IP Library Granted Patent US 8,236,869
Granted Patent B2
US 8,236,869 · App. 12/312,128 · Granted Aug 7, 2012

Polyether polyol, rigid polyurethane foam and processes for production thereof

Assignee: Mitsui Chemicals, Inc.
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,236,869
App. No.
12/312,128
Granted
Aug 7, 2012
Kind
B2
Abstract

Highly-functionalized, low-viscosity polyether polyols are obtained by dehydration condensation reaction of alcohols. The polyether polyols are obtained by dehydration condensation of glycerin and monohydric and/or dihydric alcohol with the glycerin percentage being more than 50 mol % relative to 100 mol % of the total of the glycerin and alcohol. The glycerin may be crude glycerin obtained by hydrolysis or alcoholysis of natural fat and oils.

Claims (11)

1. A polyether polyol obtained by dehydration condensation of glycerin and monohydric and/or dihydric alcohol with the glycerin percentage being in the range of more than 50 mol % to not more than 95 mol % relative to 100 mol % of the total of the glycerin and alcohol,

wherein the polyether polyol has a hydroxyl value of 200 to 1200 mg KOH/g and a viscosity at 25° C. of not more than 50000 mPa·s.

2. The polyether polyol according to claim 1 , which has an average number of hydroxyl groups per molecule of not less than 3.

3. The polyether polyol according to claim 1 , wherein the glycerin is crude glycerin obtained by hydrolysis or alcoholysis of natural fat and oils.

4. A process for producing the polyether polyols described in claim 1 , which comprises dehydration condensing glycerin and monohydric and/or dihydric alcohol with the glycerin percentage being in the range of more than 50 mol % to not more than 95 mol % relative to 100 mol % of the total of the glycerin and alcohol.

5. A process for producing the polyether polyols described in claim 1 , which comprises dehydration condensing glycerin to produce a condensate, and dehydration condensing the condensate and monohydric and/or dihydric alcohol with the glycerin being used at a percentage in the range of more than 50 mol % to not more than 95 mol % relative to 100 mol % of the total of the glycerin and alcohol.

6. The process for producing the polyether polyols according to claim 4 or 5 , wherein the glycerin is crude glycerin obtained by hydrolysis or alcoholysis of natural fat and oils.

7. A rigid polyurethane foam obtained by reacting a polyol component comprising the polyether polyol of claim 1 and a polyisocyanate in the presence of a catalyst, a foaming agent and a foam stabilizer.

8. A rigid polyurethane foam obtained by reacting a polyol component comprising the polyether polyol of claim 3 and a polyisocyanate in the presence of a catalyst, a foaming agent and a foam stabilizer.

9. A process for producing rigid polyurethane foams, which comprises reacting a polyol component comprising the polyether polyol of claim 1 and a polyisocyanate in the presence of a catalyst, a foaming agent and a foam stabilizer.

10. A process for producing rigid polyurethane foams, which comprises reacting a polyol component comprising the polyether polyol of claim 3 and a polyisocyanate in the presence of a catalyst, a foaming agent and a foam stabilizer.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 25, 2016
From: MITSUI CHEMICALS, INC.
To: MITSUI CHEMICALS & SKC POLYURETHANES INC.
Reel/Frame 037827/0077 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2009
From: MIYATA, ATSUSHI; TSUTSUI, TOMOKI; KOGA, NOBUHITO; MATSUMOTO, SHINSUKE; OHKUBO, KAZUHIKO
To: MITSUI CHEMICALS, INC.
Reel/Frame 022617/0716 →
Priority Claims (1)
JP 2006-295658 · Oct 31, 2006 · national
Continuity (1)
Related Publication 20100029799A1 · Feb 4, 2010