IP Library Granted Patent US 8,193,000
Granted Patent B2
US 8,193,000 · App. 12/336,701 · Granted Jun 5, 2012

Screening test for biodiesel fuel

Assignee: Heritage Environmental Services, LLC
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Quick Facts
Patent No.
US 8,193,000
App. No.
12/336,701
Granted
Jun 5, 2012
Kind
B2
Abstract

A colorimetric test for determining the presence or absence of biodiesel in a diesel fuel sample. The colorimetric test involves adding concentrated sulfuric acid to a sample of diesel fuel and observing any color change of the sample. A darkening of the diesel fuel sample indicates the presence of biodiesel. The degree to which the color changes after the addition of the sulfuric acid is proportional to the amount of biodiesel in the sample and therefore can be used to determine the amount of biodiesel in the sample. The reagent(s), sample containers and any necessary color scale can be provided in a kit for field testing.

Claims (18)

1. A field screening method of determining the presence or absence of biodiesel in a diesel fuel which comprises the steps of:

a) providing a diesel fuel sample;

b) combining sulfuric acid with the diesel fuel sample;

c) observing any change in color of the diesel fuel sample after the diesel fuel sample is combined with the sulfuric acid; and

d) determining, based upon the visual observation of a color change, the presence of biodiesel in the diesel fuel sample.

2. A field screening method of determining the presence or absence of biodiesel in a diesel fuel according to claim 1 , wherein the diesel fuel sample in step a) is separated into two samples, including a test sample and a reference sample, wherein the test sample is added to the sulfuric acid in step b) and the color of the test sample and reference sample are compared in step c).

3. A field screening method of determining the presence or absence of biodiesel in a diesel fuel according to claim 1 , wherein the amount of biodiesel in the diesel fuel sample is determined in step d).

4. A field screening method of determining the presence or absence of biodiesel in a diesel fuel according to claim 2 , wherein the amount of biodiesel in the diesel fuel sample is determined in step d).

5. A field screening method of determining the presence or absence of biodiesel in a diesel fuel according to claim 1 , wherein the steps are conducted in an indoor facility.

6. A field screening method of determining the presence or absence of biodiesel in a diesel fuel according to claim 1 , wherein the determination in step d) of a color change the presence of biodiesel is performed using a colorimeter.

7. A field screening method of determining the amount of biodiesel in a diesel fuel which comprises the steps of:

a) providing a diesel fuel sample;

b) combining sulfuric acid with the diesel fuel sample;

c) visually observing any change in color of the diesel fuel sample after the diesel fuel sample is combined with the sulfuric acid; and

d) determining, based upon the observation of a color change, the amount of biodiesel in the diesel fuel sample.

8. A field screening method of determining the amount of biodiesel in a diesel fuel according to claim 7 , wherein the diesel fuel sample in step a) is separated into two samples, including a test sample and a reference sample, wherein the test sample is added to the sulfuric acid in step b) and the color of the test sample and reference sample are compared in step c).

9. A field screening method of determining the amount of biodiesel in a diesel fuel according to claim 7 , wherein the steps are conducted in an indoor facility.

10. A field screening method of determining the amount of biodiesel in a diesel fuel according to claim 1 , wherein the determination in step d) of a color change the presence of biodiesel is performed using a colorimeter.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 23, 2021
From: HERITAGE RESEARCH GROUP
To: HERITAGE RESEARCH GROUP, LLC
Reel/Frame 057264/0328 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 23, 2015
From: HERITAGE ENVIRONMENTAL SERVICES LLC
To: HERITAGE RESEARCH GROUP
Reel/Frame 034801/0577 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 5, 2009
From: OSBORN, LINDA
To: HERITAGE ENVIRONMENTAL SERVICES, LLC
Reel/Frame 022348/0238 →
Continuity (2)
Provisional Application 61014461 · Dec 18, 2007
Related Publication 20090155922A1 · Jun 18, 2009