corrosion inhibitors such as benzotriazole, fluorometallic compounds, zinc compounds, thickeners, surfactants, and at least about 0.001 mole per liter of the acidic solution of a polyhydroxy and/or carboxylic compound as a stabilizing agent for the aqueous solution.

Claims (2)

1. Compositions for coating metal substrates to improve the corrosion protection and adhesion bonding strength of said metal which comprise an acidic aqueous solution having a pH ranging from about 1.0 to 5.5 and per liter of said solution from about 0.01 to 100 grams of at least one trivalent chromium compound, from about 0.01 to 24 grams of at least one fluorozirconate, an effective amount of at least one water-soluble corrosion inhibitor selected from the group consisting of triazoles, benzimidazoles, benzazoles, benzoxazoles and mixtures of said inhibitors, from about 0.0 to 20 grams of divalent zinc compounds, from about 0.0 to 20 grams of surfactants, from about 0.0 to 20 grams of thickeners, and effective amount of a stabilizing compound selected from the group consisting of polyhydroxy compounds, carboxylic compounds and mixtures of polyhydroxy and carboxylic compounds, wherein the carboxylic compound is a hydroxyl-carboxylic acid and the water soluble salts thereof, wherein the hydroxyl-carboxylic acid compound is glycolic acid and the water soluble salts thereof.

2. Compositions for coating metal substrates to improve the corrosion protection and adhesion bonding strength of said metal which comprise an acidic aqueous solution having a pH ranging from about 1.0 to 5.5 and per liter of said solution from about 0.01 to 100 grams of at least one trivalent chromium compound, from about 0.01 to 24 grams of at least one fluorozirconate, an effective amount of at least one water-soluble corrosion inhibitor selected from the group consisting of triazoles, benzimidazoles, benzazoles, benzoxazoles and mixtures of said inhibitors, from about 0.0 to 20 grams of divalent zinc compounds, from about 0.0 to 20 grams of surfactants, from about 0.0 to 20 grams of thickeners, and effective amounts of a stabilizing compound selected from the group consisting of polyhydroxy compounds, carboxylic compounds and mixtures of polyhydroxy and carboxylic compounds, wherein the carboxylic compound is a hydroxyl-carboxylic acid and the water soluble salts thereof, wherein the hydroxyl-carboxylic acid compound is lactic acid and the water soluble salts thereof.

Assignments (2)
AMENDED AND RESTATED SECURITY AGREEMENT Recorded Jun 18, 2013
From: METALAST INTERNATIONAL, LLC
To: DSM PARTNERS, LTD.
Reel/Frame 030649/0578 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 21, 2005
From: MATZDORF, CRAIG A.; NICKERSON, JR., WILLIAM C.
To: U.S. OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE NAVY, THE
Reel/Frame 016508/0158 →
Continuity (2)
Continuation In Part 1111616600 · Apr 21, 2005
Related Publication 20060237098A1 · Oct 26, 2006