IP Library Granted Patent US 8,316,917
Granted Patent B2
US 8,316,917 · App. 13/004,798 · Granted Nov 27, 2012

Solid composition having enhanced physical and electrical properties

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Quick Facts
Patent No.
US 8,316,917
App. No.
13/004,798
Granted
Nov 27, 2012
Kind
B2
Abstract

A method of making a treating wash includes mixing brass granules with acetone, mixing carbon nanotube material, iron pyrite granules and copper granules in the acetone brass mixture, and straining the liquid from the remaining solid material. Methods of treating materials such as brass granules, iron pyrite granules, carbon nanotube material, and brass granules comprises washing the materials in the treating wash, followed by straining and drying the materials.

Claims (55)

1. A method for forming a lead electrode, comprising:

providing a batch of molten lead including calcium and tin;

preparing a wash liquid comprising acetone, brass granules, carbon nanotube material, iron pyrite granules, and copper granules, mixed at high speed and strained;

treating brass granules which including about 30% zinc with the wash liquid, and straining and drying the brass granules to form treated brass granules;

treating iron pyrite granules with the wash liquid, and straining and drying the iron pyrite granules to form treated iron pyrite granules;

treating copper granules with the wash liquid, and straining and drying the copper granules to form treated copper granules;

adding the treated brass granules, the treated iron pyrite granules, and the treated copper granules to the molten lead;

pouring the molten lead alloy into a pour mold coated with a thin layer of brass granules;

allowing the lead to solidify into an ingot and then rolling the ingot in a pressure roller.

2. The method of claim 1 wherein:

providing a batch of molten lead comprises providing about 635 Kg of molten lead including calcium and tin;

preparing a wash liquid comprising acetone, brass granules, carbon nanotube material, iron pyrite granules, and copper granules, mixed at high speed and strained;

treating brass granules comprises treating about 9 Kg of brass granules having a size of about 100 mesh or finer for each about 635 Kg of molten lead;

treating iron pyrite granules comprises treating about 2.3 Kg of powdered iron pyrite having a size of about 0.025 inch or finer for each about 635 Kg of molten lead; and

treating copper granules comprises treating about 4.5 Kg of copper granules having a size of about 100 mesh or finer for each about 635 Kg of molten lead.

3. The method of claim 2 wherein preparing the wash liquid comprises:

mixing brass granules with acetone;

mixing brass granules, iron pyrite granules and copper granules in the acetone brass mixture; and

straining the liquid from the remaining solid material.

4. The method of claim 3 wherein:

mixing brass granules with acetone comprises mixing about 454 grams of brass (about 100 mesh or finer) per gallon of acetone in a commercial blender at high speed for about 10 minutes or until a gold color appears at the surface of the acetone when the blender is stopped;

mixing carbon nanotube material comprises mixing about one gram of multi-walled carbon nanotube material per gallon of acetone at high speed for about 5 minutes;

mixing iron pyrite comprises mixing about 33.5 grams of iron pyrite per gallon of acetone, the iron pyrite having an average grain size of about 0.125 inch for a minimum of about 3 minutes at high speed; and

mixing copper comprises mixing about 517 grams of copper per gallon of acetone, the copper having a mesh size of about 35 mesh or finer for about 8 minutes until a slurry begins to form on the surface after the blender is turned off.

5. The method of claim 1 wherein rolling the ingot in a pressure roller comprises rolling the ingot in a pressure roller as it is cooling.

6. The method of claim 1 wherein rolling the ingot in a pressure roller comprises rolling the ingot to a thickness of about 0.25 inches.

7. The method of claim 1 further including cutting the ingot to a finished size.

8. The method of claim 7 wherein the finished size is about 3 ft. by about 4 ft.

9. A method for forming a lead electrode, comprising:

providing a batch of molten lead including molten silver;

preparing a wash liquid comprising acetone, brass granules, carbon nanotube material, and iron pyrite granules, mixed at high speed and strained;

treating brass granules with the wash liquid, and straining and drying the brass granules to form treated brass granules;

treating iron pyrite granules with the wash liquid, and straining and drying the iron pyrite granules to form treated iron pyrite granules;

adding the treated brass granules, and the treated iron pyrite granules to the molten lead;

pouring the molten lead into a pour mold coated with a thin layer of brass granules; and

allowing the lead to solidify into an ingot and then rolling the ingot in a pressure roller.

10. The method of claim 9 wherein:

providing a batch of molten lead comprises providing about 635 Kg of molten lead;

preparing a wash liquid comprising acetone, brass granules, carbon nanotube material, iron pyrite granules, and copper granules, mixed at high speed and strained;

treating brass granules comprises treating about 11.25 Kg of brass granules and having a size of about 100 mesh or finer for each about 635 Kg of molten lead; and

treating iron pyrite granules comprises treating about 4.55 Kg of powdered iron pyrite having a size of about 0.025 inch or finer for each about 635 Kg of molten lead.

11. The method of claim 10 wherein treating brass granules comprises treating brass granules including about 30% zinc.

12. The method of claim 9 wherein providing a batch of molten lead including molten silver comprises providing a batch of molten lead including about 0.46% molten silver by weight.

13. The method of claim 9 wherein preparing the wash liquid comprises:

mixing brass granules with acetone;

mixing brass granules and iron pyrite granules in the acetone brass mixture; and

straining the liquid from the remaining solid material.

14. The method of claim 13 wherein:

mixing brass granules with acetone comprises mixing about 454 grams of brass (about 100 mesh or finer) per gallon of acetone in a commercial blender at high speed for about 10 minutes or until a gold color appears at the surface of the acetone when the blender is stopped;

mixing carbon nanotube material comprises mixing about one gram of multi-walled carbon nanotube material per gallon of acetone at high speed for about 5 minutes; and

mixing iron pyrite comprises mixing about 33.5 grams of iron pyrite per gallon of acetone, the iron pyrite having an average grain size of about 0.125 inch for a minimum of about 3 minutes at high speed.

15. The method of claim 9 wherein rolling the ingot in a pressure roller comprises rolling the ingot in a pressure roller as it is cooling.

16. The method of claim 9 wherein rolling the ingot in a pressure roller comprises rolling the ingot to a thickness of about 0.25 inches.

17. The method of claim 9 further including cutting the ingot to a finished size.

18. The method of claim 17 wherein the finished size is about 3 ft. by about 4 ft.

Assignments (2)
MERGER Recorded Jun 1, 2014
From: KRYRON GLOBAL, LLC
To: BOURQUE INDUSTRIES, INC.
Reel/Frame 033003/0106 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 22, 2014
From: BOURQUE, JOHN M.
To: KRYRON GLOBAL, LLC
Reel/Frame 032952/0702 →
Continuity (3)
Continuation 12755601 · Apr 7, 2010
Division 12268315 · Nov 10, 2008
Related Publication 20120011718A1 · Jan 19, 2012